摘要:
In a process for producing a stabilized oxymethylene copolymer by heat-melting, at a temperature ranging between the melting point of the copolymer and a temperature 100.degree. C. higher than the melting point in a degassing apparatus in the presence of a heat stabilizer, a crude oxymethylene copolymer of trioxane with a cyclic acetal or cyclic ether, to decompose and eliminate the instable portions of the copolymer, the improvement which comprises using as the degassing apparatus in heat stabilizing the crude oxymethylene copolymer a combination of (A) an extruder and (B) a surface renewing-type mixer, and carrying out the operation by first feeding a crude oxymethylene copolymer to said extruder (A) to heat-melt and decompose 30-90% by weight of the instable portions of the crude copolymer, removing the decomposed gas via a vent provided in said extruder, and thereafter introducing the molten resin continuously to said surface renewing-type mixer (B) where substantially all of the remaining instable portions of the oxymethylene copolymer are heat-decomposed until the content of the instable portions falls below about 2 wt. %, thereby heat stabilizing the copolymer; said extruder (A) having a single or a plurality of shafts, said surface renewing-type mixer functioning to mix and knead the resin thereby constantly renewing the surface of the resin to volatize the volatiles contained therein.
摘要:
A process for producing an oxymethylene copolymer by polymerizing trioxan and 1,3-dioxolan in the presence of a cationically active catalyst, wherein (1) 1,3-dioxolan is used in an amount of 0.01 to 2.9 mol % based on trioxan; and (2) the cationically active catalyst is used in an amount of 1×10−7 to 1.2×10−4 mol based on 1 mol of trioxan. The process of the present invention makes it possible to obtain at a high yield an oxymethylene copolymer which has almost as high mechanical strength and stiffness as an oxymethylene homopolymer while retaining the tenacity and heat stability of an oxymethylene copolymer.
摘要:
A polyoxymethylene copolymer which is a polyoxymethylene copolymer obtained by copolymerizing trioxane and 8 to 20 mol, per 100 mol of the trioxane, of 1,3-dioxolane and which (i) has a crystallization time period of 10 to 2,000 seconds at 143° C., (ii) withstands 30 to 1,000 cycles of a bending durability test and (iii) has residence heat stability for 40 minutes or more, and a molded article formed of the copolymer. According to the present invention, there can be provided a polyoxymethylene copolymer excellent in bending durability and heat stability and excellent in moldability, and a molded article formed thereof.
摘要:
A method for (a) determining the shear force between a wafer head and a polishing pad in a polishing tool using a CMP polishing tool with a plate above the wafer head which hangs or rests on the plate. The plate is connected to the CMP polishing tool by (b) low friction motion means (c). A load cell sensor is fixed to the framework of the polishing tool or another immovable structure. (d) The load cell determines the force from the leading edge of the plate when the wafer head is in contact with the polishing pad. (e) Signals from the load cell sensor reporting the shear force. A CMP polishing tool which includes elements corresponding to each of points (a)-(e) in the above method.
摘要:
Provided is a platform door device which makes it possible to reduce the length of time for a replacement operation when a panel-shaped portion of a door is damaged. The platform door device comprises a door, and a driving mechanism for moving the door forwardly and backwardly to close and open a gate on a platform. The driving mechanism includes a motor, a rotation body adapted to be rotated by the motor, and a driven body adapted to be driven according to the rotation of the rotation body so as to move the door, and the door has a panel-shaped main body, and a base segment detachably joined to the main body and attached to the driven body.
摘要:
An amino acid-N,N-diacetic acid (AADA) or its salt with an equivalent or less of an alkali metal is produced by reducing, through electrodialysis, alkali metal ions from an aqueous solution of the alkali metal salt of an AADA. By this configuration, an AADA salt can be produced in a much higher yield than conventional equivalents without requiring a regeneration operation of a resin as in the use of an ion exchange resin or without requiring crystallization-separation of crystals of the AADA salt as in the addition of an organic solvent. A salt of an amino acid-N,N-diacetic acid is also produced by reacting an AADA with any of metal oxides, metal hydroxides, metal carbonates, metal hydrogencarbonates, ammonium hydroxide, ammonium carbonate, ammonium hydrogencarbonate or organic amine compounds. By this configuration, a metal salt, aromonium salt or organic amine salt of an AADA can be produced with efficiency without the formation of by-products.
摘要:
A process for forming a thin metal oxide film is disclosed that comprises molding an amorphous powder of organic metal chelate complexes to obtain a target. The process also includes subjecting the target to a PVD process that forms the thin metal oxide.
摘要:
A process for preparing a target for use in production of a thin metal oxide film that comprises molding an amorphous powder of organic metal chelate complexes to obtain the target. The process also includes mixing metallic materials with an organic chelating agent so as to give a predetermined metal composition to prepare a transparent aqueous solution of organic metal chelate complexes. The process also includes spray-drying the aqueous solution to obtain an amorphous powder of the organic metal chelate complexes.
摘要:
The abrasive machine is capable of preventing deformation and bad abrasion of an abrasive cloth, maintaining flatness of an abrasive face of an abrasive plate and improving abrading accuracy. The abrasive machine comprises the abrasive plate and a holding unit for holding a work piece. In the holding unit, an inner head has a first concave section. An outer head has a second concave section. A holding plate is provided in the first concave section. An elastic holding member forms a first chamber. An outer enclosing member is provided to the outer head. An inner enclosing member is provided between the outer enclosing member and the inner head. A pressing member presses the abrasive face of the abrasive plate and encloses the holding plate. An elastic ring member a second chamber. A pressurizing unit pressurizes the chambers so as to press the work piece and the pressing member onto the abrasive face.
摘要:
Provided is a platform door device which makes it possible to reduce the length of time for a replacement operation when a panel-shaped portion of a door is damaged. The platform door device comprises a door, and a driving mechanism for moving the door forwardly and backwardly to close and open a gate on a platform. The driving mechanism includes a motor, a rotation body adapted to be rotated by the motor, and a driven body adapted to be driven according to the rotation of the rotation body so as to move the door, and the door has a panel-shaped main body, and a base segment detachably joined to the main body and attached to the driven body.