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    Preparation of aqueous concentrates of yellow azo and azoxystilbene dyes utilizing alkanolamine salts
    1.
    发明授权
    Preparation of aqueous concentrates of yellow azo and azoxystilbene dyes utilizing alkanolamine salts 失效
    使用链烷醇胺盐制备黄色偶氮和二烷染料的浓缩水

    公开(公告)号：US5041539A

    公开(公告)日：1991-08-20

    申请号：US370089

    申请日：1989-06-19

    申请人： Athanassios Tzikas ,  Paul Herzig ,  Jurgen Markert

    发明人： Athanassios Tzikas ,  Paul Herzig ,  Jurgen Markert

    IPC分类号： C09B56/04 ,  C09B67/26 ,  C09B69/04

    CPC分类号： C09B69/04 ,  C09B67/0073

    摘要： The invention relates to a process for the preparation of concentrated storage-stable aqueous solutions of yellow azo- and azoxystilbene dyes which are obtained by self-condensation of 4-nitrotoluene-2-sulfonic acid in the presence of an alkali metal hydroxide, by converting the sparingly soluble alkali metal salt of the dye into a water-soluble ammonium salt by double cation exchange via a lipophilic ammonium salt, which process comprises carrying out the double ion exchange in a two-phase system of nitrobenzene/water and using, for the first ion exchange a di- or trialkylamine containing a total of 12 to 40 carbon atoms and, for the second ion exchange, a mono-, di- or trialkanolamine containing 2 to 4 carbon atoms in each alkyl moiety.The concentrated storage-stable dye solutions so obtained are particularly suitable for dyeing paper.

    摘要翻译： 本发明涉及一种通过在碱金属氢氧化物的存在下通过4-硝基甲苯-2-磺酸的自缩合而得到的黄色偶氮 - 和二喔啉染料的浓缩储存稳定水溶液的方法， 通过亲脂性铵盐通过双阳离子交换将染料的微溶性碱金属盐转化为水溶性铵盐，该方法包括在硝基苯/水的两相体系中进行双离子交换，并使用 首先离子交换含有总共12至40个碳原子的二 - 或三烷基胺，并且对于第二离子交换，每个烷基部分含有2至4个碳原子的单 - ，二 - 或三烷醇胺。 如此得到的浓缩储存稳定的染料溶液特别适用于染色纸。

    Process for the dyeing of synthetic textile material
    4.
    发明授权
    Process for the dyeing of synthetic textile material 失效
    合成纺织材料染色工艺

    公开(公告)号：US4015934A

    公开(公告)日：1977-04-05

    申请号：US415282

    申请日：1973-11-12

    申请人： Hans Wilhelm Liechti ,  Jurgen Markert

    发明人： Hans Wilhelm Liechti ,  Jurgen Markert

    IPC分类号： C09B29/42 ,  D06P1/92 ,  D06P1/18

    CPC分类号： C09B29/363 ,  D06P1/924 ,  Y10S8/922 ,  Y10S8/938

    摘要： A process for dyeing synthetic textile material in a halogenated hydrocarbons solvent by the exhaust process, comprising the use, for dyeing, of azopyridone dyestuffs of formula I ##STR1## wherein R.sub.1 and R.sub.2 each independently represent hydrogen, or an optionally substituted lower alkyl, lower alkenyl, cycloalky or aryl radical, orR.sub.1 and R.sub.2 form together with the nitrogen atom binding them, optionally with the inclusion of a further hetero atom, a non-aromatic 5- or 6-membered hetero ring,X represents halogen, the cyano or nitro group,Y represents hydrogen, or a lower alkyl group optionally substituted by the hydroxyl or cyano group, andZ represents --CO-- or --SO.sub.2 --.

