公开(公告)号：US20230174446A1

公开(公告)日：2023-06-08

申请号：US18102141

申请日：2023-01-27

Applicant: AGC INC.

Inventor： Takuya IWASE ,  Motoshi AOYAMA

IPC: C07C43/12 ,  C07C309/80 ,  C07C41/34 ,  C07C303/44

CPC classification number: C07C43/126 ,  C07C309/80 ,  C07C41/34 ,  C07C303/44

Abstract: To provide a method for producing a fluorinated ether compound having a poly(oxyfluoroalkylene) chain and a sulfonate group with low impurity content and in high yield.
A method for producing a fluorinated ether compound, comprising



step 1 of sulfonylating a fluorinated ether compound having a poly(oxyfluoroalkylene) chain and a hydroxy group in the presence of a fluorinated solvent, a base and a sulfonylating agent to obtain a product containing a fluorinated ether compound having a poly(oxyfluoroalkylene) chain and a sulfonate group, and
step 2 of contacting the product obtained in step 1 with an adsorbent having a pH of at most 8.0.

公开(公告)号：US20250026959A1

公开(公告)日：2025-01-23

申请号：US18894110

申请日：2024-09-24

Applicant: AGC Inc.

Inventor： Motoshi AOYAMA ,  Koki WATANABE ,  Yasuhiro HIRATA ,  Hironobu SAKAGUCHI ,  Eiichiro ANRAKU ,  Shiori KAWAKAMI

IPC: C09D183/14 ,  C08G77/50 ,  C09D5/16 ,  G02B1/04

Abstract: A compound including an alkyl group having two or more carbon atoms, an organopolysiloxane residue, and a reactive silyl group, and an application thereof.

公开(公告)号：US20250026936A1

公开(公告)日：2025-01-23

申请号：US18894080

申请日：2024-09-24

Applicant: AGC Inc.

Inventor： Koki WATANABE ,  Motoshi AOYAMA

IPC: C09D5/16 ,  C07F7/21 ,  C08G77/18 ,  C09D183/08 ,  G02B1/04

Abstract: A compound including the following Group 1, a partial structure that is an alkylene chain, a polyalkylene oxide chain, a divalent organopolysiloxane residue, or a combination thereof, and the following Group 2. Group 1: monovalent cyclic polysiloxane residue or monovalent cage-like polysiloxane residue Group 2: —Si(R2)nL3-n R2 is a monovalent hydrocarbon group, each of pieces of L is independently a hydrolyzable group or a hydroxyl group, and n is an integer from 0 to 2.

公开(公告)号：US20240368494A1

公开(公告)日：2024-11-07

申请号：US18758567

申请日：2024-06-28

Applicant: AGC Inc.

Inventor： Motoshi AOYAMA

IPC: C10M155/02 ,  C10M125/18 ,  C10M139/00 ,  C10N50/02

Abstract: A surface treatment agent from which a surface layer having an excellent friction resistance can be formed, an article including such a surface layer, and a method for manufacturing such an article are provided. A surface treatment agent according to the present invention contains a fluorine-containing ether compound including a fluoro-polyether chain and a reactive silyl group; a first metallic compound containing a first metallic element; and a second metallic compound containing a second metallic element different from the first metallic element.

公开(公告)号：US20230416560A1

公开(公告)日：2023-12-28

申请号：US18367663

申请日：2023-09-13

Applicant: AGC Inc.

Inventor： Motoshi AOYAMA ,  Masayuki Haraguchi

IPC: C09D171/08 ,  C09D161/18

CPC classification number: C09D171/08 ,  C09D161/18

Abstract: A surface treatment agent includes: a fluorine-containing compound (A) having a reactive silyl group; and at least one compound (B) selected from the group consisting of a fluorine-containing ketone compound (B1): R1COR2, a fluorine-containing cyclic ketone compound (the following B2), and a fluorine-containing polyether compound (B3): R4—[OR5]q—R6. In Formula (B1), R1 and R2 represent a fluorine-containing alkyl group having from 1 to 5 carbon atoms. In Formula (B2), R3 represents a residue that forms a 3- to 5-membered ring structure with a carbon atom of a carbonyl group and that has a fluorine atom. In Formula (B3), R4 and R6 represent a fluorine-containing alkyl group having from 1 to 3 carbon atoms, q represents an integer of 1 or more, R5 represents a perfluoroalkylene group having from 1 to 6 carbon atoms, and in a case in which q is an integer of 2 or more, plural R5s may be the same or different.

公开(公告)号：US20240392159A1

公开(公告)日：2024-11-28

申请号：US18792622

申请日：2024-08-02

Applicant: AGC Inc.

