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公开(公告)号：US08053480B2
公开(公告)日：2011-11-08
申请号：US12302507
申请日：2007-05-17
申请人： Alain Hilberer , Emilie Navet , Laurent Vermeire
发明人： Alain Hilberer , Emilie Navet , Laurent Vermeire
IPC分类号： B01D19/04
CPC分类号： D21C11/00 , B01D19/04 , D21H21/12 , B01D19/0409
摘要： A process for making a foam control composition comprising a cross-linked polyorganosiloxane in which is dispersed a filler, with hydrophobic surface, comprising step (A) mixing (i) a finely divided filler, (ii) a polyorganosiloxane having on at least two reactive substituents, for example on average two reactive substituents, and (iii) a polyorganosiloxane having at least three reactive substituents, capable of addition reaction via hydrosilylation; (B) hydrosilylation reaction of components (ii) and (iii) until the mixture at least partially gels, followed by applying shearing forces to this at least partially gelled mixture. Optionally step (A) comprises a diluent or solvent and after step (B) an emulsification step is carried out to make the foam control composition into an O/W emulsion. Also a process for controlling foam in an aqueous environment by using a foam control composition according to the invention, selected from inks, coatings, paints, detergents, black liquor of from those encountered during pulp and paper manufacture, waste water treatment, textile dyeing processes or the scrubbing of natural gas.
摘要翻译： 一种制备泡沫控制组合物的方法，其包含交联的聚有机硅氧烷，其中分散有疏水表面的填料，所述方法包括步骤（A）将（i）细碎填料，（ii）至少两个反应性的聚有机硅氧烷 取代基，例如平均两个反应性取代基，和（iii）具有至少三个反应性取代基的聚有机硅氧烷，能够通过氢化硅烷化进行加成反应; （B）组分（ii）和（iii）的氢化硅烷化反应，直到混合物至少部分凝胶化，然后对该至少部分胶凝的混合物施加剪切力。 任选地，步骤（A）包括稀释剂或溶剂，并且在步骤（B）之后，进行乳化步骤以使泡沫控制组合物成为O / W乳液。 还有一种通过使用根据本发明的泡沫控制组合物来控制泡沫的方法，所述组合物选自油墨，涂料，油漆，洗涤剂，在纸浆和造纸过程中遇到的黑液，废水处理，纺织品染色方法 或擦洗天然气。
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公开(公告)号：US20090306282A1
公开(公告)日：2009-12-10
申请号：US12302507
申请日：2007-05-17
申请人： Alain Hilberer , Emilie Navet , Laurent Vermeire
发明人： Alain Hilberer , Emilie Navet , Laurent Vermeire
IPC分类号： C08L83/04
CPC分类号： D21C11/00 , B01D19/04 , D21H21/12 , B01D19/0409
摘要： A process for making a foam control composition comprising a cross-linked polyorganosiloxane in which is dispersed a filler, with hydrophobic surface, comprising step (A) mixing (i) a finely divided filler, (ii) a polyorganosiloxane having on at least two reactive substituents, for example on average two reactive substituents, and (iii) a polyorganosiloxane having at least three reactive substituents, capable of addition reaction via hydrosilylation; (B) hydrosilylation reaction of components (ii) and (iii) until the mixture at least partially gels, followed by applying shearing forces to this at least partially gelled mixture. Optionally step (A) comprises a diluent or solvent and after step (B) an emulsification step is carried out to make the foam control composition into an O/W emulsion. Also a process for controlling foam in an aqueous environment by using a foam control composition according to the invention, selected from inks, coatings, paints, detergents, black liquor of from those encountered during pulp and paper manufacture, waste water treatment, textile dyeing processes or the scrubbing of natural gas.
