公开(公告)号：US4134929A

公开(公告)日：1979-01-16

申请号：US708158

申请日：1976-07-23

申请人： Diane M. Stoakley ,  John R. Dombroski

发明人： Diane M. Stoakley ,  John R. Dombroski

IPC分类号： A61K6/00 ,  C09J4/06 ,  C08L33/14

CPC分类号： C09J4/06

摘要： An adhesive composition comprising Components A, B and C as follows:A. a polymerizable monomeric allyl 2-cyanoacrylate containing portion comprising1. from about 75 to about 92 parts by weight of allyl 2-cyanoacrylate;2. from about 1 to about 12 parts by weight of a difunctional monomer diester of an acid from the group consisting of acrylic and methacrylic acid and an aromatic diol; and3. from about 3 to 20 parts by weight of a thickening agent selected from poly(methylacrylate-coacrylonitrile) polymers;B. from 0.1 to 3.0 weight percent based upon the weight of component A of a hydrophobic cyclic imino initiator selected from 2,4,6-tri(allyloxy)-S-triazine, tri(alkyloxy)-S-triazines having 1 to about 20 exocyclic carbon atoms, benzoxazole and substituted benzoxazoles; andC. an amount of an organic peroxide free radical providing compound sufficient to cause cross linking of the difunctional monomer diester with the allyl 2-cyanoacrylate.

摘要翻译： 包含如下组分A，B和C的粘合剂组合物：

公开(公告)号：US4136138A

公开(公告)日：1979-01-23

申请号：US708160

申请日：1976-07-23

申请人： John R. Dombroski ,  Diane M. Stoakley

发明人： John R. Dombroski ,  Diane M. Stoakley

IPC分类号： A61K6/00 ,  C09J4/00 ,  C08L33/14

CPC分类号： C09J4/00

摘要： An adhesive composition comprising Components A, B and C as follows:A. a polymerizable monomeric 2-cyanoacrylate containing portion comprising1. from 60 to 90 parts by weight of allyl 2-cyanoacrylate;2. from 3 to 25 parts by weight of an alkyl 2-cyanoacrylate having the formula ##STR1## wherein R is alkyl having 60 to 10 carbon atoms; 3. FROM 0.25 TO 5 PARTS BY WEIGHT OF A DIFUNCTIONAL MONOMER DIESTER OF AN ACID FROM THE GROUP CONSISTING OF ACRYLIC AND METHACRYLIC ACID AND AN AROMATIC DIOL; AND4. from 3 to 15 parts by weight of a 2-cyanoacrylate compatible polymeric thickener;B. from 0.05 to about 1.5 weight percent based upon the weight of component A of a cyclic imino initiator selected from 2,4,6-tri(allyloxy)-S-triazine, 2,4,6-tri(alkyloxy)-S-triazines having 1 to about 20 exocyclic carbon atoms, benzoxazole and substituted benzoxazoles; andC. an amount of an organic peroxide free radical providing compound sufficient to cause crosslinking of a difunctional monomer diester with the 2-cyanoacrylates.

公开(公告)号：US6019926A

公开(公告)日：2000-02-01

申请号：US26591

申请日：1998-02-20

申请人： Robin E. Southward ,  David W. Thompson ,  Anne K. St. Clair ,  Diane M. Stoakley

发明人： Robin E. Southward ,  David W. Thompson ,  Anne K. St. Clair ,  Diane M. Stoakley

IPC分类号： B29C41/24 ,  B29D11/00

CPC分类号： B29C41/24 ,  B29D11/00 ,  B29K2079/08 ,  Y10T428/24909

摘要： Self-metallizing, flexible polyimide films with highly reflective surfaces are prepared by an in situ self-metallization procedure involving thermally initiated reduction of polymer-soluble silver(I) complexes. Polyamic acid solutions are doped with silver(I) acetate and solubilizing agents. Thermally curing the silver(I)-doped resins leads to flexible, metallized films which have reflectivities as high as 100%, abrasion-resistant surfaces, thermal stability and, in some cases, electrical conductivity, rendering them useful for space applications.

摘要翻译： 具有高反射表面的自金属化柔性聚酰亚胺膜通过原位自金属化方法制备，其涉及聚合物可溶性银（I）络合物的热引发还原。 聚酰胺酸溶液用乙酸银（I）和增溶剂掺杂。 将I（I）掺杂的树脂热固化导致柔性的金属化膜，其反射率高达100％，耐磨损表面，热稳定性，并且在某些情况下导电性可使其适用于空间应用。

公开(公告)号：US5272248A

公开(公告)日：1993-12-21

申请号：US892058

申请日：1992-05-22

申请人： J. Richard Pratt ,  Terry L. St. Clair ,  Diane M. Stoakley ,  Harold D. Burks

发明人： J. Richard Pratt ,  Terry L. St. Clair ,  Diane M. Stoakley ,  Harold D. Burks

IPC分类号： C08G73/10 ,  C08K5/21 ,  C08K5/3415 ,  C08G69/26

CPC分类号： C08K5/21 ,  C08G73/1067 ,  C08K5/3415

摘要： A process for preparing polyamides having enhanced melt flow properties is described. The process consists of heating a mixture of a high molecular weight poly(amic acid) or polyimide with a low molecular weight amic acid or imide additive in the range of 0.05 to 15% by weight of additive. The polyimide powders so obtained show improved processability, as evidenced by lower melt viscosity by capillary rheometry. Likewise, films prepared from mixtures of polymers with additives show improved processability with earlier onset of stretching by TMA.

