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1.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 有权用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US07109452B2
公开(公告)日：2006-09-19
申请号：US11228767
申请日：2005-09-16
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis that includes heterogeneous or highly viscous materials includes a fluid reservoir for supplying or receiving fluids, a fluid pump in fluid communication with the reservoir for pumping fluids to or from the reservoir, a microwave transparent reaction vessel in fluid communication with the pump for supplying or receiving fluids to or from the pump and the reservoir, a pressure sensor in fluid communication with the reservoir and the vessel for measuring the pressure of fluids in the instrument at the sensor, and a processor in signal communication with the pressure sensor and the pump for controlling the pump and the flow of fluids in the instrument based at least in part on the pressure measured at the sensor.
摘要翻译： 包括异质或高粘度材料的用于化学合成的受控流微波仪器包括用于供应或接收流体的流体储存器，与储存器流体连通的流体泵，以将流体泵送到储存器或从储存器泵送流体;微波透明反应容器 与用于向泵和储存器供应或接收流体的泵的流体连通，与储存器和容器流体连通的压力传感器，用于测量传感器中仪器中的流体的压力，以及信号通信处理器 压力传感器和泵用于至少部分地基于在传感器处测量的压力来控制泵和仪器中的流体流。
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公开(公告)号：US06927371B1
公开(公告)日：2005-08-09
申请号：US09668811
申请日：2000-09-23
IPC分类号： B01J3/04 , B01J19/02 , B01J19/12 , F16J13/02 , G01N1/44 , G01N35/00 , H05B6/64 , H05B6/80 , B65D6/34
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymeric cylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding can be a filament or a yarn.
摘要翻译： 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆筒的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面的下边缘，当帽位于聚合物圆柱体上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个卷绕的织物层，其中绕组可以是丝或纱线。
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3.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 失效用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US07041947B2
公开(公告)日：2006-05-09
申请号：US10709060
申请日：2004-04-09
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis that includes heterogeneous or highly viscous materials. Includes a fluid reservoir for supplying or receiving fluids, a fluid pump in fluid communication with the reservoir for pumping fluids to or from the reservoir, a microwave transparent reaction vessel in fluid communication with the pump for supplying or receiving fluids to or from the pump and the reservoir, a pressure sensor in fluid communication with the reservoir and the vessel for measuring the pressure of fluids in the instrument at the sensor, and a processor in signal communication with the pressure sensor and the pump for controlling the pump and the flow of fluids in the instrument based at least in part on the pressure measured at the sensor.
摘要翻译： 用于化学合成的受控流微波仪器，包括异质或高粘度材料。 包括用于供应或接收流体的流体储存器，与储存器流体连通以将流体泵送到储存器的流体泵，与泵流体连通的微波透明反应容器，用于向或从泵供应或接收流体;以及 储存器，与储存器流体连通的压力传感器和用于测量传感器中仪器中的流体压力的容器，以及与压力传感器和泵信号通信的处理器，用于控制泵和流体流动 在仪器中至少部分地基于在传感器处测量的压力。
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4.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 有权用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US06989519B2
公开(公告)日：2006-01-24
申请号：US10605021
申请日：2003-09-02
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis using heterogeneous or highly viscous starting materials includes a microwave source for generating electromagnetic radiation in the microwave frequencies, a microwave cavity in wave communication with the source for exposing compositions placed therein to microwave radiation, a microwave-transparent pressure resistant reaction vessel in the cavity, a source reservoir for starting materials and related compositions, a pump in communication with the source reservoir for pumping heterogeneous or highly viscous materials from the source reservoir to the reaction vessel, and a pressure-resistant valve between the pump and the reaction vessel for isolating the reaction vessel from the pump and the source reservoir during application of microwave energy to compositions in the vessel and from any resulting high pressures generated therein.
摘要翻译： 用于使用异质或高粘度起始材料的化学合成的受控流微波仪器包括用于产生微波频率的电磁辐射的微波源，与所述源波浪连通的微波腔，用于将放置在其中的组合物暴露于微波辐射中; 在空腔中的透明耐压反应容器，用于起始材料和相关组合物的源储存器，与源储存器连通的泵，用于将来自源储器的非均质或高粘度物质泵送到反应容器，以及在源储存器之间的耐压阀， 泵和反应容器，用于在将微波能量应用于容器中的组合物和从其中产生的任何所得到的高压时将反应容器与泵和源储存器隔离。
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公开(公告)号：US06246038B1
公开(公告)日：2001-06-12
申请号：US09516329
申请日：2000-03-01
IPC分类号： H05B650
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , G01L9/0051 , G01N1/44
摘要： A microwave vessel system for external and noninvasive pressure monitoring and control is disclosed. The system comprises a reaction vessel formed of a material that is transparent to microwave radiation, with the reaction vessel including a portion that is movable under pressure generated by a chemical reaction inside the vessel while maintaining the reaction sealed inside the vessel. A sensor is adjacent to the movable portion of the vessel for detecting the motion of the movable portion as the portion responds to pressure generated inside the vessel. The system includes means for maintaining the sensor against the movable portion while microwaves are applied to the vessel so that the movement of the movable portion under pressure is detected by the sensor.
