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1.发明授权Process for preparing a dinitronaphthalene isomer mixture having an increased proportion of 1,5- dinitronaphthalene 失效制备1,5-二硝基萘比例增加的二硝基萘异构体混合物的方法公开(公告)号：US06420616B1
公开(公告)日：2002-07-16
申请号：US09726241
申请日：2000-11-29
IPC分类号： C07C20500
CPC分类号： C07C201/08 , C07C205/06
摘要： The present invention relates to a process for preparing a dinitronaphthalene isomer mixture having an increased proportion of 1,5-dinitronaphthalene by nitrating naphthalene in the presence of at least one ionic liquid.
摘要翻译： 本发明涉及一种通过在至少一种离子液体的存在下硝化萘来制备二硝基萘异构体混合物的方法，该混合物具有增加的1,5-二硝基萘的比例。
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公开(公告)号：US07148374B2
公开(公告)日：2006-12-12
申请号：US10738729
申请日：2003-12-17
申请人： Dorota Greszta-Franz , Christoph Gürtler , Reinhard Halpaap , Michael Schelhaas , Michael Grahl
发明人： Dorota Greszta-Franz , Christoph Gürtler , Reinhard Halpaap , Michael Schelhaas , Michael Grahl
IPC分类号： C07C265/00 , C04B9/02
CPC分类号： C08G18/798 , C08G18/755 , C08G18/758 , C08G18/792 , C08G18/8009 , C08G18/8093 , C08G2150/20 , C09D175/04
摘要： The present invention relates to novel blocked, elimination-free polyurethane (PUR) crosslinking agents, to a process for their preparation and to their use as starting components for the production of polyurethane plastics, especially as crosslinking agents for thermally crosslinkable powder coatings.
摘要翻译： 本发明涉及新型的封闭，无消除聚氨酯（PUR）交联剂，其制备方法及其作为用于生产聚氨酯塑料的起始组分的用途，特别是用于热交联粉末涂料的交联剂。
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公开(公告)号：US06843933B2
公开(公告)日：2005-01-18
申请号：US10458040
申请日：2003-06-10
IPC分类号： C07C235/82 , C08G18/79 , C08G18/80 , C09D175/04 , C09D175/06 , C07C26/500
CPC分类号： C09D175/06 , C08G18/792 , C08G18/8093 , Y10T428/31551 , Y10T428/31605
摘要： Blocked polyisocyanates, their preparation and use in one-component coating materials. In organic polyisocyanates having at least two isocyanate groups, the isocyanate groups are blocked with OH acidic cyclic ketones of the general formula (I). The blocked polyisocyanate system of the invention reacts without elimination of the blocking agent and possesses low crosslinking temperatures.
摘要翻译： 封闭的多异氰酸酯，其制备和用于单组分涂料。 在具有至少两个异氰酸酯基团的有机多异氰酸酯中，异氰酸酯基团用通式（I）的OH酸性环酮封闭。 本发明的封端多异氰酸酯体系在不消除封闭剂的情况下反应并具有低交联温度。
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公开(公告)号：US07057003B2
公开(公告)日：2006-06-06
申请号：US10738742
申请日：2003-12-17
申请人： Kamelia Detig-Karlou , Joachim Simon , Michael Mager , Thomas Stingl , Christoph Gürtler , Michael Schelhaas
发明人： Kamelia Detig-Karlou , Joachim Simon , Michael Mager , Thomas Stingl , Christoph Gürtler , Michael Schelhaas
IPC分类号： C08G18/80
CPC分类号： C08G18/4866 , C08G18/10 , C08G18/12 , Y10T428/31551 , C08G18/64 , C08G18/2895
摘要： The invention relates to novel blocked polyurethane prepolymers, to a process for their preparation, to reactive systems prepared therefrom that cure at room temperature, and to their use.
摘要翻译： 本发明涉及新的封端聚氨酯预聚物，其制备方法，由其制备的反应体系，其在室温下固化及其用途。
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公开(公告)号：US06827875B2
公开(公告)日：2004-12-07
申请号：US10185512
申请日：2002-06-28
IPC分类号： C08G1880
CPC分类号： C08G18/792 , C08G18/8093 , C09D175/06 , Y10T428/31551 , Y10T428/31605
摘要： The present invention relates to new blocked polyisocyanates with which high-grade, emission-free coatings and lacquer coatings with reduced yellowing values can be obtained, to a method of producing them, and to the use thereof in one-component polyurethane systems, particularly as crosslinking agents in automobile primer surfacers.
摘要翻译： 本发明涉及新的封端多异氰酸酯，其可获得具有降低的黄变值的高级无排放涂料和漆层，其制备方法及其在单组分聚氨酯体系中的用途，特别是作为 汽车底漆表面活性剂中的交联剂。
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公开(公告)号：US07553906B2
公开(公告)日：2009-06-30
申请号：US10738879
申请日：2003-12-17
IPC分类号： C08G18/80 , C08G18/81 , C08L75/14 , C07C233/57 , C07C263/00
CPC分类号： C08G18/672 , C08G18/8048 , C08G18/8093 , C08G18/8096 , C08G18/8175 , C08L75/16 , C09D175/16 , Y10T428/31551 , C08G18/62 , C08L2666/20
摘要： An organic polyisocyanate with at least one unsaturated functional group is capable of copolymerizing when exposed to actinic radiation. The polyisocyanate comprises structural units with the formula (1): wherein: X is an electron-attracting group; R1, and R2 are hydrogen atoms, a saturated or unsaturated aliphatic or cycloaliphatic radical, or an aromatic or araliphatic radical; and n is an integer from 0 to 5. A process for producing this polyisocyanate is also disclosed.
