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公开(公告)号：US08772552B2
公开(公告)日：2014-07-08
申请号：US13623653
申请日：2012-09-20
发明人： Rajaram Bal , Shubhra Acharyya Shankha , Shilpi Ghosh , Bipul Sarkar , Karan Singh Rawat , Chandrashekar Pendem
摘要： The present invention provides an improved process for the selective hydroxylation of benzene. The process provides a direct single step selective vapor phase hydroxylation of benzene to phenol using molecular oxygen (air) over Cu—Cr oxide catalysts. The process provides benzene conversion of 10 to 45% and selectivity for phenol up to 100%.
摘要翻译： 本发明提供了苯的选择性羟基化的改进方法。 该方法在Cu-Cr氧化物催化剂上使用分子氧（空气）提供苯与苯的直接单步选择性气相羟基化。 该方法提供10至45％的苯转化率，苯酚的选择性高达100％。
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公开(公告)号：US09889434B2
公开(公告)日：2018-02-13
申请号：US15233572
申请日：2016-08-10
发明人： Rajaram Bal , Bipul Sarkar , Reena Goyal , Ankur Bordoloi , Chandrashekar Pendem , Laxmi Narayan Sivakumar Konathala
IPC分类号： B01J21/06 , B01J23/89 , B01J35/00 , B01J35/10 , B01J37/00 , B01J37/03 , B01J37/06 , B01J37/08 , C01B3/40
CPC分类号： B01J23/892 , B01J23/8953 , B01J35/0013 , B01J35/002 , B01J35/023 , B01J35/1014 , B01J37/0072 , B01J37/009 , B01J37/031 , B01J37/035 , B01J2523/00 , C01B3/40 , C01B2203/0238 , C01B2203/0261 , C01B2203/1058 , C01B2203/107 , C01B2203/1082 , C01B2203/1241 , Y02P20/52 , B01J2523/48 , B01J2523/828 , B01J2523/847
摘要： The present invention provides a process and catalyst for the autothermal and dry reforming of methane to produce syngas. The process provides a direct single step gas phase reforming of methane or natural gas to syngas over Ni—Pt supported nanocrystalline ZrO2. The process provides methane conversion of 54-99% with H2/CO ratio of 1.14 to 1.42 (mol %) in the temperature range of 250 to 750 800° C. at atmospheric pressure.
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3.发明授权Process for the preparation of phosphorous containing mesoporous alumina catalyst for selective dehydration of methanol to dimethyl ether 有权用于制备含磷介孔氧化铝催化剂的方法，用于将甲醇选择性脱水至二甲醚公开(公告)号：US09468914B2
公开(公告)日：2016-10-18
申请号：US14634200
申请日：2015-02-27
发明人： Ankur Bordoloi , Reena Goyal , Subhasis Das , Rajib Kumar Singha , Chandrashekar Pendem , Laxmi Narayan Sivakumar Konathala , Rajaram Bal , Sandeep Saran , Madhukar Onkarnath Garg
CPC分类号： B01J27/16 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/04 , B01J37/08 , C07C41/09 , C07C43/043
摘要： The present invention provides an improved process for the preparation of phosphorous containing mesoporous alumina catalyst for selective dehydration of methanol to dimethyl ether. The process provides a single step selective vapor phase dehydration of methanol to produce dimethyl ether over phosphorous containing mesoporous alumina (P/Al2O3) catalyst at a temperature in the range of 150-350° C. The process provides methanol conversion of 45-100% with a selectivity of the DME up to 100%.
摘要翻译： 本发明提供了一种制备用于将甲醇选择性脱水成二甲醚的含磷介孔氧化铝催化剂的改进方法。 该方法在150-350℃的温度范围内，通过在含磷介孔氧化铝（P / Al 2 O 3）催化剂上提供甲醇单步选择气相脱水生产二甲醚。该方法提供甲醇转化率为45-100％ DME的选择性高达100％。
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4.发明授权Process for the preparation of Cu—Cr oxides for selective oxidation reactions 有权制备用于选择性氧化反应的Cu-Cr氧化物的方法公开(公告)号：US08697916B2
公开(公告)日：2014-04-15
申请号：US13623618
申请日：2012-09-20
发明人： Rajaram Bal , Bipul Sarkar , Shubhra Acharyya Shankha , Shilpi Ghosh , Chandrashekar Pendem , Kumar Jagdish
CPC分类号： B01J23/868 , B01J35/002 , B01J37/0018 , B01J37/036 , B01J37/10 , B01J37/16 , C07B33/00 , C07C29/48 , C07C45/28 , C07C49/78 , C07C47/54
摘要： The present invention provides a process for the preparation of Cu—Cr oxides by hydrothermal synthesis method using hydrazine as a reducing agent and cetyltrimethylammonium bromide as a surfactant and these oxides are very active for selective oxidation of benzene, toluene and ethylbenzene to produce phenol, benzaldehyde and acetophenone, respectively.
