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1.发明授权Process for the production of oligoglycerol mixtures of increased diglycerol content 失效制备增加二甘油含量的低聚甘油混合物的方法
公开(公告)号：US5349094A
公开(公告)日：1994-09-20
申请号：US898061
申请日：1992-06-12
IPC分类号： B01J29/08 , B01J29/18 , B01J29/60 , B01J29/70 , C07B61/00 , C07C41/09 , C07C43/13 , C08G65/34
摘要： Oligoglycerol mixtures having a high diglycerol content are prepared by a process in which glycerol is condensed in the presence of zeolites corresponding to formula (I)M.sub.2/z O * Al.sub.2 O.sub.3 * x SIO.sub.2 * y H.sub.2 O (I)in which M is an alkali metal or alkaline earth metal having a valency of z, x is a number of 1.8 to 12 and y is a number of 0 to 8. The water of condensation which is formed during the reaction, is continuously removed from the reaction mixture and the reaction is terminated when the quantity of water theoretically necessary for the formation of diglycerol has been separated.
摘要翻译： 具有高二甘油含量的低聚甘油混合物通过其中甘油在对应于式（I）M2 / zO * Al 2 O 3 * x SIO 2 * y H 2 O（I）的沸石存在下缩合的方法制备，其中M是碱金属或 碱土金属的化合价为z，x为1.8〜12，y为0〜8的数。反应中形成的缩合水从反应混合物中连续除去，反应结束 当理想上形成双甘油所需的水量已被分离时。
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公开(公告)号：US4636571A
公开(公告)日：1987-01-13
申请号：US726220
申请日：1985-04-23
IPC分类号： C07D307/30 , C07D307/02
CPC分类号： C07D307/30
摘要： 2,3-Dihydrofurans having highly desirable odor characteristics closely mimicking that of natural products are provided herein. The 2,3-dihydrofurans correspond to the formula ##STR1## wherein R' is an alkyl group having from 1 to 4 carbon atoms, R** is an alkyl group having from 1 to 5 carbon atoms, R.sub.1 is an alkyl group having from 1 to 4 carbon atoms, R.sub.2 is hydrogen or an alkyl group having from 1 to 6 carbon atoms, and R.sub.3 and R.sub.4 are hydrogen or a methyl group. The 2,3-dihydrofuran compounds are useful in the preparation of fragrance compositions and fragranced articles and can be employed in conjunction with known fragrance materials to augment or enhance the aromas thereof.
摘要翻译： 本文提供了具有与天然产物密切相似的非常理想的气味特征的2,3-二氢呋喃。 2,3-二氢呋喃对应于式“IMAGE”，其中R'是具有1至4个碳原子的烷基，R **是具有1至5个碳原子的烷基，R 1是具有 1至4个碳原子，R 2是氢或具有1至6个碳原子的烷基，R 3和R 4是氢或甲基。 2,3-二氢呋喃化合物可用于制备香料组合物和香料制品，并且可以与已知的香料材料结合使用以增强或增强其香味。
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3.发明授权
公开(公告)号：US4594434A
公开(公告)日：1986-06-10
申请号：US668597
申请日：1984-11-05
IPC分类号： C07D313/00 , C07D321/00 , C07D323/00 , C07D327/00 , C07D327/02 , C08G63/16 , C08G63/82 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07D313/00 , C07D321/00 , C07D323/00 , C07D327/00 , C07D327/02 , C08G63/16 , C08G63/82 , C11B9/0084
摘要： Dawsonite is a highly effective and useful catalyst for the thermal depolymerization of polyesters to produce macrocyclic compounds. High yields and enhanced rates of reaction are obtained using Dawsonite obtained from natural or synthetic sources.
摘要翻译： 片钠铝石是一种高效有效的催化剂，用于聚酯热解聚合产生大环化合物。 使用从天然或合成来源得到的片钠铝石可以获得高产率和提高的反应速率。
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公开(公告)号：US4536349A
公开(公告)日：1985-08-20
申请号：US426527
申请日：1982-09-29
申请人： Eugene G. Harris
发明人： Eugene G. Harris
CPC分类号： C07D307/42 , A23L27/2052
摘要： Furan derivatives, useful as fragrances, having the formula ##STR1## wherein R is alkyl or alkenyl and R.sub.1 is alkyl, alkenyl, cycloalkyl, cycloalkenyl or aryl.
摘要翻译： 呋喃衍生物，可用作香料，具有式“IMAGE”，其中R是烷基或烯基，R 1是烷基，烯基，环烷基，环烯基或芳基。
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公开(公告)号：US4252739A
公开(公告)日：1981-02-24
申请号：US68135
申请日：1979-08-20
IPC分类号： B01J31/02 , B01J31/16 , B01J31/26 , C07B37/10 , C07C45/68 , C07C49/533 , C07C49/563 , C07C67/333 , C07C69/743 , C07C255/45 , C07C103/19 , C07C121/48
CPC分类号： B01J31/0239 , B01J31/0268 , B01J31/26 , C07C255/00
摘要： This invention provides a convenient and commercially adaptable process for the preparation of vinylcyclopropane derivatives in high yields. The process involves reacting an alkylating agent and an activated methylene compound in the presence of an onium compound, an alkali metal compound and water, which while only necessary in trace amounts can be present in substantial quantities.
