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公开(公告)号：US5087714A
公开(公告)日：1992-02-11
申请号：US709593
申请日：1991-06-03
CPC分类号： C07F7/1896 , C07F7/20
摘要： Discoloration of vinylacetoxysilanes is prevented by adding thereto 25 to 500 ppm, based on the amount of vinylacetoxysilane, of 3,5-di-tert.-butylpyrocatechol, 2,6-di-tert.-butyl-4-methylphenol, 2-mercaptobenzimidazole or a mixture thereof.
摘要翻译： 通过向乙烯基乙酰氧基硅烷的量加入25〜500ppm 3,5-二叔丁基邻苯二酚，2,6-二叔丁基-4-甲基苯酚，2-巯基苯并咪唑 或其混合物。
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2.发明授权
公开(公告)号：US5187291A
公开(公告)日：1993-02-16
申请号：US868548
申请日：1992-04-14
申请人： Claus-Dietrich Seiler , Reinhold Schork , Albert Frings , Hans-Joachim Kotzsch , Hartwig Rauleder
发明人： Claus-Dietrich Seiler , Reinhold Schork , Albert Frings , Hans-Joachim Kotzsch , Hartwig Rauleder
CPC分类号： C07F7/20 , C07C51/60 , C07F7/1896
摘要： Acyloxysilanes and carboxylic acid chlorides can be prepared simultaneously and continuously from organochlorosilanes and monocarboxylic acid anhydrides. Catalytically active amounts of organic bases soluble in the reaction mixture, their salts or organic acid amides are employed here.
摘要翻译： 氰基硅烷和羧酸氯化物可以从有机氯硅烷和一元羧酸酐同时连续制备。 催化活性量的可溶于反应混合物的有机碱，其盐或有机酸酰胺在这里被使用。
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公开(公告)号：US5591818A
公开(公告)日：1997-01-07
申请号：US413042
申请日：1995-03-29
申请人： Burkhard Standke , Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Kotzsch , Hermann Peeters
发明人： Burkhard Standke , Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Kotzsch , Hermann Peeters
IPC分类号： C08G77/26 , C08G77/28 , C08G77/388 , C08K9/06 , C09J183/00 , C09J183/08
CPC分类号： C08G77/388 , C08G77/26 , C08K9/06
摘要： Disclosed are organosilane polycondensation products prepared by hydrolysis of an hydrogen salt of an aminosilane compound or by hydrolysis of an aminosilane followed by reaction with an alkyl salt. The compounds are useful in forming stable aqueous solutions and as adhesion promoters between inorganic and organic surfaces.
摘要翻译： 公开了通过氨基硅烷化合物的氢盐的水解或氨基硅烷的水解，然后与烷基盐反应制备的有机硅烷缩聚产物。 该化合物可用于形成稳定的水溶液和作为无机和有机表面之间的粘合促进剂。
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公开(公告)号：US5107009A
公开(公告)日：1992-04-21
申请号：US738348
申请日：1991-07-31
IPC分类号： C07F7/18
CPC分类号： C07F7/1892
摘要： Mercaptosilanes are prepared from haloorganylsilyl compounds and an alkali metal hydrogen sulfide in the presence of a polar, aprotic medium.
摘要翻译： 巯基硅烷由卤代有机基甲硅烷基化合物和碱金属硫化氢在极性非质子介质存在下制备。
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公开(公告)号：US5208359A
公开(公告)日：1993-05-04
申请号：US812586
申请日：1991-12-20
CPC分类号： C07F7/045 , C07F7/1896
摘要： Di-tert.butoxydiacetoxysilane is prepared by reacting tetraacetoxysilane with tert.butanol at a reaction temperature of up to 60.degree. C., and the resulting di-tert.butoxydiacetoxysilane is isolated.
摘要翻译： 二叔丁氧基二乙酰氧基硅烷是通过在高达60℃的反应温度下使四乙酰氧基硅烷与叔丁醇反应制得的，分离所得的二叔丁氧基二乙酰氧基硅烷。
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6.发明授权Water-based organopolysiloxane-containing compositions, processes for their preparation and their use 失效含水基的含有机聚硅氧烷的组合物，其制备方法及其用途
公开(公告)号：US5629400A
公开(公告)日：1997-05-13
申请号：US568384
申请日：1995-12-06
申请人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Kotzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Jim Steinmetz
发明人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Kotzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Jim Steinmetz
IPC分类号： C08L83/08 , B01F17/54 , C08G77/26 , C08G77/28 , C08L83/04 , C09D183/04 , C09D183/08 , C09J183/00 , C09J183/08
CPC分类号： C09D183/08 , C08G77/26
摘要： The invention relates to water-based organopolysiloxane containing compositions which are essentially free from organic solvents, have a flash point above 70.degree. C. and essentially liberate no alcohols by hydrolysis on dilution with water. The organopolysiloxane-containing compositions according to the invention are obtainable by mixing M mol of water-insoluble organotrialkoxysilanes with Q mol of water-soluble aminoalkylalkoxysilanes in a molar ratio of 0
摘要翻译： 本发明涉及基本上不含有机溶剂的含水基有机聚硅氧烷的组合物，其闪点高于70℃，并且在用水稀释时基本上不通过水解释放醇。 根据本发明的含有机聚硅氧烷的组合物可通过将M摩尔不溶于水的有机三烷氧基硅烷与摩尔比为0
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公开(公告)号：US4228092A
公开(公告)日：1980-10-14
申请号：US000605
申请日：1979-01-02
摘要： An improvement in a process for the esterification of a organochlorosilane by feeding alcohol into a chlorosilane maintained within a reaction zone without said alcohol contacting said chlorosilane in the gas phase wherein the esterification is performed stepwise with extraction of hydrogen chloride which has developed, the improvement which comprises employing in at least a final esterification step an organochlorosilane of the formulaH.sub.a R.sub.b SiCl.sub.4-a-bwhereinR represents an optionally halogen-substituted alkyl radical which can also contain an oxygen or sulfur atom in the chain, or a halogen or a NO.sub.2 group or a protected phenolic group containing aryl radical,a equals 0, 1, or 2,b equals 1 or 2, anda+b amounts to a maximum of 3,said final esterification step being performed with the addition of heat.
