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公开(公告)号：US20180065910A1
公开(公告)日：2018-03-08
申请号：US15790235
申请日：2017-10-23
发明人： Alan B. Levy , Scott R. Keenan , Robert Raja , Arran M. Gill , Matthew E. Potter , Sivan A. Van Aswegen
IPC分类号： C07C45/39 , B01J37/08 , B01J37/04 , B01J27/13 , B01J27/185 , C07C49/403
CPC分类号： C07C45/39 , B01J23/42 , B01J23/44 , B01J23/52 , B01J23/8926 , B01J27/13 , B01J27/1856 , B01J35/0013 , B01J35/002 , B01J37/04 , B01J37/08 , B01J37/088 , B01J37/18 , B01J37/343 , C07C2601/14 , C07C49/403
摘要： Methods for converting an alcohol, such as cyclohexanol to a ketone, such as cyclohexanone, include reacting the alcohol in the presence of a catalyst and oxygen to produce the ketone. In one exemplary embodiment, the catalyst comprises a microporous copper chloropyrophosphate framework including a plurality of noble metal nanoparticles. In one exemplary embodiment, the noble metal nanoparticles include at least one metal selected from the group consisting of platinum, palladium, and gold.
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公开(公告)号：US09662643B2
公开(公告)日：2017-05-30
申请号：US14263156
申请日：2014-04-28
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： C01B39/54 , B01J29/85 , C07D201/04 , B01J35/00 , C07D223/10 , C07D225/02 , C01B37/08
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
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公开(公告)号：US09822052B2
公开(公告)日：2017-11-21
申请号：US15279837
申请日：2016-09-29
发明人： Alan B. Levy , Scott R. Keenan , Robert Raja , Arran M. Gill , Matthew E. Potter , Sivan A. Van Aswegen
IPC分类号： C07C45/35 , B01J27/00 , B01J37/00 , C07C45/39 , B01J27/13 , B01J27/185 , B01J37/04 , B01J37/08
CPC分类号： C07C45/39 , B01J23/42 , B01J23/44 , B01J23/52 , B01J23/8926 , B01J27/13 , B01J27/1856 , B01J35/0013 , B01J35/002 , B01J37/04 , B01J37/08 , B01J37/088 , B01J37/18 , B01J37/343 , C07C2601/14 , C07C49/403
摘要： Methods for converting an alcohol, such as cyclohexanol to a ketone, such as cyclohexanone, include reacting the alcohol in the presence of a catalyst and oxygen to produce the ketone. In one exemplary embodiment, the catalyst comprises a microporous copper chloropyrophosphate framework including a plurality of noble metal nanoparticles. In one exemplary embodiment, the noble metal nanoparticles include at least one metal selected from the group consisting of platinum, palladium, and gold.