    摘要翻译： 一种通过排气方法在卤代烃溶剂中染色合成纺织材料的方法，包括用于染色式I的叠氮吡啶酮染料（I），其中R 1和R 2各自独立地表示氢，或任选取代的低级 烷基，低级烯基，环烷基或芳基，或R 1和R 2与与它们结合的氮原子一起形成，任选地包含另外的杂原子，非芳族5-或6-元杂环，X表示卤素， 氰基或硝基，Y表示氢或任选被羟基或氰基取代的低级烷基，Z表示-CO-或-SO 2 - 。

    Process for the determination of liquid absorption of powdery solids
    5.
    发明授权
    Process for the determination of liquid absorption of powdery solids 失效
    测定粉末状固体液体吸收的方法

    公开(公告)号：US4881402A

    公开(公告)日：1989-11-21

    申请号：US233743

    申请日：1988-08-19

    申请人： Jurgen Markert ,  Klaus-Dieter Schubel ,  Milan Krizek

    发明人： Jurgen Markert ,  Klaus-Dieter Schubel ,  Milan Krizek

    IPC分类号： G01N13/00 ,  G01N11/00 ,  G01N11/14 ,  G01N15/08

    CPC分类号： G01N11/14 ,  G01N15/08 ,  G01N2011/0046

    摘要： A process for measuring the liquid absorption capacity of a powder includes the step of spraying a liquid in the form of a spray cone at a constant throughput from at least one spraying device onto a powder being stirred in the mixing chamber of a mixer, the powder filing between 10 to 80% of the mixing chamber. The torque of the stirrer of the mixer is measured both before and during the spraying step, and from this measurement both a maximum level of the torque and the time difference between the beginning of the spraying step and the time when the maximum level is reached are determined. An amount of liquid absorption of the powder is then determined based upon the liquid mass which is sprayed during that time difference.

    摘要翻译： 用于测量粉末的液体吸收能力的方法包括将喷雾锥形式的液体以至少一种喷雾装置的恒定通过量喷射到在混合器的混合室中搅拌的粉末的步骤，粉末 填充在混合室的10至80％之间。 在喷雾步骤之前和期间测量混合器的搅拌器的扭矩，并且从该测量中，扭矩的最大水平和喷雾步骤开始之间的时间差与达到最大水平的时间之间是 决心。 然后基于在该时间差期间喷射的液体质量来确定粉末的液体吸收量。

    Azo dyes and the production and use thereof
    6.
    发明授权
    Azo dyes and the production and use thereof 失效
    偶氮染料及其生产和使用

    公开(公告)号：US4327018A

    公开(公告)日：1982-04-27

    申请号：US75861

    申请日：1979-09-17

    申请人： Hans W. Liechti ,  Kurt Burdeska ,  Jurgen Markert

    发明人： Hans W. Liechti ,  Kurt Burdeska ,  Jurgen Markert

    IPC分类号： C09B29/42 ,  C09B44/08 ,  D06P1/16 ,  C09B29/36

    CPC分类号： C09B29/363

    摘要： New azo dyes are disclosed which are free from sulphonic acid groups and which are optionally quaternized in the coupling component, and mixtures of such dyes, which dyes correspond to the formula ##STR1## wherein X represents chlorine, optionally substituted phenyloxy, phenylmercapto, alkylmercapto, naphthyloxy, naphthylmercapto, or a heterocyclic radical which is bound by way of --O--, --NH-- or --S--, X.sub.1 represents hydrogen, cyano, lower alkoxy, carboxy, optionally branched and/or substituted alkyl having 1 to 12 carbon atoms, optionally branched and/or substituted lower alkenyl, optionally substituted cycloalkyl, aralkyl having 7 to 10 carbon atoms, aryl, carbamoyl, or a heterocyclic radical, W represents hydrogen, a cyano group, an optionally branched and/or substituted lower alkyl group, an optionally substituted cycloalkyl group, an aralkyl group (having 7 to 10 carbon atoms), an aryl group or the radicals ##STR2## wherein R.sub.1 and R.sub.2 represent lower alkyl, R.sub.2 also represents optionally substituted cycloalkyl, aralkyl or aryl, and R.sub.3 and R.sub.4 represent hydrogen, lower alkyl, hydroxyalkyl, lower alkoxyaryl, cycloalkyl, aralkyl or aryl, and the alkyl radicals R.sub.3 and R.sub.4 can also be bound direct or by way of a hetero atom, R represents hydrogen, optionally substituted amino, optionally branched and/or substituted alkyl, optionally branched and/or substituted alkenyl, optionally substituted cycloalkyl, aralkyl or aryl or a heterocyclic radical, which dyes are useful for the dyeing and printing of synthetic fibres, especially polyester fibres if non quaternized dyes are used or acrylic fibres if quaternized dyes are used.