摘要翻译： 本发明提供了以高产率制备乙烯基环丙烷衍生物的方便和商业上适应性的方法。 该方法包括在鎓化合物，碱金属化合物和水的存在下使烷基化试剂和活化的亚甲基化合物反应，其中必要时可以大量存在痕量。
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公开(公告)号：US4980342A
公开(公告)日：1990-12-25
申请号：US402105
申请日：1989-09-01
申请人： Louis Rebrovic , Eugene G. Harris
发明人： Louis Rebrovic , Eugene G. Harris
IPC分类号： A61K8/49 , A61Q13/00 , B01J23/40 , B01J23/755 , C07B61/00 , C07D307/33 , C07D309/30 , C07D315/00 , C11B9/00
CPC分类号： C07D307/33 , C07D309/30 , C07D315/00
摘要： A convenient process for the preparation of .gamma.-alkyl-substituted-.gamma.-butyrolactones and .delta.-valerolactones is provided. The process involves forming the .alpha.-alkylidene lactone by reacting essentially equimolar amounts of an .alpha.-acyl lactone, an aldehyde, and an alkali metal hydroxide in an inert diluent at an elevated temperature while removing water and hydrogenating the .alpha.-alkylidene lactone to obtain the corresponding .alpha.-alkyl lactone.
摘要翻译： 提供了制备γ-烷基取代的γ-丁内酯和δ-戊内酯的方便的方法。 该方法包括通过在惰性稀释剂中在升高的温度下使基本上等摩尔量的α-酰基内酯，醛和碱金属氢氧化物反应形成α-亚烷基内酯，同时除去水并氢化α-亚烷基内酯，得到 相应的α-烷基内酯。
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7.发明授权4-alkylphenyl-2-alkoxyethyl ethers and fragrance compositions containing same 失效4-烷基苯基-2-烷氧基乙基醚和含有它们的香料组合物
公开(公告)号：US4716146A
公开(公告)日：1987-12-29
申请号：US944143
申请日：1986-12-19
申请人： Eugene G. Harris
发明人： Eugene G. Harris
IPC分类号： C07C43/205 , C11B9/02 , A61K7/46 , C07C43/20 , C11B9/00
CPC分类号： C07C43/2055 , C11B9/02
摘要： This invention relates to compounds of the general structure ##STR1## wherein R and R.sup.1 are lower alkyl having from 1 to 2 carbon atoms useful as fragrance additives and to the fragrance compositions containing the same.
摘要翻译： 本发明涉及通用结构化合物（IMAGE），其中R和R 1是可用作香料添加剂的具有1至2个碳原子的低级烷基酯和含有它们的香料组合物。
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公开(公告)号：US4681703A
公开(公告)日：1987-07-21
申请号：US870594
申请日：1986-06-04
IPC分类号： C07D307/30 , C07D307/02
CPC分类号： C07D307/30
摘要： Fragranced compositions and fragranced articles containing an aroma-augmenting or aroma-enhancing amount of a 2,3-dihydrofuran corresponding to the formula ##STR1## wherein R' is an alkyl group having from 1 to 4 carbon atoms, R** is an alkyl group having from 1 to 5 carbon atoms, R.sub.1 is an alkyl group having from 1 to 4 carbon atoms, R.sub.2 is hydrogen or an alkyl group having from 1 to 6 carbon atoms, and R.sub.3 and R.sub.4 are hydrogen or a methyl group, and a process for obtaining same are provided.
摘要翻译： 含有对应于式“IMAGE”的芳香增强或芳香增强量的2,3-二氢呋喃的芳香组合物和芳香物品，其中R'是具有1至4个碳原子的烷基，R **是烷基 具有1至5个碳原子的基团，R 1是具有1至4个碳原子的烷基，R 2是氢或具有1至6个碳原子的烷基，并且R 3和R 4是氢或甲基，和 提供了获得相同的方法。
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公开(公告)号：US4661285A
公开(公告)日：1987-04-28
申请号：US860268
申请日：1986-05-05
IPC分类号： A61L9/01 , C07C69/608 , C07C69/635 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0003
摘要： Balsamic fragrance compositions having fruity, fir needle notes with the character of fir balsam absolute are produced by reacting camphene, and ethylhaloacetate and di-t-butyl peroxide; reacting the mixture obtained therefrom with zinc and water; vacuum distilling the resulting product; and collecting a specified fraction.
摘要翻译： 通过使camp烯和卤代乙酸乙酯和二叔丁基过氧化物反应生成具有果实，冷杉针刺的苦味香味组合物，具有冷杉苦涩苦涩的特征。 使得到的混合物与锌和水反应; 真空蒸馏得到的产品; 并收集指定的分数。
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公开(公告)号：US5898086A
公开(公告)日：1999-04-27
申请号：US820520
申请日：1997-03-19
申请人： Eugene G. Harris
发明人： Eugene G. Harris
CPC分类号： C07C41/01
摘要： A process for making alkyl ether glycerols involving: (a) providing a feedstock component having at least one terminal hydroxyl group selected from the group consisting of glycerides and polyols; (b) providing a heavy metal catalyst; and (c) contacting the feedstock component with the heavy metal catalyst.
摘要翻译： 一种制备烷基醚甘油的方法，包括：（a）提供具有至少一个选自甘油酯和多元醇的末端羟基的原料组分; （b）提供重金属催化剂; 和（c）使原料组分与重金属催化剂接触。
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