摘要翻译： 通过将醇保持在反应区内的氯硅烷中而不使醇与气相中的氯代硅烷接触来改善有机氯代硅烷的酯化反应，其中通过萃取开发的氯化氢逐步进行酯化，其改进是 包括在至少最终酯化步骤中使用式HaRbSiCl4-ab的有机氯硅烷，其中R表示任选的卤素取代的烷基，其还可以在链中含有氧或硫原子，或卤素或NO 2基团或被保护的 含酚基的芳基，等于0,1或2，b等于1或2，a + b最多达3，所述最终酯化步骤是通过加热进行的。
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8.发明授权
公开(公告)号：US4226793A
公开(公告)日：1980-10-07
申请号：US946464
申请日：1978-09-28
CPC分类号： C07F7/04
摘要： An improvement in a process for forming an orthosilicic acid ester or an oligomer thereof by contacting a tetrachlorosilane or higher homolog thereof with a primary alcohol, the improvement which comprises introducing the alcohol directly into a tetrachlorosilane liquid phase without said alcohol touching the gas phase and, after completion of the reaction, removing hydrogen chloride formed during the reaction from the reaction zone.
摘要翻译： 通过使四氯硅烷或其高级同系物与伯醇接触来形成正硅酸酯或其低聚物的方法的改进，其包括将醇直接引入四氯硅烷液相中而没有所述醇与气相接触， 反应完成后，从反应区除去反应期间形成的氯化氢。
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公开(公告)号：US4152346A
公开(公告)日：1979-05-01
申请号：US533728
申请日：1974-12-17
IPC分类号： C08K9/00 , C07F7/10 , C07F7/18 , C08G77/00 , C08G77/06 , C08G77/22 , C08G77/28 , C08G77/38 , C08K9/06
CPC分类号： C07F7/182
摘要： Aminoethylsilanes of the following formula: ##STR1## AMINOETHYLSILOXANES HAVING THE STRUCTURAL UNITS ##STR2## IN WHICH R' represents an aliphatic, saturated or unsaturated hydrocarbon group having 1 to 10 carbon atoms, R" represents an alkyl or oxalkyl radical or the phenyl radical, and a can be equal to 0 or 1 and x equal to 0 or 1 or 2; a process for preparing such aminoethylsilane or aminoethylsiloxane which comprises contacting a beta-halogenethylsilane of the formula: ##STR3## A SILOXANE WITH THE RECURRENT STRUCTURAL UNIT ##STR4## WHEREIN R' is a saturated or unsaturated aliphatic hydrocarbon radical, R" is an alkyl, oxyalkyl or phenyl radical, Y is a halogen atom, a is O or 1 and with ammonia at a temperature between 50 and 120.degree. C.
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公开(公告)号：US4029679A
公开(公告)日：1977-06-14
申请号：US502125
申请日：1974-08-30
IPC分类号： C23C22/48 , C07F9/40 , C09D5/08 , C23F11/167
CPC分类号： C09D5/086 , C07F9/40 , C23F11/1676
摘要： A method for protecting the surface of a metal surface which comprises applying to said surface an organophosphorus compound of the formula ##STR1## wherein A IS 0 OR 1R is a branched or unbranched chained bivalent alkylene radical of 1 to 12 carbon atoms which is substituted or unsubstituted and can contain in the chain structure --O--, --S--, ##STR2## R' is a branched or unbranched alkyl radical of 1 to 12 carbon atoms which can be halogen substituted and can contain in the chain structure ##STR3## X is an epoxy ring, halogen, alkylene, carboxylic acid ester residue, amino, isocyanato, isothiocyanato, urea, thiourea, urethano, alkyl substituted thio radical or the radical or a heterocyclic ring containing O, S or N in the ring structure; a new organophosphorus compounds having the formula set forth above and more particularly defined by specific chemical structures.
摘要翻译： 一种用于保护金属表面的方法，其包括向所述表面施加下式的有机磷化合物，其中A 0 OR 1 R是被取代的1至12个碳原子的支链或非支链链式二价亚烷基 或未取代的并且可以在链结构中包含-O - ， - S-，R'是具有1至12个碳原子的支链或非支链烷基，其可以被卤素取代并且可以含有链结构
X是环状环，卤素，亚烷基，羧酸酯残基，氨基，异氰酸酯基，异硫氰酸根合，脲基，硫脲，氨基甲酰基，烷基取代的硫基或环或在环结构中含有O，S或N的杂环; 具有上述式的新的有机磷化合物，更具体地由具体的化学结构定义。
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