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公开(公告)号：US5455369A
公开(公告)日：1995-10-03
申请号：US348524
申请日：1994-12-02
IPC分类号： C07C253/30 , C07C255/23
CPC分类号： C07C255/23 , C07C253/30
摘要： A process for preparing methyl .alpha.-cyanoacrylate in which methyl cyanoacetate is reacted with formaldehyde to form a polymer, which is subsequently depolymerized to the monomeric product, comprises using an ester of poly(ethylene glycol) as the solvent for the polymerization and depolymerization reactions.
摘要翻译： 一种制备α-氰基丙烯酸甲酯的方法，其中氰基乙酸甲酯与甲醛反应形成聚合物，随后解聚成单体产物，包括使用聚（乙二醇）酯作为聚合和解聚反应的溶剂。
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公开(公告)号：US4268656A
公开(公告)日：1981-05-19
申请号：US112496
申请日：1980-01-16
CPC分类号： C08G59/4021 , C08G59/184 , C08G59/4035 , C08G59/5073
摘要： A N-substituted piperazine or N-substituted homopiperazine adduct with a polyepoxide is used as a co-curing agent in epoxy resin systems containing a polyepoxide and a known curing agent such as dicyandiamide, a carboxylic acid anhydride, or a dihydrazide. The preferred adducts have a ratio of epoxy groups to secondary amino groups of between 1.2:1 and 3:1. The preferred polyepoxides are polyglycidyl ethers of 4,4'-isopropylidenediphenol (bisphenol A). Suitable adducts are prepared from N-methyl-, N-(2-hydroxyethyl)-, N-octyl-, N-phenyl- and N-benzyl piperazine and N-methyl homopiperazine.
摘要翻译： 在包含聚环氧化物和已知的固化剂如双氰胺，羧酸酐或二酰肼的环氧树脂体系中，使用N-取代的哌嗪或N-取代的高聚哌嗪与多环氧化物的加合物作为共固化剂。 优选的加合物具有1.2:1至3:1之间的环氧基与仲氨基的比率。 优选的聚环氧化物是4,4'-异丙基二苯酚（双酚A）的聚缩水甘油醚。 合适的加合物由N-甲基 - ，N-（2-羟乙基） - ，N-辛基 - ，N-苯基 - 和N-苄基哌嗪和N-甲基高哌嗪制备。
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公开(公告)号：US4125494A
公开(公告)日：1978-11-14
申请号：US823981
申请日：1977-08-12
CPC分类号： C07C255/00 , C09J4/00
摘要： Improved 2-cyanoacrylate adhesive compositions containing acetic acid exhibit greatly enhanced bond strength with no significant reduction in cure rate. Such compositions may be used on a wide variety of substrates and are particularly useful on metals.
摘要翻译： 包含乙酸的改进的2-氰基丙烯酸酯粘合剂组合物显示出极大的增强的粘合强度，而没有明显的固化速率降低。 这样的组合物可以用于各种各样的基底上，并且特别适用于金属。
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4.发明授权Hot-melt adhesives based on vinyl polymer and process for adhering surfaces therewith 失效基于乙烯基聚合物的热熔粘合剂和用于粘合表面的工艺
公开(公告)号：US4588767A
公开(公告)日：1986-05-13
申请号：US737647
申请日：1985-05-24
IPC分类号： A61L15/58 , C08F220/12 , C09J133/08 , C08F210/14
CPC分类号： C09J133/08 , A61L15/58 , C08F220/12 , C09J2201/61
摘要： A hot-melt adhesive especially useful in the construction of disposable diapers contains a vinyl polymer of 40-90% by weight of a C.sub.1 -C.sub.12 alkyl acrylate and 10-60% by weight of an alpha-olefin of C.sub.20 -C.sub.40, wherein the alkyl acrylate may be partially replaced with vinyl acetate or with a C.sub.6 -C.sub.12 olefin or with mixtures thereof, provided that the polymer contain at least 10% by weight of the alkyl acrylate. The adhesive may also contain a tackifying resin, a wax, an oil or a stabilizer depending on the specific end-use desired. In a preferred embodiment the polymer contains 20-45% by weight of the alpha-olefin.