摘要翻译： 一种制备泡沫控制组合物的方法，其包含交联的聚有机硅氧烷，其中分散有疏水表面的填料，所述方法包括步骤（A）将（i）细碎填料，（ii）至少两个反应性的聚有机硅氧烷 取代基，例如平均两个反应性取代基，和（iii）具有至少三个反应性取代基的聚有机硅氧烷，能够通过氢化硅烷化进行加成反应; （B）组分（ii）和（iii）的氢化硅烷化反应，直到混合物至少部分凝胶化，然后对该至少部分胶凝的混合物施加剪切力。 任选地，步骤（A）包括稀释剂或溶剂，并且在步骤（B）之后，进行乳化步骤以使泡沫控制组合物成为O / W乳液。 还有一种通过使用根据本发明的泡沫控制组合物来控制泡沫的方法，该组合物选自油墨，涂料，油漆，洗涤剂，在纸浆和造纸过程中遇到的黑液，废水处理，纺织染色方法 或擦洗天然气。
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公开(公告)号：US20100093598A1
公开(公告)日：2010-04-15
申请号：US12445108
申请日：2007-10-09
申请人： Delphine Davio , Alain Hilberer , Jacqueline L'Hostis , Jean-Paul H. Lecomte , Andreas Stammer , Nicolas Ziolkowski
发明人： Delphine Davio , Alain Hilberer , Jacqueline L'Hostis , Jean-Paul H. Lecomte , Andreas Stammer , Nicolas Ziolkowski
IPC分类号： C11D3/37 , C08G18/42 , C08K5/54 , C08K3/22 , C08K3/34 , C08K5/09 , C08K5/17 , C08K3/32 , C08K3/30 , C08K3/38 , C08K3/26
CPC分类号： C10M155/02 , A61K8/062 , A61K8/068 , A61K8/891 , A61Q1/10 , A61Q5/02 , A61Q5/12 , A61Q19/00 , A61Q19/10 , C08J3/03 , C08J2383/04 , C10M107/50 , C10M173/02 , C10M2229/04 , C10M2229/0405 , C10M2229/041 , C10M2229/0415 , C10M2229/043 , C10M2229/0435 , C10M2229/045 , C10M2229/0455 , C11D3/373 , D06M15/643
摘要： A method of making silicone-based foam control agents comprising: i) preparing a polysiloxane containing polymer by the polymerisation of siloxane containing monomers and/or oligomers in the presence of an inert organopolysiloxane and/or an organic fluid, a suitable catalyst and optionally an end-blocking agent; ii) where required quenching the polymerisation process; wherein the inert organopolysiloxane and/or organic fluid is substantially retained within the resulting diluted polysiloxane containing polymer; iii) introducing from 0.1 to 10% by weight of a suitable filler prior to during or subsequent to step (i); iv) optionally introducing up to 5% by weight of a suitable silicone resin during or subsequent to step (i) and v) where required, adapting the foam control agent produced in steps (i) to (iv) into a suitable form of delivery therefor.
摘要翻译： 一种制备基于硅氧烷的泡沫控制剂的方法，其包括：i）通过在惰性有机聚硅氧烷和/或有机流体，合适的催化剂和任选的一种催化剂存在下聚合含硅氧烷的单体和/或低聚物来制备含聚硅氧烷的聚合物 封端剂; ii）在需要时淬灭聚合过程; 其中所述惰性有机聚硅氧烷和/或有机流体基本上保留在所得稀释的含聚硅氧烷聚合物中; iii）在步骤（i）之前或之后，将0.1至10重量％的合适填料引入; iv）任选地在步骤（i）和（iv）期间或之后引入高达5重量％的合适的有机硅树脂，以及v）如果需要，将步骤（i）至（iv）中制备的泡沫控制剂适应成合适的递送形式 因此。
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公开(公告)号：US20130309498A1
公开(公告)日：2013-11-21
申请号：US13991670
申请日：2011-12-09
IPC分类号： C11D17/06
CPC分类号： C11D17/06 , B01D19/0404 , B01D19/0409 , B01D19/0422 , C11D3/046 , C11D3/373 , C11D7/10 , C11D17/0034 , Y10T428/2982
摘要： A granulated product comprises a liquid organosilicon compound supported on a particulate carrier which is agglomerated into granules by a binder. A process for the production of a granulated product comprises depositing an organosilicon compound and a binder in a liquid state on a particulate carrier and subjecting the carrier thus treated to conditions in which the binder is solidified, thereby agglomerating carrier particles into granules. The particulate carrier is anhydrous sodium sulfate of mean particle size 1 to 40 μm.
