摘要:
A process for purifying propylene homopolymers or copolymers which comprises:(i) polymerizing or copolymerizing propylene with other unsaturated hydrocarbon monomers in liquid propylene in the presence of a catalyst system consisting essentially of (a) an activated titanium trichloride obtained by reducing titanium tetrachloride with an organo-aluminum compound followed by activation and (b) an organo-aluminum compound;(ii) introducing the resulting polymer slurry into an upper portion of a counter-current washing tower to counter-currently contact the polymer slurry with a C.sub.3 -C.sub.8 alcohol and liquid propylene, whereby said catalyst is deactivated and at the same time the propylene homopolymers or copolymers dissolved in the polymer slurry and the catalyst are removed by washing, wherein said alcohol is used in an amount 0.1 to 50 times by mole based on said organo-aluminum compound (b) and is supplied to the washing tower lower than the point of introduction of said polymer slurry, and said liquid propylene is supplied to a lower portion of the washing tower; and(iii) then after removing volatile monomers by flashing, contacting the powdery propylene homopolymers or copolymers with a gaseous epoxide at a temperature lower than melting point of said polymer or copolymer.
摘要:
In a process for producing a homopolymer or a copolymer of propylene comprising polymerizing propylene or copolymerizing propylene and at least one other unsaturated hydrocarbon monomer in liquid propylene using a catalyst system containing activated titanium trichloride (a) and an organoaluminum compound (b), the activated titanium trichloride (a) being prepared by reducing titanium tetrachloride with an organoaluminum compound followed by activation, to produce a polymer slurry; introducing the polymer slurry produced into the top of a counter-current washing tower; and washing the polymer slurry by counter-currently contacting the polymer slurry with liquid propylene introduced into the bottom of the washing tower, the improvement which comprises purifying the homopolymer or copolymer of propylene by feeding an epoxide in a molar amount of about 1 to about 15 times the molar amount of the total of activated titanium trichloride (a) and organoaluminum compound (b), to a part of said washing tower, thereby deactivating the catalyst and removing the catalyst residue and the homopolymer or copolymer of propylene dissolved in the polymer slurry.
摘要:
In a process for producing a propylene homopolymer or copolymer which comprises polymerizing propylene or copolymerizing propylene and at least one other unsaturated hydrocarbon monomer in liquid propylene using a catalyst comprising activated titanium trichloride and an organo-aluminum compound, the activated titanium trichloride being prepared by reducing titanium tetrachloride with an organo-aluminum compound followed by activation, introducing the polymer slurry produced into the top of a counter-current washing tower, and washing the slurry by bringing the slurry into counter-current contact with liquid propylene which is introduced into the bottom of the washing tower, the improvement which comprises refining the homopolymer or copolymer of propylene by feeding (a) an alcohol having 3 to 8 carbon atoms in a molar amount of about 0.1 to about 10 times the molar amount of the organo-aluminum compound in the slurry, or (b) a mixture of an alcohol having 3 to 8 carbon atoms and an epoxide, the molar amount of the alcohol being about 0.1 to about 10 times the molar amount of the organo-aluminum compound in the slurry and the molar amount of the epoxide compound being about 0.1 to about 3 times the molar amount of the organo-aluminum compound in the slurry, to a part of the washing tower, thereby simultaneously deactivating the catalyst and removing the catalyst and the propylene homopolymer or copolymer dissolved in the polymer slurry.
摘要:
A polymer slurry formed by polymerizing ethylene or propylene optionally with other olefin monomer copolymerizable therewith in a hydrocarbon solvent such as propylene, propane, butane, etc., is continuously or intermittently supplied to a filter having a filtering surface on which a slight quantity of polymer particles are retained. Most of the hydrocarbon solvent is recovered by passing through the filtering surface, and the polymer particles are overflown from the filter to recover as a wet cake. By the use of such a specific filter, the quantity of the solvent to be vaporized can be greatly reduced.