摘要翻译： 特别可用于一次性尿布结构的热熔粘合剂包含40-90重量％的丙烯酸C1-C12烷基酯和10-60重量％的C20-C40的α-烯烃的乙烯基聚合物，其中 丙烯酸烷基酯可以用乙酸乙烯酯或与C 6 -C 12烯烃或其混合物部分替代，条件是聚合物含有至少10重量％的丙烯酸烷基酯。 粘合剂还可以含有增粘树脂，蜡，油或稳定剂，这取决于所需的特定最终用途。 在优选的实施方案中，聚合物含有20-45重量％的α-烯烃。
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5.发明授权Copolyesters, method of manufacturing same, and hot melt adhesive compositions incorporating same 失效共聚酯，其制造方法，以及加入其的热熔粘合剂组合物
公开(公告)号：US3975323A
公开(公告)日：1976-08-17
申请号：US542692
申请日：1975-01-21
IPC分类号： C08G63/00 , C08G63/08 , C08G63/16 , C08G63/181 , C08G63/52 , C08G63/60 , C09J167/00 , C08L91/00
摘要： A copolyester is formed of at least one symmetrical aromatic dicarboxylic acid member, at least one dimer acid, and at least one C.sub.2 --C.sub.10 glycol, and at least one polyester polyol member. The polyester polyol member is either a polycaprolactone polyol having a molecular weight of 500-5,000, or a mixture of a polycaprolactone diol having a molecular weight of 300-5,000 and a nonpolymeric polyol. The resultant thermoplastic copolyester has a glass transition temperature of less than 25.degree.C and a polymer melting temperature greater than 70.degree.C, and is useful both as a hot melt adhesive by itself and as an ingredient of both pressure sensitive and non-pressure sensitive hot melt adhesive formulations. In producing the copolyester, an intermediate copolyester of the symmetrical aromatic dicarboxylic acid member, the dimer acid, and the glycol is chain extended by reaction with the polyester polyol member in a 2-6 hour reaction at about 225.degree.-270.degree.C under a vacuum of about 1-30 mm. Hg. pressure.
摘要翻译： 共聚酯由至少一种对称的芳族二羧酸构件，至少一种二聚酸和至少一种C 2 -C 10二元醇和至少一种聚酯多元醇构件形成。 聚酯多元醇构件是分子量为500-5,000的聚己内酯多元醇或分子量为300-5,000的聚己内酯二醇和非聚合多元醇的混合物。 所得的热塑性共聚酯的玻璃化转变温度低于25℃，聚合物熔融温度大于70℃，并且作为热熔粘合剂本身可用作压敏和非压敏成分 热熔胶配方。 在共聚酯的制造中，对称的芳族二羧酸成
分，二聚酸和二醇的中间共聚酯在约225-270℃的2-6小时反应中，与聚酯多元醇成
分反应，在 真空度约1-30毫米。 汞。 压力。-
公开(公告)号：US4535140A
公开(公告)日：1985-08-13
申请号：US284162
申请日：1981-07-17
IPC分类号： A61L15/58 , C08F220/12 , C09J133/08 , C08F210/14
CPC分类号： C09J133/08 , A61L15/58 , C08F220/12 , C09J2201/61
摘要： A hot-melt adhesive especially useful in the construction of disposable diapers contains a vinyl polymer of 40-90% by weight of a C.sub.1 -C.sub.12 alkyl acrylate and 10-60% by weight of an alpha-olefin of C.sub.20 -C.sub.40, wherein the alkyl acrylate may be partially replaced with vinyl acetate or with a C.sub.6 -C.sub.12 olefin or with mixtures thereof, provided that the polymer contain at least 10% by weight of the alkyl acrylate. The adhesive may also contain a tackifying resin, a wax, an oil or a stabilizer depending on the specific end-use desired. In a preferred embodiment the polymer contains 20-45% by weight of the alpha-olefin.
摘要翻译： 特别可用于一次性尿布结构的热熔粘合剂包含40-90重量％的丙烯酸C1-C12烷基酯和10-60重量％的C20-C40的α-烯烃的乙烯基聚合物，其中 丙烯酸烷基酯可以用乙酸乙烯酯或与C 6 -C 12烯烃或其混合物部分替代，条件是聚合物含有至少10重量％的丙烯酸烷基酯。 粘合剂还可以含有增粘树脂，蜡，油或稳定剂，这取决于所需的特定最终用途。 在优选的实施方案中，聚合物含有20-45重量％的α-烯烃。
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公开(公告)号：US3944428A
公开(公告)日：1976-03-16
申请号：US555934
申请日：1975-03-06
CPC分类号： D21H27/40 , C08G6/02 , C09J103/02 , Y10T428/24711
摘要： Starch-based alkaline curing corrugating adhesives, containing a novel crosslinking additive comprising acetoacetamide-formaldehyde condensate, are useful in the manufacture of corrugated paperboard. These adhesives are characterized by their excellent stability with respect to viscosity, their long pot life and their ability to form water-resistant bonds, particularly after aging.