摘要翻译： 颗粒状产品包括负载在颗粒载体上的液体有机硅化合物，其通过粘合剂聚结成颗粒。 制备造粒产物的方法包括将有机硅化合物和液态粘合剂沉积在颗粒状载体上，并对经过这样处理的载体进行粘合剂固化的条件，从而将载体颗粒聚结成颗粒。 颗粒状载体为平均粒径1〜40μm的无水硫酸钠。
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公开(公告)号：US09567244B2
公开(公告)日：2017-02-14
申请号：US14342266
申请日：2012-08-23
申请人： Tatsuo Souda , Jianren Zeng , Sung-Hsuen Chao , Serge Creutz , Alain Hilberer , Corina Pagnoni , Fabian Rouffiange , Haruhiko Furukawa
发明人： Tatsuo Souda , Jianren Zeng , Sung-Hsuen Chao , Serge Creutz , Alain Hilberer , Corina Pagnoni , Fabian Rouffiange , Haruhiko Furukawa
IPC分类号： C11D3/12 , C02F1/54 , C02F1/56 , C11D3/37 , C11D11/00 , D21C9/02 , D21C9/08 , D21H17/59 , D21H21/10 , D21C9/18 , C02F11/14 , C02F103/00 , C02F103/28 , C08G77/12 , C08G77/46 , C02F103/10
CPC分类号： C02F1/547 , C02F1/545 , C02F1/56 , C02F11/14 , C02F2103/002 , C02F2103/10 , C02F2103/28 , C02F2305/04 , C02F2307/12 , C08G77/12 , C08G77/46 , C11D3/3738 , C11D11/0017 , D21C9/02 , D21C9/086 , D21C9/18 , D21H17/59 , D21H21/10
摘要： In a process for separating a solid material from a suspension of the solid material in water, an organopolysiloxane polyalkylene oxide copolymer comprising a branched organopolysiloxane structure is added to the suspension of solid material in water and the suspension is drained. The organopolysiloxane polyalkylene oxide copolymer comprising a branched organopolysiloxane structure increases the rate of drainage of the suspension.
摘要翻译： 在从固体材料在水中的悬浮液中分离固体材料的方法中，将包含支链有机聚硅氧烷结构的有机聚硅氧烷聚环氧烷烃共聚物加入固体材料在水中的悬浮液中，并将该悬浮液排出。 包含支链有机聚硅氧烷结构的有机聚硅氧烷聚环氧烷共聚物增加了悬浮液的排出速率。
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公开(公告)号：US20070276056A1
公开(公告)日：2007-11-29
申请号：US10581436
申请日：2004-12-09
CPC分类号： C11D17/0034 , B01D19/0404 , C11D3/0026 , C11D3/2093 , C11D3/373 , B01D19/0409
摘要： Foam control compositions herein can be used in aqueous compositions that are liable to foam. The foam control compositions is added to detergent compositions, particularly detergent powders, to inhibit excessive foaming when the detergent is used in washing. In particular, the foam control composition contains a non-silicon-containing organic liquid, a branched siloxane resin, a particulate filler which is insoluble in the organic liquid, and an additive composition of melting point 35 to 100° C. that is substantially non-polar organic material which is miscible with the organic liquid.
