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    Process for producing glycerol carbonate methacrylate
    1.
    发明授权
    Process for producing glycerol carbonate methacrylate 有权

    公开(公告)号：US11254648B2

    公开(公告)日：2022-02-22

    申请号：US16771885

    申请日：2018-12-07

    Applicant: BASF SE

    Inventor： Andrea Misske ,  Christoph Fleckenstein ,  Matthias Klueglein

    IPC: C07D317/38

    Abstract: A process for preparing glycerol carbonate methacrylate, wherein glycidyl methacrylate is reacted with carbon dioxide in the presence of a catalyst and a solvent,
    wherein the catalyst is potassium iodide, the solvent is acetonitrile, one or more monoalcohols, or any desired mixture of acetonitrile and one or more monoalcohols, and the reaction of glycidyl methacrylate with carbon dioxide is carried out at a pressure from 0.5 to 5 bar.

    Process for preparing isosorbide ethoxylate di(meth)acrylate
    4.
    发明授权
    Process for preparing isosorbide ethoxylate di(meth)acrylate 有权
    异山梨醇乙氧基化二（甲基）丙烯酸酯的制备方法

    公开(公告)号：US09562054B2

    公开(公告)日：2017-02-07

    申请号：US15051974

    申请日：2016-02-24

    Applicant: BASF SE

    Inventor： Andrea Misske ,  Friederike Fleischhaker ,  Christoph Fleckenstein ,  Martin Kaller ,  Ulrik Stengel ,  Mathieu Blanchot ,  Claudia Stoer ,  Ritesh Nair

    IPC: C07D493/04 ,  C08F24/00 ,  C09J4/06 ,  C08F222/10 ,  C09J4/00

    CPC classification number: C07D493/04 ,  C08F222/1006 ,  C09J4/00 ,  C09J4/06

    Abstract: A process for preparing isosorbide ethoxylate di(meth)acrylate by transesterifying alkyl (meth)acrylate with isosorbide ethoxylate, comprising the steps of: (i) ethoxylating isosorbide to give isosorbide ethoxylate, (ii) reacting alkyl (meth)acrylate with isosorbide ethoxylate in the presence of potassium phosphate as catalyst and a stabilizer and in the presence of an azeotroping agent which forms an azeotrope with the alcohol bound in the alkyl (meth)acrylate, (iii) continuously distilling off the azeotrope of azeotroping agent and alcohol, wherein steps (ii) and (iii) are conducted simultaneously until the isosorbide ethoxylate has been essentially fully converted, (iv) removing the catalyst from the product mixture comprising isosorbide ethoxylate di(meth)acrylate, (v) distilling unconverted alkyl (meth)acrylate and azeotroping agent out of the product mixture.

    Abstract translation: 包括以下步骤：（i）乙氧基化异山梨醇，得到异山梨醇乙氧基化物，（ii）使（甲基）丙烯酸烷基酯与异山梨醇乙氧基化物反应，得到异山梨醇乙氧基化物 在与（甲基）丙烯酸烷基酯结合的醇形成共沸物的共沸物存在下，连续蒸馏共沸剂和醇的共沸物，其中步骤 （ii）和（iii）同时进行，直到异山梨醇乙氧基化物已经基本上完全转化，（iv）从包含异山梨醇乙氧基化物二（甲基）丙烯酸酯的产物混合物中除去催化剂，（v）蒸馏未转化的（甲基） 共沸剂排出产品混合物。

    Curable compositions
    5.
    发明授权
    Curable compositions 有权

    公开(公告)号：US10829588B2

    公开(公告)日：2020-11-10

    申请号：US15742675

    申请日：2016-06-22

    Applicant: BASF SE

    Inventor： Friederike Fleischhaker ,  Andrea Misske ,  Christoph Fleckenstein ,  Miran Yu ,  Martin Kaller ,  Uwe Meisenburg

    IPC: C08G59/56 ,  C08G59/58 ,  C08G59/50

    Abstract: A curable composition comprises a) at least one epoxide compound E having at least two epoxide groups; b) at least one amine A having at least two amine hydrogens; and c) at least one acrylic ester U; wherein the epoxide compound E comprises at least one epoxide compound E′, the amine A comprises at least one amine A′, and the acrylic ester U comprises at least one acrylic ester U′ whose Hansen solubility parameters for the dipole forces δp and for the specific interactions δh satisfy the following conditions: ( δ p ⁡ ( U ′ ) - δ p ⁡ ( E ′ ) ) 2 + ( δ h ⁡ ( U ′ ) - δ h ⁡ ( E ′ ) ) 2 ≥ 1.5 ⁢ ⁢ and ( δ p ⁡ ( U ′ ) 2 + δ h ⁡ ( U ′ ) 2 ) - ( δ p ⁡ ( A ′ ) 2 + δ h ⁡ ( A ′ ) 2 ) ≥ 0 . A suitable choice of the Hansen solubility parameters of the constituents ensures that the acrylic ester is incorporated covalently into the curing material, preventing subsequent evaporation of the diluent.

    Acrylate-based monomers for use as reactive diluents in printing formulations
    10.
    发明授权
    Acrylate-based monomers for use as reactive diluents in printing formulations 有权

    公开(公告)号：US10745576B2

    公开(公告)日：2020-08-18

    申请号：US16484896

    申请日：2018-02-09

    Applicant: BASF SE

    Inventor： Christoph Fleckenstein ,  Juergen Baro ,  Erich Beck ,  Martin Kaller ,  Andrea Misske ,  Friederike Fleischhaker

    IPC: C09D11/107 ,  C09D11/101 ,  C09D11/30 ,  B41J11/00 ,  C08L33/14 ,  C08L67/06 ,  C08L75/14

    Abstract: The invention relates to compositions, comprising. a) 1.00 to 65.00% by weight of at least one compound of formula (I), wherein R1, R2, R3, R4 are each independently H, C1-C6-alkyl, C1-C6-alkoxy, or C1-C6-alkoxy-C1-C6-alkyl; R is H or C1-C6-alkyl; X is CR6R7, O, or NR8; R6R7 are each independently H, C1-C6-alkyl, C1-C6-alkoxy, or C1-C6-alkoxy-C1-C6-alkyl; R8 is H, C1-C6-alkyl, or C1-C6-alkoxy-C1-C6-alkyl; k is 1, 2, 3, 4 or 5, as component A; b) 1.00 to 60.00% by weight of at least one monomer having two (meth)acrylate groups and having a molecular weight of no more than 500 Dalton, as component B; c) 0 to 25% by weight of at least one monomer having at least three (meth)acrylate groups and having a molecular weight of no more than 600 Dalton, as component C; and d) 1.00 to 30.00% by weight of at least one polymer having at least two (meth)acrylate groups and having a molecular weight of at least 700 Dalton, as component D; with the proviso that the amount of components A+B is at least 50% by weight, as well as the use of these compositions as printing inks, in particular inkjet printing inks.

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