摘要翻译： 本发明提供了通过使用肼作为还原剂和十六烷基三甲基溴化铵作为表面活性剂的水热合成方法制备Cu-Cr氧化物的方法，并且这些氧化物对苯，甲苯和乙苯的选择性氧化非常有活性，以产生苯酚，苯甲醛 和苯乙酮。
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5.发明申请PROCESS FOR THE PREPARATION OF CU-CR OXIDES FOR SELECTIVE OXIDATION REACTIONS 有权用于选择性氧化反应的CU-CR氧化物的制备方法公开(公告)号：US20130085305A1
公开(公告)日：2013-04-04
申请号：US13623618
申请日：2012-09-20
发明人： Rajaram Bal , Bipul Sarkar , Shubhra Acharyya Shankha , Shilpi Ghosh , Chandrashekar Pendem , Kumar Jagdish
CPC分类号： B01J23/868 , B01J35/002 , B01J37/0018 , B01J37/036 , B01J37/10 , B01J37/16 , C07B33/00 , C07C29/48 , C07C45/28 , C07C49/78 , C07C47/54
摘要： The present invention provides a process for the preparation of Cu—Cr oxides by hydrothermal synthesis method using hydrazine as a reducing agent and cetyltrimethylammonium bromide as a surfactant and these oxides are very active for selective oxidation of benzene, toluene and ethylbenzene to produce phenol, benzaldehyde and acetophenone, respectively.
摘要翻译： 本发明提供了通过使用肼作为还原剂和十六烷基三甲基溴化铵作为表面活性剂的水热合成方法制备Cu-Cr氧化物的方法，并且这些氧化物对苯，甲苯和乙苯的选择性氧化非常有活性，以产生苯酚，苯甲醛 和苯乙酮。
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公开(公告)号：US10322407B2
公开(公告)日：2019-06-18
申请号：US15380378
申请日：2016-12-15
摘要： The present invention provides a catalyst and a process for the selective oxidation of carbon monoxide (CO) to produce carbon dioxide gas (CO2). The process provides a process which selectively oxidizes CO to CO2 in presence of excess hydrogen. The process provides a selective oxidation of CO to CO2 gas over Cu/CeO2 catalyst between temperature range 40° C. to 90° C. at atmospheric pressure in presence of excess H2, H2O and CO2. The process provides a CO conversion up to 100% without deactivation till 100 h.
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公开(公告)号：US09908101B2
公开(公告)日：2018-03-06
申请号：US14074351
申请日：2013-11-07
发明人： Rajaram Bal , Bipul Sarkar , Rajib Kumar Singha , Chandrashekar Pendem , Shubhra Acharyya Shankha , Shilpi Ghosh
IPC分类号： B01J23/28 , B01J37/03 , B01J37/08 , B01J37/10 , B01J21/06 , B01J35/00 , B01J37/00 , C07C5/48
CPC分类号： B01J23/28 , B01J21/063 , B01J35/002 , B01J37/0018 , B01J37/035 , B01J37/082 , B01J37/10 , C07C5/48 , C07C2521/06 , C07C2523/28 , Y02P20/52 , C07C11/04
摘要： The present invention provides a process and catalyst for the direct and selective conversion of ethane to ethylene. The process provides a direct single step vapor phase selective dehydrogenation/oxidative dehydrogenation of ethane to ethylene over Mo supported nanocrystalline TiO2. The process provides ethane conversion of 65-96% and selectivity of ethylene up to 100%. The process may be conducted in the presence or absence of oxygen.