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4.发明授权Gas and liquid phase catalytic beckmann rearrangement of oximes to produce lactams 有权气相和液相催化贝克曼重排肟产生内酰胺公开(公告)号：US09221762B2
公开(公告)日：2015-12-29
申请号：US14273688
申请日：2014-05-09
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： C07D201/04 , C07D223/10 , B01J29/85 , B01J35/00 , C07D225/02
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
摘要翻译： 提供了通过使用硅铝磷酸盐催化剂进行贝克曼重排来从肟产生内酰胺的方法。 这些催化剂可用于气相或液相反应以将肟转化成内酰胺。 使用所公开的方法制备肟的高转化率和高选择性，包括由环己酮肟产生的ε-己内酰胺的高转化率和选择性，以及由环十二酮肟产生的ω-月桂内酰胺的高转化率和选择性。
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5.发明授权Gas and liquid phase catalytic Beckmann rearrangement of oximes to produce lactams 有权气相和液相催化贝克曼重排肟产生内酰胺公开(公告)号：US08772476B2
公开(公告)日：2014-07-08
申请号：US13658495
申请日：2012-10-23
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： C07D201/04 , C07D223/10
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
摘要翻译： 提供了通过使用硅铝磷酸盐催化剂进行贝克曼重排来从肟产生内酰胺的方法。 这些催化剂可用于气相或液相反应以将肟转化成内酰胺。 使用所公开的方法制备肟的高转化率和高选择性，包括由环己酮肟产生的ε-己内酰胺的高转化率和选择性，以及由环十二酮肟产生的ω-月桂内酰胺的高转化率和选择性。
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6.发明申请GAS AND LIQUID PHASE CATALYTIC BECKMANN REARRANGEMENT OF OXIMES TO PRODUCE LACTAMS 有权气体和液相催化剂BECKMANN对生产LACTAMS的氧化物排放公开(公告)号：US20160279622A9
公开(公告)日：2016-09-29
申请号：US14263156
申请日：2014-04-28
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： B01J29/85
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
摘要翻译： 提供了通过使用硅铝磷酸盐催化剂进行贝克曼重排来从肟产生内酰胺的方法。 这些催化剂可用于气相或液相反应以将肟转化成内酰胺。 使用所公开的方法制备肟的高转化率和对选择性内酰胺的高选择性，包括由环己酮肟产生的ε-己内酰胺的高转化率和选择性以及由环十二酮肟产生的ω-月桂内酰胺的高转化率和选择性。
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7.发明申请GAS AND LIQUID PHASE CATALYTIC BECKMANN REARRANGEMENT OF OXIMES TO PRODUCE LACTAMS 有权气体和液相催化剂BECKMANN对生产LACTAMS的氧化物排放公开(公告)号：US20150306586A1
公开(公告)日：2015-10-29
申请号：US14263156
申请日：2014-04-28
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： B01J29/85
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
摘要翻译： 提供了通过使用硅铝磷酸盐催化剂进行贝克曼重排来从肟产生内酰胺的方法。 这些催化剂可用于气相或液相反应以将肟转化成内酰胺。 使用所公开的方法制备肟的高转化率和高选择性，包括由环己酮肟产生的ε-己内酰胺的高转化率和选择性，以及由环十二酮肟产生的ω-月桂内酰胺的高转化率和选择性。
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公开(公告)号：US20150126732A1
公开(公告)日：2015-05-07
申请号：US14273688
申请日：2014-05-09
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： C07D223/10 , C07D225/02
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
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9.发明申请GAS AND LIQUID PHASE CATALYTIC BECKMANN REARRANGEMENT OF OXIMES TO PRODUCE LACTAMS 有权气体和液相催化剂BECKMANN对生产LACTAMS的氧化物排放公开(公告)号：US20130109851A1
公开(公告)日：2013-05-02
申请号：US13658495
申请日：2012-10-23
发明人： Alan B. Levy , Robert Raja , Matthew E. Potter
IPC分类号： C07D201/04 , C01B39/54
CPC分类号： B01J29/85 , B01J35/002 , C01B37/08 , C01B39/54 , C07D201/04 , C07D223/10 , C07D225/02 , Y02P20/52
摘要： Methods for producing lactams from oximes by performing a Beckmann rearrangement using a silicoaluminophosphate catalyst are provided. These catalysts may be used in gas phase or liquid phase reactions to convert oximes into lactams. High conversion of oxime and high selectivity for the desired lactams are produced using the disclosed methods, including high conversion and selectivity for ε-caprolactam produced from cyclohexanone oxime and high conversion and selectivity for ω-laurolactam produced from cyclododecanone oxime.
摘要翻译： 提供了通过使用硅铝磷酸盐催化剂进行贝克曼重排来从肟产生内酰胺的方法。 这些催化剂可用于气相或液相反应以将肟转化成内酰胺。 使用所公开的方法产生肟的高转化率和对所需内酰胺的高选择性，包括由环己酮肟产生的ε-己内酰胺的高转化率和选择性，以及由环十二烷酮肟产生的ω-月桂内酰胺的高转化率和选择性。
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