摘要:
Granules containing 60 wt. % or more filler, having such particle size distribution that 90 wt. % or more granular particles have a particle size of (1/3)d.sub.50.sup.b to 3d.sub.50.sup.b (d.sub.50.sup.b : mean particle size of the granules), and being produced by blending (a) 60 to 90 parts by weight of a filler having a mean particle size of 0.05 to 100.mu., (b) 5 to 35 parts by weight of crystalline polyolefin powder having a mean particle size (d.sub.50.sup.a) of 150 to 1,000.mu. and having such particle size distribution that 90 wt. % or more particles thereof have a particle size of (1/2)d.sub.50.sup.a to 2d.sub.50.sup.a, (c) 5 to 35 parts by weight of a binder having a melting point lower than that of said crystalline polyolefin powder by a least 10.degree.C., and optionally, (d) a compounding additive, at a temperature lower than the melting point of the crystalline polyolefin powder and higher than the melting point of the binder, is disclosed.
摘要:
Sealing performance between a sealing member and a reinforcing plate adhered to a wiring unit is prevent from being deteriorated. An FPC 1 is integrated with a sealing member 2, and a cover 3 is attached to a front end portion. On upper and lower surfaces of the FPC 1, reinforcing plates 12 each having a shape of a rectangular flat plate are arranged and adhered in an opposing manner interposing the FPC 1. The sealing member 2 is formed of elastic material such as rubber, and is fixedly attached to the FPC 1 such that the sealing member 2 covers the reinforcing plates 12 adhered to the upper and lower surfaces of the FPC 1 together with the FPC 1 located along front edges and rear edges of the reinforcing plates 12.
摘要:
A multiplier calculates a product S'(x)=S(x).multidot..lambda.(x) mod X.sup.d-1 of a syndrome polynomial S(x) generated by a syndrome generator and an erasure position polynomial .lambda.(x) generated by an erasure position polynomial generator, modulo X.sup.d-1. A constant multiplier sequentially multiplies coefficients of the polynomial S'(x) and the erasure position polynomial .lambda.(x) with a power of a primitive root .alpha. of a code. The power exponents in this multiplication are determined in units of coefficients. Every time this multiplication is executed, an adder sequentially adds predetermined combinations of products. A plurality of arithmetic and logic operations according to the numbers of correctable erasures and errors are sequentially executed using the sums. A divisor and dividend are selected in accordance with the number of erasures included in the code on the basis of the plurality of arithmetic and logic operation results. A division is executed using the selected divisor and dividend. A value at a position, discriminated to be an error position, of the code is corrected based on the division result, thus performing error correction including erasure correction with a simple circuit arrangement.
摘要:
A light beam is applied to an information recording medium to record information. A light amount of the light beam reflected by the recording medium is detected simultaneously with the recording of information. A defect of the recording medium is detected by comparing the detected light amount with a reference value. When a degree of the detected defect exceeds a predetermined level, the information is rerecorded on another portion of the recording medium.
摘要:
An apparatus for discriminating a machining state from a non-machining state in a machine tool wherein a workpiece is machined with a cutting tool or grinder, comprising plural vibration sensors including at least one acoustic-emission sensor, which detect vibrations of different frequency bands, respectively, which are produced during machining of the workpiece by the tool. A discriminating device judges that the workpiece is being machined by the tool when levels of output signals generated from at least two of the vibration sensors are higher than respective predetermined threshold levels, and judges that the workpiece is not being machined by the tool when the level of an output signal generated from less than two of the vibration sensors is higher than a predetermined threshold level. Also disclosed is a method for discrimination between the machining and non-machining states.
摘要:
[Problems] To provide a method of packing fiber for artificial hair, while suppressing generation of folding mark during packaging, transportation and storage and yet preserving preferable processability and hairdressing characteristics.[Means for Solving Problems] There is provided a method of packing fiber for artificial hair, characterized by packing the artificial hair fibers in a packaging container at a filling density of no lesser than 0.1 kg/l and no more than 0.8 kg/l. Further in the packing method, the pressure of the packed artificial hair fibers applied to the top face of the packaging container is adjusted to no lesser than 0.1 kPa and no more than 8.0 kPa.