摘要:
In a process for producing an anthraquinone dye intermediate, 1,4-diamino-2,3-dicyanoanthraquinone, by reacting 1,4-diaminoanthraquinone-2-sulfonic acid, a salt thereof, 1,4-diaminoanthraquinone-2-cyanoanthraquinone, 1,4-diamino-2,3-disulfonic acid, or a salt thereof with a cyanogenating agent in an aqueous medium, the yield and quality of the product can be improved markedly by carrying out the reaction in the presence of a quaternary ammonium compound, and further, depending upon the starting material used, in the presence or absence of a dehydrogenating agent.
摘要:
A process for producing 1,4-diaminoanthraquinone-2,3-disulfonic acid or a salt thereof which comprises reacting a 1,4-diamino-2,3-dihalogenoanthraquinone with a sulfonating agent in an aqueous medium in the presence of at least one of a quaternary ammonium compound and a quaternary phosphonium compound and optionally, in the presence of an inert organic solvent is disclosed. A process for producing 1,4-diamino-2,3-dicyanoanthraquinone which comprises further reacting the thus obtained 1,4-diaminoanthraquinone-2,3-disulfonic acid or salt thereof with a cyanogenation agent is also disclosed.
摘要:
A process for the production of 1,4-diaminoanthraquinone-2-sulfonic acid or a salt thereof is disclosed, comprising reacting 1-amino-4-bromoanthraquinone-2-sulfonic acid or its salt with liquid ammonia in the presence of a copper catalyst wherein the reaction is carried out in the presence of an inert organic solvent, e.g., n-heptane and cyclohexane. In this process, crystals of the desired product do not substantially deposit on reactor walls, and distillation recovery of ammonia can be performed easily without causing deterioration of the desired product. 1,4-Diaminoanthraquinone-2-sulfonic acid or salt thereof is a useful intermediate for the preparation of, e.g., anthraquinone dyes.
摘要:
A virtual computer system executes a virtual computer control program on a physical computer and thereby causes guest programs on the logical partitions, respectively. The virtual computer control program includes an error recovery module to periodically recover from an error in a cache memory, an error interruption handler module responsive to an interruption notice caused by an error which has occurred in the cache memory, to recover from an error in the cache memory, and an error data initialization module to recover from an error in the cache memory with shutdown or restart of one of the logical partitions as a momentum. And the virtual computer control program conducts recovery processing from an error in the cache memory.
摘要:
Process for producing hydroxy-containing alkylated aromatic compounds by the liquid phase reaction of an aromatic compound having at least one hydroxyl group with an alkylating agent in the presence of a heteropoly acid and water.
摘要:
A power transmission device for a vehicle includes a casing mounted on a vehicle, a rotational shaft supported in the casing and rotated by an engine, first and second speed changing shafts, supported in the casing and changing a speed of rotation of the rotational shaft, a first speed clutch mechanism and a second speed clutch mechanism provided between the rotational shaft and the first and second speed changing shafts, respectively, and an output shaft outputting rotation of one speed changing shaft selected by each of the clutch mechanisms. A first brake device applying a braking force to the first speed changing shaft and a second brake device applying the braking force to the second speed changing shaft are provided in the casing.
摘要:
A redundant disk storage system having data stored on one disk and identical data on second disk, wherein the data stored on the second disk is in a different radial location determined by an offset. The offset could be such that the data on the first disk is stored near the inner circumference and the identical data is stored on the second disk near the outer circumference. Moreover, a RAM associated with each disk drive which stores the address and offset eliminates a RAM in the main disk controller.
摘要:
A phthalocyanine compound represented by the following formula, ##STR1## wherein Pc is a metal-containing or metal-free phthalocyanine residue, R.sup.1 is a hydrogen atom or substituted or unsubstituted lower alkyl group, A is a substituted or unsubstituted phenylene or naphthylene group, Y is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z, in which Z is a splittable group by the action of an alkali, W is a bridging group of the following formula, ##STR2## in which R.sup.2 and R.sup.3 are independently a hydrogen atom or a methyl or ethyl group, and n is an integer of from 2 through 6, X is a halogen atom, a is 0 or a number of not more than 2 (0.ltoreq.a.ltoreq.2), and b and c are independently a number of 1 through 3 (1.ltoreq.b.ltoreq.3, 1.ltoreq.c.ltoreq.3), provided that the total of a, b and c is not more than 4 (a+b+c.ltoreq.4), which is useful for dyeing or printing materials, particularly cellulose fiber materials, in a brilliant turquoise blue color excellent in various fastness properties.
摘要:
A hydraulic power transmission device in a work vehicle transmits motive power from two hydraulic motors disposed in parallel to each other. The hydraulic power transmission device includes: a case; a first motor shaft and a second motor shaft respectively disposed in a right-side area and in a left-side area inside the case, each linked to one of the two hydraulic motors; a counter shaft disposed in an area ranging between the first motor shaft and the second motor shaft in the case; an output shaft; a first transmission mechanism that transmits motive power from the first motor shaft to the output shaft via the counter shaft; a second transmission mechanism that transmits motive power from the second motor shaft to the output shaft; and a hydraulic clutch device disposed at the counter shaft, that transmits the motive power from the first motor shaft to the output shaft or cuts off transmission of the motive power.
摘要:
Preventives and/or remedies for liver diseases, which comprise monocyte chemoattractant protein-I (MCP-I) function inhibitors as active ingredients, respectively. Administration of the MCP-I function inhibitors brings about effects in preventing and/or remedying liver diseases.