    摘要翻译： 公开了新的偶氮染料，其不含磺酸基团，并且其任选在偶联组分中季铵化，以及这些染料的混合物，其染料对应于下式：其中X表示氯，任选取代的苯氧基，苯巯基，烷基巯基， 萘基氧基，萘基巯基或通过-O - ， - NH-或-S-键合的杂环基，X1表示氢，氰基，低级烷氧基，羧基，任选支链和/或取代的碳原子数1〜12的烷基 ，任选支链和/或取代的低级烯基，任选取代的环烷基，具有7至10个碳原子的芳烷基，芳基，氨基甲酰基或杂环基，W表示氢，氰基，任选支链和/或取代的低级烷基， 任选取代的环烷基，芳烷基（具有7至10个碳原子），芳基或基团，其中R 1和R 2表示低级烷基，R 2也表示任选的 取代的环烷基，芳烷基或芳基，R3和R4表示氢，低级烷基，羟基烷基，低级烷氧基芳基，环烷基，芳烷基或芳基，烷基R3和R4也可以直接或通过杂原子结合，R表示 氢，任选取代的氨基，任选支链和/或取代的烷基，任选支链和/或取代的烯基，任选取代的环烷基，芳烷基或芳基或杂环基，该染料可用于合成纤维，特别是聚酯纤维的染色和印花 如果使用非季铵化染料，如果使用季铵化染料，则使用丙烯酸纤维。

    Process for the pretreatment or finishing of materials with application of a short liquor ratio
    7.
    发明授权
    Process for the pretreatment or finishing of materials with application of a short liquor ratio 失效
    使用短液比的材料的预处理或整理过程

    公开(公告)号：US3957429A

    公开(公告)日：1976-05-18

    申请号：US480455

    申请日：1974-06-18

    申请人： Willi Leutenegger ,  Jakob Buhler ,  Jurgen Markert ,  Jacques Zurbuchen

    发明人： Willi Leutenegger ,  Jakob Buhler ,  Jurgen Markert ,  Jacques Zurbuchen

    IPC分类号： D06M13/00 ,  D06L3/12 ,  D06M13/02 ,  D06M13/325 ,  D06M13/328 ,  D06M13/33 ,  D06M15/00 ,  D06M23/10 ,  D06P1/90 ,  D06P1/92 ,  D06P5/00 ,  D06P5/04

    CPC分类号： D06P1/924 ,  D06L3/12 ,  D06L3/1271 ,  D06M23/10 ,  D06P1/928 ,  Y10S8/917

    摘要： A Process is described for the pretreatment or finishing of materials with processing agents dissolved or dispersed in water or in organic solvents, wherein the portion of the treatment liquor or of the pretreatment liquor containing the processing agent constitutes the volumetrically smaller part, and the remaining portion of this treatment liquor consists of at least one inert organic compound selected from a water-insoluble, aliphatic, cycloaliphatic and aromatic compound which is perfluorinated or mixed-halogenated, or which contains a perfluorinated or mixed-halogenated radical which compounds are immiscible with the treatment liquor; and wherein the liquor optionally contains additional auxiliaries that do not form an emulsion with the inert organic compound, and the system is very thoroughly mixed during the pretreatment or finishing process.