摘要翻译： 公开了一种用于外部和无创压力监测和控制的微波容器系统。 该系统包括由对微波辐射透明的材料形成的反应容器，反应容器包括在容器内部通过化学反应产生的压力下可移动的部分，同时保持反应密封在容器内。 传感器邻近容器的可移动部分，用于检测可动部分的运动，因为该部分响应于容器内产生的压力。 该系统包括用于在将微波施加到容器的同时将传感器保持在可移动部分上的装置，使得在压力下的可移动部分的运动被传感器检测到。
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6.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 有权用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US07214913B2
公开(公告)日：2007-05-08
申请号：US11151500
申请日：2005-06-13
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis using heterogeneous or highly viscous starting materials includes a microwave source for generating electromagnetic radiation in the microwave frequencies, a microwave cavity in wave communication with the source for exposing compositions placed therein to microwave radiation, a microwave-transparent pressure resistant reaction vessel in the cavity, a source reservoir for starting materials and related compositions, a pump in communication with the source reservoir for pumping heterogeneous or highly viscous materials from the source reservoir to the reaction vessel, and a pressure-resistant valve between the pump and the reaction vessel for isolating the reaction vessel from the pump and the source reservoir during application of microwave energy to compositions in the vessel and from any resulting high pressures generated therein.
摘要翻译： 用于使用异质或高粘度起始材料的化学合成的受控流微波仪器包括用于产生微波频率的电磁辐射的微波源，与所述源波浪连通的微波腔，用于将放置在其中的组合物暴露于微波辐射中; 在空腔中的透明耐压反应容器，用于起始材料和相关组合物的源储存器，与源储存器连通的泵，用于将来自源储器的非均质或高粘度物质泵送到反应容器，以及在源储存器之间的耐压阀， 泵和反应容器，用于在将微波能量应用于容器中的组合物和从其中产生的任何所得到的高压时将反应容器与泵和源储存器隔离。
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公开(公告)号：US06926939B2
公开(公告)日：2005-08-09
申请号：US10064718
申请日：2002-08-09
IPC分类号： B01J3/04 , B01J19/02 , B01J19/12 , F16J13/02 , G01N1/44 , G01N35/00 , H05B6/64 , H05B6/80 , B32B1/08 , A61L2/12 , B01L9/00 , B01L11/00
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymericcylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding is selected from the group consisting of filaments and yarns. A supporting frame extends along the cylinder and across the lid and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.
摘要翻译： 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆柱体的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面下边缘，当帽位于聚合圆筒上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个缠绕织物层，其中绕组选自长丝和纱线。 支撑框架沿着圆柱体延伸并且横过盖子并且横过气缸的封闭端延伸，并且当在容器内部产生压力时防止盖子从气缸移位。
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公开(公告)号：US06534140B2
公开(公告)日：2003-03-18
申请号：US09260209
申请日：1999-03-01
IPC分类号： B29D2300
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymeric cylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding is selected from the group consisting of filaments and yarns. A supporting frame extends along the cylinder and across the lid and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.
摘要翻译： 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆筒的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面的下边缘，当帽位于聚合物圆柱体上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个缠绕织物层，其中绕组选自长丝和纱线。 支撑框架沿着圆柱体延伸并且横过盖子并且横过气缸的封闭端延伸，并且当在容器内部产生压力时防止盖子从气缸移位。
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公开(公告)号：US6124582A
公开(公告)日：2000-09-26
申请号：US265917
申请日：1999-03-10
CPC分类号： H05B6/806 , B01J19/126 , G01L9/0051 , G01N1/44 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218
摘要： A microwave vessel system for external and noninvasive pressure monitoring and control is disclosed. The system comprises a reaction vessel formed of a material that is transparent to microwave radiation, with the reaction vessel including a portion that is movable under pressure generated by a chemical reaction inside the vessel while maintaining the reaction sealed inside the vessel. A sensor is adjacent to the movable portion of the vessel for detecting the motion of the movable portion as the portion responds to pressure generated inside the vessel. The system includes means for maintaining the sensor against the movable portion while microwaves are applied to the vessel so that the movement of the movable portion under pressure is detected by the sensor.
摘要翻译： 公开了一种用于外部和无创压力监测和控制的微波容器系统。 该系统包括由对微波辐射透明的材料形成的反应容器，反应容器包括在容器内部通过化学反应产生的压力下可移动的部分，同时保持反应密封在容器内。 传感器邻近容器的可移动部分，用于检测可动部分的运动，因为该部分响应于容器内产生的压力。 该系统包括用于在将微波施加到容器的同时将传感器保持在可移动部分上的装置，使得在压力下的可移动部分的运动被传感器检测到。
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公开(公告)号：US6086826A
公开(公告)日：2000-07-11
申请号：US929589
申请日：1997-09-15
CPC分类号： H05B6/806 , B01J19/126 , G01L9/0051 , G01N1/44 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218
摘要： A microwave vessel system for external and noninvasive pressure monitoring and control is disclosed. The system comprises a reaction vessel formed of a material that is transparent to microwave radiation, with the reaction vessel including a portion that is movable under pressure generated by a chemical reaction inside the vessel while maintaining the reaction sealed inside the vessel. A sensor is adjacent to the movable portion of the vessel for detecting the motion of the movable portion as the portion responds to pressure generated inside the vessel. The system includes a structure for maintaining the sensor against the movable portion while microwaves are applied to the vessel so that the movement of the movable portion under pressure is detected by the sensor.
摘要翻译： 公开了一种用于外部和无创压力监测和控制的微波容器系统。 该系统包括由对微波辐射透明的材料形成的反应容器，反应容器包括在容器内部通过化学反应产生的压力下可移动的部分，同时保持反应密封在容器内。 传感器邻近容器的可移动部分，用于检测可动部分的运动，因为该部分响应于容器内产生的压力。 该系统包括用于在将微波施加到容器上的情况下将传感器保持在可移动部分上的结构，从而可以通过传感器检测压力下的可移动部分的移动。
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