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公开(公告)号:US20210246291A1
公开(公告)日:2021-08-12
申请号:US17049492
申请日:2018-04-27
Applicant: Dow Global Technologies LLC
Inventor: Bo Lyu , Yong Chen , Rongjuan Cong , Yabin Sun , Tao Han , Bharat I. Chaudhary
Abstract: The present application relates to a composition comprising the following components: A) at least one ethylene/alpha-olefin interpolymer; B) a peroxide; C) at least one filler selected from one or more carbon black samples, MgO, or a combination thereof; and optionally, at least one filler selected from silica, ZnO, CaCO3, A1 (OH)3, Mg (OH)2, or a combination thereof; D) a calculated P content from 0.010 wt % to 0.300 wt %, based on the weight of the composition, and wherein the calculated P content is the calculated content the phosphorus element present in one or more phosphate compounds selected from Structure 1 below: O═P (OR1) (OR2) (OR3) (Structure 1), wherein R1, R2 and R3 are each, independently, selected from i) a non-aromatic hydrocarbon or ii) a non-aromatic hydrocarbon comprising at least one heteroatom, excluding P.
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公开(公告)号:US10761072B2
公开(公告)日:2020-09-01
申请号:US15738939
申请日:2016-08-24
Applicant: Dow Global Technologies LLC
Inventor: Rongjuan Cong , Albert Parrott , Cherry Hollis , Charles Michael Cheatham
Abstract: A temperature gradient chromatography, and apparatus for the same, said method comprising the following: a) dissolving a composition comprising at least one polymer in at least one solvent, to form a polymer solution; b) injecting at least a portion of the polymer solution onto a support material and wherein the support material has a CI from 0.70 to 1.50; c) cooling the support material at a rate greater than, or equal to, 0.2° C./min; d) increasing the temperature of the support material to elute at least some of the polymer; e) generating the chromatogram.
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公开(公告)号:US20190299517A1
公开(公告)日:2019-10-03
申请号:US16435935
申请日:2019-06-10
Applicant: Dow Global Technologies LLC
Inventor: Xiao Bing Yun , Rongjuan Cong , Jianping Pan , Teresa P. Karjala
IPC: B29C55/00 , B32B27/32 , B32B27/34 , B29C55/14 , B32B7/02 , C08J5/18 , C08L23/08 , B32B15/20 , B29C48/00 , B32B15/08 , B32B27/16 , B32B27/10 , B32B27/08 , B32B27/36
Abstract: The present invention discloses a process for forming a biaxially oriented film. The process includes first selecting a polyolefin resin wherein said polyolefin resin comprises a linear low density polyethylene resin characterized by having from 9 to 35 weight percent of the total weight of linear low density polyethylene resin eluting from a CEF at a temperature greater than 97.0° C.; and further characterized by having a CDR of from 33 to 80 and a Mw Ratio of from 0.15 to 0.45. Next a film is formed from the polyolefin resin selected in the first step. Finally the film formed in the second step is oriented in a sequential manner. The films produced by this process are characterized by having an ultimate elongation at least 1.5 times greater in the MD as compared to the CD and the 2% secant modulus is a least 1.25 times greater in the CD as compared to the MD. The films are further characterized by having free residual shrinkage of less than 10% in the MD and less than 10% in the CD when exposed to a temperature of 90° C. for 10 minutes.
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公开(公告)号:US20190210333A1
公开(公告)日:2019-07-11
申请号:US16325888
申请日:2017-08-14
Applicant: Dow Global Technologies LLC
Inventor: Jianping Pan , Xiao Bing Yun , Yijian Lin , Rongjuan Cong
Abstract: Embodiments of the present invention relate to biaxially oriented, multilayer polyethylene films and to laminates and articles formed therefrom. In one aspect, a biaxially oriented, multilayer polyethylene film comprises Layer A which is a sealant layer p having a top facial surface and a bottom facial surface and comprising a first polyethylene, wherein the first polyethylene has a density of at least 0.900 g/cm3, an IHDF>95 of 20-60 kg/mol, and a MWHDF>95 of greater than 130 kg/mol, wherein Layer A comprises at least 50 weight percent of the first polyethylene based on the weight of Layer A, and Layer B having a top facial surface and a bottom facial surface, wherein Layer B comprises one or more additional polyethylenes, and wherein the top facial surface of Layer B is in adhering contact with a bottom facial surface of Layer A, wherein the density of the first polyethylene is at least 0.002 g/cm3 less than the density of Layer B.