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8.发明申请Ni-Pt-ZrO2 NANOCRYSTALLINE OXIDE CATALYST AND PROCESS THEREOF USEFUL FOR THE PRODUCTION OF SYNGAS BY COMBINING OXY- DRY REFORMING OF NATURAL GAS 有权Ni-Pt-ZrO2纳米氧化物催化剂及其通过组合天然气的氧气改性有利于生产SYNGAS的方法公开(公告)号：US20170043324A1
公开(公告)日：2017-02-16
申请号：US15233572
申请日：2016-08-10
发明人： Rajaram Bal , Bipul Sarkar , Reena Goyal , Ankur Bordoloi , Chandrashekar Pendem , Laxmi Narayan Sivakumar Konathala
IPC分类号： B01J23/89 , B01J35/10 , B01J35/00 , C01B3/40 , B01J37/06 , B01J37/08 , B01J37/03 , B01J21/06 , B01J37/00
CPC分类号： B01J23/892 , B01J23/8953 , B01J35/0013 , B01J35/002 , B01J35/023 , B01J35/1014 , B01J37/0072 , B01J37/009 , B01J37/031 , B01J37/035 , B01J2523/00 , C01B3/40 , C01B2203/0238 , C01B2203/0261 , C01B2203/1058 , C01B2203/107 , C01B2203/1082 , C01B2203/1241 , Y02P20/52 , B01J2523/48 , B01J2523/828 , B01J2523/847
摘要： The present invention provides a process and catalyst for the autothermal and dry reforming of methane to produce syngas. The process provides a direct single step gas phase reforming of methane or natural gas to syngas over Ni—Pt supported nanocrystalline ZrO2. The process provides methane conversion of 54-99% with H2/CO ratio of 1.14 to 1.42 (mol %) in the temperature range of 250 to 750 800° C. at atmospheric pressure.
摘要翻译： 本发明提供了用于甲烷自热和干重整以产生合成气的方法和催化剂。 该方法在Ni-Pt负载纳米晶ZrO2上提供甲烷或天然气对合成气的直接单步气相重整。 该方法在大气压下，在250〜750 800℃的温度范围内，H 2 / CO比为1.14〜1.42（mol％），甲烷转化率为54-99％。
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9.发明授权公开(公告)号：US09409847B2
公开(公告)日：2016-08-09
申请号：US14072916
申请日：2013-11-06
发明人： Rajaram Bal , Bipul Sarkar , Rajib Kumar Singha , Chandrashekar Pendem , Shubhra Acharyya Shankha , Shilpi Ghosh
IPC分类号： B01J23/889 , B01J35/00 , B01J37/00 , C07C51/285 , B01J37/03 , B01J37/10
CPC分类号： C07C51/285 , B01J23/8892 , B01J35/002 , B01J37/0018 , B01J37/031 , B01J37/10 , C07C57/04
摘要： The present invention provides a process and a solid catalyst for oxydehydration of glycerol to acrylic acid with H2O2 under mild experimental condition at atmospheric pressure. The process provides a single step liquid phase selective oxidation glycerol to acrylic acid over nanocrystalline Cu supported α-MnO2 catalyst. The process provides glycerol conversion of 20-78% and selectivity of acrylic acid up to 86%.
摘要翻译： 本发明提供了一种在大气压下在温和的实验条件下将甘油氧化成丙烯酸与H 2 O 2的方法和固体催化剂。 该方法提供单相液相选择性氧化甘油至丙烯酸超过纳米晶体负载的α-MnO2催化剂。 该方法提供20-78％的甘油转化率和高达86％丙烯酸的选择性。
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公开(公告)号：US10351424B2
公开(公告)日：2019-07-16
申请号：US15085697
申请日：2016-03-30
发明人： Rajaram Bal , Rajib Kumar Singha , Ankur Bordoloi , Chandrashekar Pendem , Laxmi narayan Sivakumar Konathala
IPC分类号： C01B3/40 , B01J37/04 , B01J37/03 , B01J23/755
摘要： The present invention provides a Ni—Zr oxide catalyst and a process for the preparation of the catalyst. The invention further provides use of the catalyst for the production of synthesis gas (a mixture of CO and H2) by Tri-reforming of methane. The process provides a direct single step selective vapor phase partial oxidation of methane to synthesis gas over Ni—ZrO2 catalyst between temperature range of 600° C. to 800° C. at atmospheric pressure. The process provides a methane conversion of 1-99% with H2 to CO mole ratio of 1.6 to 2.2.
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