摘要翻译： 含有乙酰乙酰胺 - 甲醛缩合物的新型交联添加剂的基于淀粉的碱性固化波纹粘合剂可用于制造瓦楞纸板。 这些粘合剂的特征在于它们在粘度方面的优异的稳定性，它们的长使用期和形成耐水键的能力，特别是在老化之后。
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公开(公告)号：US4215209A
公开(公告)日：1980-07-29
申请号：US50988
申请日：1979-06-22
CPC分类号： C09J4/00
摘要： Improved storage-stable anaerobic curing adhesive compositions useful as anaerobic adhesives and sealants are prepared by first mixing a polymerizable acrylate ester monomer, an inhibitor for free radical polymerization, a chelator, and at least an effective amount of an accelerator system consisting of an N-substituted sulfonamide and an aromatic tertiary amine. The resultant homogeneous mixture is thereafter maintained at a temperature of at least about 20.degree. C. for a period of time sufficient to provide the composition with anaerobic curing properties and a specified minimum amount of active oxygen. In one embodiment, the mixture is stirred at a temperature of 45.degree.-80.degree. C. for 10-30 hours. In another embodiment, the mixture is maintained at an elevated temperature without stirring.
摘要翻译： 通过首先混合可聚合的丙烯酸酯单体，用于自由基聚合的抑制剂，螯合剂和至少一种有效量的由N-甲基吗啉组成的促进剂体系，制备用作厌氧粘合剂和密封剂的改进的储存稳定的厌氧固化粘合剂组合物， 取代磺酰胺和芳族叔胺。 然后将所得的均匀混合物保持在至少约20℃的温度下足以使组合物具有厌氧固化性能和规定的最小量的活性氧的时间。 在一个实施方案中，将混合物在45-80℃的温度下搅拌10-30小时。 在另一个实施方案中，将混合物保持在升高的温度下而不搅拌。
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公开(公告)号：US4510324A
公开(公告)日：1985-04-09
申请号：US489665
申请日：1983-04-28
IPC分类号： C08F12/30 , C09J4/00 , G03C1/053 , C07C143/78
摘要： The invention provides disulfonimide compounds of the general formula ##STR1## wherein X is bromine, chlorine or iodine; R is hydrogen or methyl; and R' is alkyl, aryl or substituted aryl. The compounds are useful as activators for anaerobic adhesive compositions and also as intermediates in the preparation of monomers of the general formula ##STR2## wherein R and R' are as defined above. The monomers are polymerizable to form homo- and copolymers useful in the photographic industry as well as in formulating anaerobic adhesive compositions.
摘要翻译： 本发明提供了通式“IMAGE”的二磺酰亚胺化合物，其中X是溴，氯或碘; R是氢或甲基; 和R'是烷基，芳基或取代的芳基。 这些化合物可用作厌氧粘合剂组合物的活化剂，也可用作制备通式“IMAGE”的单体的中间体，其中R和R'如上所定义。 单体可聚合以形成可用于照相工业以及配制厌氧粘合剂组合物的均聚物和共聚物。
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10.发明授权Electrophotographic coating compositions having bromine-containing polymer binders 失效具有含溴聚合物粘合剂的电子照相涂料组合物
公开(公告)号：US3932181A
公开(公告)日：1976-01-13
申请号：US484758
申请日：1974-07-01
CPC分类号： G03G5/082 , G03G5/0589
摘要： Photoconductive coating compositions for application to solid substrates which are to be utilized in electrophotographic operations are described; the resultant photoconductive coatings comprise a layer of photoconductive pigment particles bonded to themselves and to the solid substrate with a binder comprising a novel interpolymer, at least one of whose constituent monomers contains bromine. Novel bromine-containing monomers are also disclosed.
摘要翻译： 描述了用于在电照相操作中使用的用于固体基质的光导涂料组合物; 所得到的光导涂层包含一层光导电颜料颗粒，它们与粘合剂本身和固体基质一起使用含有新型互聚物的粘合剂，其中至少一种构成单体含有溴。 还公开了新的含溴单体。
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