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公开(公告)号:US11988650B2
公开(公告)日:2024-05-21
申请号:US17256994
申请日:2019-06-25
Applicant: Dow Global Technologies LLC
Inventor: Rongjuan Cong , Kimberly L. Bailey , Vickie Ricca
CPC classification number: G01N30/54 , G01N30/8679 , G01N33/442 , G01N2030/008 , G01N2030/885
Abstract: A method to determine the weight percent of an “amorphous” fraction in an olefin-based polymer composition, comprising one or more olefin-based polymers; said method comprising the following steps: a) dissolving the olefin-based polymer composition in an organic solvent to form a polymer solution; b) injecting at least a portion of the polymer solution onto a support material, and wherein the support material has a Co-crystallization Index (CI) value from 0.70 to 1.20; c) cooling the support material at a rate greater than, or equal to, 0.2 C/min; d) increasing the temperature of the support material to elute the polymers of the olefin-based polymer composition; e) generating a chromatogram; f) determining the peak area of the first elution from its lower integration limit to its upper integration limit; g) calculating the “amorphous” fraction” based on the following Equation A below: wt % “amorphous” fraction=PAamorphous/PAtotal×100 (Eqn. A); wherein PAamorp=peak area of the first elution, and PAtotal #191=total peak area of the polymers of the olefin-based polymer composition.
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公开(公告)号:US20220389139A1
公开(公告)日:2022-12-08
申请号:US17773582
申请日:2020-12-17
Applicant: DOW GLOBAL TECHNOLOGIES LLC
Inventor: Gaoxiang Wu , Brian M. Habersberger , Johnathan E. DeLorbe , Thomas Wesley Karjala, Jr. , Yabin Sun , Rongjuan Cong
IPC: C08F210/16 , C08J5/18 , G01N30/14 , G01N30/86 , H01L31/048
Abstract: A composition comprising an ethylene/alpha-olefin interpolymer that comprises the following properties: a) a total unsaturation/1000C≥0.30; b) a molecular weight distribution (MWD)≤3.0; c) a TGIC broadness parameter B1/4≤8.0. A solution N polymerization process to prepare an ethylene/alpha-olefin/interpolymer, said process comprising polymerizing, in one reactor, at a reactor temperature ≥150° C., a reaction mixture comprising ethylene, an alpha-olefin, a solvent, and a metal complex as described herein. A method to determine the TGIC broadness parameter B1/x of a polymer composition comprising one or more olefin-based polymers.
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公开(公告)号:US11261544B2
公开(公告)日:2022-03-01
申请号:US16486521
申请日:2018-03-07
Applicant: Dow Global Technologies LLC
Inventor: Viraj Shah , Yijian Lin , Ronald Wevers , Rongjuan Cong , Mehmet Demirors
IPC: D01F6/30 , D04H1/56 , C08F210/16 , D01D5/34 , D01F8/06 , D04H1/4291 , D04H3/007 , D04H3/16
Abstract: An ethylene/alpha-olefin interpolymer suitable for use in fibers and nonwovens having a density of from 0.911 to 0.939 g/cc, a Brookfield viscosity of less than or equal to 50,000 cP, and a molecular weight distribution (Mw,cc/Mn,cc) of 1.8 to 3.5, and articles thereof.
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公开(公告)号:US11248075B2
公开(公告)日:2022-02-15
申请号:US16654973
申请日:2019-10-16
Applicant: Dow Global Technologies LLC
Inventor: Frank J. Cerk , Rongjuan Cong , Shrikant Dhodapkar , Selim Yalvac , Morgan M. Hughes , Timothy W. Gambrel , Yi Jin
IPC: C08F210/02 , C08F210/16 , C08F4/659 , C08F2/04
Abstract: The invention provides compositions, each comprising an ethylene/alpha-olefin interpolymer, which has a reduced level of a low density, low molecular weight oligomeric fraction, as indicated by an HCC value, as described herein, and reduced levels of inorganic content or lower Tm. The invention also provides processes for forming such interpolymers.
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公开(公告)号:US10450393B2
公开(公告)日:2019-10-22
申请号:US16405811
申请日:2019-05-07
Applicant: Dow Global Technologies LLC
Inventor: Frank J. Cerk , Rongjuan Cong , Shrikant Dhodapkar , Selim Yalvac , Morgan M. Hughes , Timothy W. Gambrel , Yi Jin
IPC: C08F210/16 , C08F4/659 , C08F2/04
Abstract: The invention provides compositions, each comprising an ethylene/alpha-olefin interpolymer, which has a reduced level of a low density, low molecular weight oligomeric fraction, as indicated by an HCC value, as described herein, and reduced levels of inorganic content or lower Tm. The invention also provides processes for forming such interpolymers.
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公开(公告)号:US20180172648A1
公开(公告)日:2018-06-21
申请号:US15738939
申请日:2016-08-24
Applicant: Dow Global Technologies LLC
Inventor: Rongjuan Cong , Albert Parrott , Cherry Hollis , Charles Michael Cheatham
Abstract: A temperature gradient chromatography, and apparatus for the same, said method comprising the following: a) dissolving a composition comprising at least one polymer in at least one solvent, to form a polymer solution; b) injecting at least a portion of the polymer solution onto a support material and wherein the support material has a CI from 0.70 to 1.50; c) cooling the support material at a rate greater than, or equal to, 0.2° C./min; d) increasing the temperature of the support material to elute at least some of the polymer; e) generating the chromatogram.
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