Inventor： Hikaru ONO ,  Motoshi AOYAMA ,  Takuya IWASE

IPC: C09D171/08 ,  C09D7/20

Abstract: Provided are a surface treating agent which is capable of forming a surface layer excellent in acid resistance and has excellent long-term storage stability, an article having the surface layer, and a method for producing the article. The surface treating agent of the present invention is a surface treating agent containing a fluorine-containing ether compound having a fluoropolyether chain and a reactive silyl group, and one or more ions selected from the group consisting of an iodide ion and a bromide ion, in which the content of the ions is 0.05 to 2.00 ppm by mass with respect to the total mass of the surface treating agent.

公开(公告)号：US20240392069A1

公开(公告)日：2024-11-28

申请号：US18793221

申请日：2024-08-02

Applicant: AGC Inc.

Inventor： Hikaru ONO ,  Motoshi AOYAMA ,  Takuya IWASE

IPC: C08G65/336 ,  C08G65/22 ,  C09D7/20 ,  C09D171/02

Abstract: Provided are a surface treating agent which is capable of forming a surface layer excellent in light resistance and has excellent long-term storage stability, an article having the surface layer, and a method for producing the article. The surface treating agent of the present invention is a surface treating agent containing a fluorine-containing ether compound having a fluoropolyether chain and a reactive silyl group, and a fluoride ion, in which the content of the fluoride ion is 0.1 to 3.0 ppm by mass with respect to the total mass of the surface treating agent.

公开(公告)号：US20240317936A1

公开(公告)日：2024-09-26

申请号：US18672363

申请日：2024-05-23

Applicant: AGC Inc.

Inventor： Takuya IWASE ,  Motoshi AOYAMA

IPC: C08G65/336 ,  C09D7/65

CPC classification number: C08G65/336 ,  C09D7/65 ,  C08G2150/00

Abstract: A fluorine-containing ether compound represented by formula (1) or (2):


A1-(ORf1)y1—R1-Q1-R2-L1-(R3-T1)x1  Formula (1)



(T3-R9)x3-L3-R8-Q3-R7—Rf—(ORf2)y2—R4-Q2-R5-L2-(R6-T2)x2   Formula (2)

where each symbol in the formula is as described in the description.

公开(公告)号：US20230407003A1

公开(公告)日：2023-12-21

申请号：US18456804

申请日：2023-08-28

Applicant: AGC Inc.

Inventor： Motoshi AOYAMA ,  Makoto UNO

IPC: C08G65/00 ,  C08G65/336 ,  C09D171/00

CPC classification number: C08G65/007 ,  C08G65/336 ,  C09D171/00 ,  C08G2650/04

Abstract: There is provided a fluorine-containing ether compound excellent in light fastness, a surface treatment agent, a fluorine-containing ether composition, a coating liquid, an article having a surface layer excellent in light fastness, a method for producing the same, and a compound useful as a raw material of the fluorine-containing ether compound excellent in light fastness.
A fluorine-containing ether compound represented by the following general formula (A).


(R1R2C═CR3-L1-)n1Q1-Rf-Q2(-T)n2  Formula (A)



where, each reference sign in the formula (A) is as described in the specification.

公开(公告)号：US20210348024A1

公开(公告)日：2021-11-11

申请号：US17443038

申请日：2021-07-20

Applicant: AGC Inc.

Inventor： Keigo MATSUURA ,  Taiki HOSHINO ,  Kiyotaka TAKAO ,  Makoto UNO ,  Eiichiro ANRAKU ,  Motoshi AOYAMA ,  Naoki KATSUKI ,  Yusuke TOMIYORI ,  Toyokazu ENTA ,  Hiromasa YAMAMOTO

IPC: C09D183/10 ,  C09D5/00 ,  C09D7/20

Abstract: To provide a composition with which a surface layer excellent in abrasion resistance and sliding resistance can be formed, and an article.
The composition of the present invention comprises a compound represented by the formula (1) and a compound represented by the formula (2), wherein the ratio of the number of moles of the group represented by —CF3 in Rf1 in the formula (1) to the total of the number of moles of the group represented by —CF2— closest to Y1 in Rf2 in the formula (1), the number of moles of the group represented by —CF2— closest to Y2 in Rf3 in the formula (2) and the number of moles of the group represented by —CF2— closest to Y3 in Rf3 in the formula (2), is from 0.001 to 0.1: Rf1—(OX1)m1—O—Rf2—Y1—[Si(R1)n1L13-n1]g1  (1) [L23-n2(R2)n2Si]g2—Y2—Rf3—(OX2)m2—O—Rf4—Y3—[Si(R3)n3L33-n3]g3  (2)