摘要翻译： 描述了一种制备具有增强的熔体流动性能的聚酰胺的方法。 该方法包括将高分子量聚（酰胺酸）或聚酰亚胺与低分子量酰胺酸添加剂的混合物加入0.05至15重量％的添加剂。 如此获得的聚酰亚胺粉末显示出改进的加工性能，如通过毛细管流变测定法的较低熔体粘度所证明的。 同样，由聚合物与添加剂的混合物制备的薄膜也显示改善的加工性能，并且通过TMA早期开始拉伸。

公开(公告)号：US5116939A

公开(公告)日：1992-05-26

申请号：US84064

申请日：1987-08-11

申请人： James C. Fletcher ,  J. Richard Pratt ,  Terry L. St. Clair ,  Diane M. Stoakley ,  Harold D. Burks

发明人： James C. Fletcher ,  J. Richard Pratt ,  Terry L. St. Clair ,  Diane M. Stoakley ,  Harold D. Burks

IPC分类号： C08G73/10 ,  C08K5/21 ,  C08K5/3415

CPC分类号： C08K5/21 ,  C08G73/1067 ,  C08K5/3415

摘要： A process for preparing polyimides having enhanced melt flow properties is described. The process consists of heating a mixture of a high molecular weight poly(amic acid) or polyimide with a low molecular weight amic acid or imide additive in the range of 0.05 to 15% by weight of additive. The polyimide powders so obtained show improved processability, as evidenced by lower melt viscosity by capillary rheometry. Likewise, films prepared from mixtures of polymers with additives show improved processability with earlier onset of stretching by TMA.

摘要翻译： 描述了制备具有增强的熔体流动性能的聚酰亚胺的方法。 该方法包括将高分子量聚（酰胺酸）或聚酰亚胺与低分子量酰胺酸添加剂的混合物加入0.05至15重量％的添加剂。 如此获得的聚酰亚胺粉末显示出改进的加工性能，如通过毛细管流变测定法的较低熔体粘度所证明的。 同样，由聚合物与添加剂的混合物制备的薄膜也显示改善的加工性能，并且通过TMA早期开始拉伸。

公开(公告)号：US08529825B2

公开(公告)日：2013-09-10

申请号：US12928128

申请日：2010-12-03

申请人： Sang-Hyon Chu ,  Sang H. Choi ,  Jae-Woo Kim ,  Yeonjoon Park ,  James R. Elliott ,  Glen C. King ,  Diane M. Stoakley

发明人： Sang-Hyon Chu ,  Sang H. Choi ,  Jae-Woo Kim ,  Yeonjoon Park ,  James R. Elliott ,  Glen C. King ,  Diane M. Stoakley

IPC分类号： B28B1/00

CPC分类号： B64B1/06 ,  B64B1/20 ,  B64B1/30 ,  B64C2201/022 ,  B64C2201/042 ,  B64C2201/122 ,  B64C2201/125 ,  B64C2201/127 ,  H01L35/16 ,  H01L35/22 ,  H01L35/26

摘要： A new fabrication method for nanovoids-imbedded bismuth telluride (Bi—Te) material with low dimensional (quantum-dots, quantum-wires, or quantum-wells) structure was conceived during the development of advanced thermoelectric (TE) materials. Bismuth telluride is currently the best-known candidate material for solid-state TE cooling devices because it possesses the highest TE figure of merit at room temperature. The innovative process described here allows nanometer-scale voids to be incorporated in Bi—Te material. The final nanovoid structure such as void size, size distribution, void location, etc. can be also controlled under various process conditions.

摘要翻译： 在先进的热电（TE）材料的开发中，设计了一种新型的纳米复合碲化铋（Bi-Te）材料，具有低维（量子点，量子线或量子阱）结构。 碲化铋目前是固态TE冷却装置最有名的候选材料，因为它在室温下具有最高的TE品质因数。 这里描述的创新工艺允许将纳米尺度的空隙纳入Bi-Te材料。 最终的纳米结构如空隙尺寸，尺寸分布，空隙位置等也可以在各种工艺条件下进行控制。

公开(公告)号：US4864865A

公开(公告)日：1989-09-12

申请号：US267146

申请日：1988-11-04

申请人： Diane M. Stoakley ,  Anne K. St. Clair ,  Bruce D. Little

发明人： Diane M. Stoakley ,  Anne K. St. Clair ,  Bruce D. Little

IPC分类号： G01N3/04

CPC分类号： G01N3/04 ,  G01N2203/0017 ,  G01N2203/0222 ,  G01N2203/0405

摘要： A set of film clamps and a mounting block for use in the determination of tensile modulus and damping properties of films in a manually operated or automated Rheovibron. These clamps and mounting block provide uniformity of sample gripping and alignment in the instrument. Operator dependence and data variability are greatly reduced.