摘要翻译： 本发明的泡沫控制组合物可用于容易发泡的含水组合物中。 将泡沫控制组合物加入到洗涤剂组合物中，特别是洗涤剂粉末中，以在洗涤剂用于洗涤时抑制过量起泡。 特别地，泡沫控制组合物含有不含硅的有机液体，支链硅氧烷树脂，不溶于有机液体的颗粒填料，以及基本上不含有机液体的熔点为35-100℃的添加剂组合物 与有机液体可混溶的极性有机材料。
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公开(公告)号：US07632890B2
公开(公告)日：2009-12-15
申请号：US10521321
申请日：2003-08-01
申请人： Serge Creutz , Alain Hilberer
发明人： Serge Creutz , Alain Hilberer
IPC分类号： C08L83/04
CPC分类号： C11D17/0034 , B01D19/0404 , C11D3/0026 , C11D3/2093 , C11D3/373 , C11D11/0088 , B01D19/0409 , B01D19/0431 , B01D19/0413
摘要： A foam control composition comprises a polydiorganosiloxane fluid comprising units of the formula where each group R, which may be the same or different, is selected from an alkyl group having 1 to 36 carbon atoms or an aryl group or aralkyl group having up to 36 carbon atoms, the mean number of carbon atoms in the groups R being at least 1.3, and an additive composition of melting point 35 to 100° C. comprising a substantially non-polar organic material, preferably a polyol substantially fully esterified by carboxylate groups each having 7 to 36 carbon atoms.
摘要翻译： 泡沫控制组合物包含聚二有机基硅氧烷流体，其包含下式的单元，其中每个基团R可以相同或不同，选自具有1至36个碳原子的烷基或具有至多36个碳原子的芳基或芳烷基 原子，基团R中的平均碳原子数至少为1.3，以及熔点为35-100℃的添加剂组合物，其包含基本上非极性的有机材料，优选通过羧酸酯基团完全酯化的多元醇，各自具有 7至36个碳原子。
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公开(公告)号：US20070167346A1
公开(公告)日：2007-07-19
申请号：US10581435
申请日：2004-12-09
申请人： Serge Creutz , Kenneth Fey , Alain Hilberer , Jean-Paul Lecomte , George Sawicki
发明人： Serge Creutz , Kenneth Fey , Alain Hilberer , Jean-Paul Lecomte , George Sawicki
IPC分类号： C11D3/02
CPC分类号： B01D19/0404 , C11D3/0026 , C11D3/124 , C11D3/373 , C11D3/3749 , B01D19/0409
摘要： A foam control composition contains a liquid polymer of an unsaturated hydrocarbon, a branched siloxane resin, and a particulate filler which is insoluble in the liquid hydrocarbon polymer. The foam control composition can additionally contain a polysiloxane fluid.
摘要翻译： 泡沫控制组合物含有不溶于液态烃聚合物的不饱和烃，支链硅氧烷树脂和颗粒填料的液体聚合物。 泡沫控制组合物可另外含有聚硅氧烷流体。
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公开(公告)号：US20050239908A1
公开(公告)日：2005-10-27
申请号：US10521321
申请日：2003-08-01
申请人： Serge Creutz , Alain Hilberer
发明人： Serge Creutz , Alain Hilberer
CPC分类号： C11D17/0034 , B01D19/0404 , C11D3/0026 , C11D3/2093 , C11D3/373 , C11D11/0088 , B01D19/0409 , B01D19/0431 , B01D19/0413
摘要： A foam control composition comprises a polydiorganosiloxane fluid comprising units of the formula where each group R, which may be the same or different, is selected from an alkyl group having 1 to 36 carbon atoms or an aryl group or aralkyl group having up to 36 carbon atoms, the mean number of carbon atoms in the groups R being at least 1.3, and an additive composition of melting point 35 to 100° C. comprising a substantially non-polar organic material, preferably a polyol substantially fully esterified by carboxylate groups each having 7 to 36 carbon atoms.
摘要翻译： 泡沫控制组合物包含聚二有机基硅氧烷流体，其包含下式的单元，其中每个基团R可以相同或不同，选自具有1至36个碳原子的烷基或具有至多36个碳原子的芳基或芳烷基 原子，基团R中的平均碳原子数至少为1.3，以及熔点为35-100℃的添加剂组合物，其包含基本上非极性的有机材料，优选通过羧酸酯基团完全酯化的多元醇，各自具有 7至36个碳原子。
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