    摘要翻译： 描述了用于溶解或分散在水中或在有机溶剂中的处理剂预处理或整理材料的方法，其中处理液或含有处理剂的预处理液的部分构成体积较小的部分，剩余部分 该处理液由至少一种选自全氟化或混合卤化的水不溶性，脂肪族，脂环族和芳族化合物的惰性有机化合物组成，或含有全氟化或混合卤化基团，该化合物与处理不混溶 酒; 并且其中所述液体任选地含有不与所述惰性有机化合物形成乳液的附加助剂，并且在所述预处理或整理过程期间所述体系非常完全混合。

    Composition based on liquid crystal for electro-optical device
    10.
    发明授权
    Composition based on liquid crystal for electro-optical device 失效
    基于液晶的组合物用于电光装置

    公开(公告)号：US4428858A

    公开(公告)日：1984-01-31

    申请号：US186138

    申请日：1980-09-11

    申请人： Jacques Cognard ,  Trung H. Phan ,  Jurgen Markert

    发明人： Jacques Cognard ,  Trung H. Phan ,  Jurgen Markert

    IPC分类号： C09B1/54 ,  C09K19/60 ,  G02F1/13 ,  G02F1/137 ,  G09F9/35 ,  C09K3/34

    CPC分类号： C09K19/603 ,  C09B1/547

    摘要： A composition for use in an electro-optical device, particularly a display device, contains anthraquinone pleochroic dye of formula (I): ##STR1## where R.sub.1 is a substituted or unsubstituted amino group or a hydroxy group; R.sub.2 is a hydrogen, a substituted or unsubstituted amino, a hydroxy or a cyano group; each of R.sub.3 and R.sub.4, which are identical or different, is a hydrogen atom, a substituted or unsubstituted amino group, a hydroxy, a nitro or a cyano group; R is a hydrogen or halogen atom or a hydroxy, lower alkyl or lower alkoxy group; n is 1, 2, 3 or 4, the Rs being identical or different when n is 2, 3 or 4; and X is a hydrogen or halogen atom, a hydroxy or mercapto group, a straight, branched or cyclic C.sub.1-16 alkyl radical, a substituted or unsubstituted aryl group or a group of formula OR', OAr, SR', SAr, COOR', COOAr, COO--C.sub.6 H.sub.4 --R', OOCR', OOCAr, OOC--C.sub.6 H.sub.4 --R', CONHR', CONHAr, NHR', NHAr, NHCOR', NHCOAr, OCOOR', OCOOAr, CH.dbd.N--C.sub.6 H.sub.4 --R', N.dbd.CH--C.sub.6 H.sub.4 --R', N.dbd.N--C.sub.6 H.sub.4 --R' or ##STR2## where R' is a hydrogen atom or a straight, branched or cyclic C.sub.1-10 alkyl residue.Compounds of formula (I) have a high order parameter and are very stable.

    摘要翻译： 用于电光装置，特别是显示装置的组合物含有式（I）的蒽醌多色染料：其中R1是取代或未取代的氨基或羟基; R2是氢，取代或未取代的氨基，羟基或氰基; R 3和R 4各自相同或不同，为氢原子，取代或未取代的氨基，羟基，硝基或氰基; R是氢或卤素原子或羟基，低级烷基或低级烷氧基; n为1,2,3或4，当n为2,3或4时，Rs相同或不同; X是氢或卤原子，羟基或巯基，直链，支链或环状的C 1-16烷基，取代或未取代的芳基或式OR'的基团，OAr，SR'，SAr，COOR' ，COOAr，COO-C6H4-R'，OOCR'，OOCAr，OOC-C6H4-R'，CONHR'，CONHAr，NHR'，NHAr，NHCOR'，NHCOAr，OCOOR'，OCOOAr，CH = N-C6H4-R' ，N = CH-C 6 H 4 -R'，N = N-C 6 H 4 -R'或者其中R'是氢原子或直链，支链或环状C 1-10烷基残基。 式（I）化合物具有高阶参数并且非常稳定。