摘要翻译： 一组胶片夹具和用于确定手动操作或自动化Rheovibron中膜的拉伸模量和阻尼性能的安装块。 这些夹具和安装块提供了仪器中样品夹持和对准的均匀性。 操作员依赖和数据变异性大大降低。

公开(公告)号：US5520960A

公开(公告)日：1996-05-28

申请号：US286032

申请日：1994-08-03

申请人： James D. Rancourt ,  Diane M. Stoakley ,  Maggie L. Caplan ,  Anne K. St. Clair ,  Larry T. Taylor

发明人： James D. Rancourt ,  Diane M. Stoakley ,  Maggie L. Caplan ,  Anne K. St. Clair ,  Larry T. Taylor

IPC分类号： C09D179/08 ,  H01B1/12 ,  B05D3/02 ,  B05D5/12

CPC分类号： H01B1/128 ,  C09D179/08

摘要： Polyimides with enhanced electrical conductivity are produced by adding a silver ion-containing additive to the polyamic acid resin formed by the condensation of an aromatic dianhydride with an aromatic diamine. After thermal treatment the resulting polyimides had surface conductivities in the range of 1.7.times.10.sup.-3 4.5 .OMEGA..sup.-1 making them useful in low the electronics industry as flexible, electrically conductive polymeric films and coatings.

摘要翻译： 通过向通过芳族二酐与芳族二胺的缩合形成的聚酰胺酸树脂中加入含有银离子的添加​​剂来生产具有增强的导电性的聚酰亚胺。 热处理后，得到的聚酰亚胺的表面电导率在1.7×10 -3 4.5欧米加-1范围内，使得它们在电子工业中用作柔性导电聚合物膜和涂层。

公开(公告)号：US5376209A

公开(公告)日：1994-12-27

申请号：US141430

申请日：1993-10-20

申请人： Diane M. Stoakley ,  Anne K. St. Clair

发明人： Diane M. Stoakley ,  Anne K. St. Clair

IPC分类号： C08G73/10 ,  C08J5/12 ,  C09J5/00 ,  H05K1/03 ,  B05D1/00

CPC分类号： C08J5/124 ,  C08G73/1039 ,  C09J5/00 ,  H05K1/0346 ,  C08J2379/08 ,  H05K1/0373 ,  Y10T156/10

摘要： An assembly of an article and a polyimide composition is prepared. The assembly resists dimensional change, delamination, or debonding when exposed to changes in temperature. An article is provided. A polyamic acid solution which yields a polyimide having a low coefficient of thermal expansion (CTE) was prepared. Equimolar quantities of an aromatic diamine and an aromatic dianhydride were reacted in a solvent medium to form a polyamic acid solution. A metal ion-containing additive was added to the solution. Examples of this additive are: TbCl.sub.3, DyCl.sub.3, ErCl.sub.3, TmCl.sub.3, Al(C.sub.5 H.sub.7 O.sub.2).sub.3, and Er.sub.2 S.sub.3. The polyamic acid solution was imidized and is combined with the article to form the assembly.

摘要翻译： 制备制品和聚酰亚胺组合物的组合物。 当暴露于温度变化时，组件抵抗尺寸变化，分层或剥离。 提供了一篇文章。 制备具有低热膨胀系数（CTE）的聚酰亚胺的聚酰胺酸溶液。 将等摩尔量的芳族二胺和芳族二酐在溶剂介质中反应形成聚酰胺酸溶液。 向溶液中加入含金属离子的添加​​剂。 该添加剂的实例是：TbCl 3，DyCl 3，ErCl 3，TmCl 3，Al（C 5 H 7 O 2）3和Er 2 S 3。 将聚酰胺酸溶液酰亚胺化并与制品组合以形成组件。

公开(公告)号：US4895972A

公开(公告)日：1990-01-23

申请号：US239259

申请日：1988-09-01

申请人： Diane M. Stoakley ,  Anne K. St. Clair

发明人： Diane M. Stoakley ,  Anne K. St. Clair

IPC分类号： B05D7/24 ,  C08G73/10 ,  C08J5/18 ,  C09D179/08 ,  H01B3/30 ,  H01L21/312

CPC分类号： C08G73/1067 ,  C08G73/1007 ,  C08G73/1039 ,  C08G73/1046 ,  C08G73/1064 ,  C08G73/1071 ,  H01B3/306

摘要： Linear aromatic polyimides with low dielectric constants are produced by adding a diamic acid additive to the polyamic acid resin formed by the condensation of an aromatic dianhydride with an aromatic diamine. The resulting modified polyimide is a better electrical insulator than state-of-the-art commercially available polyimides.

摘要翻译： 通过将芳族二酸酐与芳族二胺的缩合形成的聚酰胺酸树脂中加入二胺酸添加剂来制备具有低介电常数的线性芳族聚酰亚胺。 所得到的改性聚酰亚胺是比现有技术的市售聚酰亚胺更好的电绝缘体。