摘要翻译： 具有至少一个不饱和官能团的有机多异氰酸酯在暴露于光化辐射时能够共聚。 多异氰酸酯包括具有式（1）的结构单元：其中：X是吸电子基团; R1和R2是氢原子，饱和或不饱和的脂族或脂环族基团，或芳族或芳脂族基团; 并且n为0至5的整数。还公开了制备该多异氰酸酯的方法。
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公开(公告)号：US06790976B2
公开(公告)日：2004-09-14
申请号：US09893858
申请日：2001-06-28
IPC分类号： C07C25300
CPC分类号： C07C253/00 , C07C255/05
摘要： The present invention relates to a process for producing tricarbonitriles corresponding to formula I wherein n is an integer from 2 to 11 by forming an intermediate in the presence of a strong base in a first stage from an aliphatic &agr;-&ohgr;-dinitrile corresponding to formula II wherein n is an integer from 3 to 12, and reacting the intermediate in a second stage to form a trinitrile corresponding to formula I by the addition of acrylonitrile.
摘要翻译： 本发明涉及一种制备相应于式I的方法，其中n为2至11的整数，通过在第一阶段中在强碱存在下，形成对应于式II的脂族α-ω-二腈的中间体，其中n为 3至12的整数，并在第二阶段使中间体反应，通过加入丙烯腈形成对应于式I的三腈。
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公开(公告)号：US06437180B1
公开(公告)日：2002-08-20
申请号：US09568894
申请日：2000-05-11
IPC分类号： C07C5116
CPC分类号： C07C51/285 , C07C55/02 , C07C55/14
摘要： A process for preparing aliphatic C4-18 &agr;,&ohgr;-dicarboxylic acids by oxidation of C6-20 &agr;,&ohgr;-dienes with hydrogen peroxide or compounds which release hydrogen peroxide under the reaction conditions as is characterized in that the reaction is carried out in the presence of a transition metal catalyst of group VI and of a mixture containing at least one organic acid and one aprotic organic solvent. A specific temperature profile is maintained at different phases of the reaction, which increases yield and selectivity.
摘要翻译： 通过在反应条件下通过氧化C6-20α，ω-二烯与过氧化氢或释放过氧化氢的化合物来制备脂族C4-18α，ω-二羧酸的方法，其特征在于反应在 存在第VI族的过渡金属催化剂和含有至少一种有机酸和一种非质子有机溶剂的混合物。 在反应的不同阶段保持特定的温度曲线，这提高了产率和选择性。
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公开(公告)号：US06414192B1
公开(公告)日：2002-07-02
申请号：US10007014
申请日：2001-11-06
申请人： Michael Schelhaas , Carl Casser , Dietmar Bielefeldt , Pieter Ooms , Joachim Haider , Manfred Jautelat , Christian Laue , Henry Giera
发明人： Michael Schelhaas , Carl Casser , Dietmar Bielefeldt , Pieter Ooms , Joachim Haider , Manfred Jautelat , Christian Laue , Henry Giera
IPC分类号： C07C20900
CPC分类号： C07C209/38 , C07C211/55
摘要： The invention provides a process for preparing 4-aminodiphenylamine, an important starting product for synthesizing antioxidants and stabilizers in the rubber and polymer industry, by hydrogenating nitrosobenzene with hydrogen in the presence of a proton acid as catalyst and in the presence of a hydrogenating catalyst, optionally in the presence of an inert organic solvent and thermally decomposing the 4-ADPA ammonium salt produced in this way, wherein 4-ADPA is obtained. 4-aminodiphenylamine is produced in good yields and high purity by the process according to the present invention. Furthermore, no effluent is produced, which makes the process particularly economic and ecological.
摘要翻译： 本发明提供一种制备4-氨基二苯胺的方法，该方法是在质子酸作为催化剂存在下，在氢化催化剂存在下，通过在氢气存在下，用氢气将亚硝基苯氢化，在橡胶和聚合物工业中合成抗氧化剂和稳定剂的重要起始产物， 任选地在惰性有机溶剂的存在下，并以这种方式产生的4-ADPA铵盐热分解，得到4-ADPA。4-氨基二苯胺通过本发明的方法以良好的产率和高纯度生产。 此外，没有产生流出物，这使得该过程特别经济和生态。
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公开(公告)号：US06706924B2
公开(公告)日：2004-03-16
申请号：US10028892
申请日：2001-12-18
IPC分类号： C07C21158
CPC分类号： C07C251/20 , C07C201/12 , C07C205/45 , C07C209/28 , C07C209/36 , C07C209/48 , C07C209/60 , C07C209/68 , C07C211/60 , C07C221/00 , C07C233/11 , C07C249/02 , C07C253/30 , C07C255/42 , C07C2602/10 , C07C225/22 , C07C211/58 , C07C255/35 , C07C211/48
摘要： The invention relates to a process for the production of 1,5-naphthalenediamine and to the intermediates 4-(2-nitrophenyl)butyronitrile, 5-nitro-3,4-dihydro-1(2H)-naphthyl-imine, 5-nitroso-1-naphthylamine, 5-nitro-1-naphthylamine, 4-(2-aminophenyl)-butyronitrile, 5-amino-3,4-dihydro-1(2H)-naphthalene imine, 4-(2-nitrophenyl)ethyl butyrate and 4-(2-nitrophenyl)butyramide obtainable during the process.
摘要翻译： 本发明涉及一种生产1,5-萘二胺的方法和中间体4-（2-硝基苯基）丁腈，5-硝基-3,4-二氢-1（2H） - 萘基亚胺，5-亚硝基 1-萘胺，5-硝基-1-萘胺，4-（2-氨基苯基） - 丁腈，5-氨基-3,4-二氢-1（2H） - 萘亚胺，4-（2-硝基苯基）丁酸乙酯 和4-（2-硝基苯基）丁酰胺。
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