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1.发明授权Method of making an article having a layer of a nickel-phosphorus alloy and coated with a protective layer 失效制造具有镍 - 磷合金层并涂覆有保护层的制品的方法
公开(公告)号：US4545871A
公开(公告)日：1985-10-08
申请号：US667936
申请日：1984-11-02
CPC分类号： C25D11/36 , C25D11/38 , Y10S126/908 , Y10S428/926 , Y10S428/936 , Y10T428/12583 , Y10T428/1259 , Y10T428/12847 , Y10T428/12937 , Y10T428/12944 , Y10T428/261 , Y10T428/31678
摘要： An article which is covered with a nickel-phosphorus alloy is covered on its outer surface with a protective layer which comprises CrPO.sub.4, Cr(OH).sub.3 and may also comprise Cr.sub.2 (SO.sub.4).sub.3 and in which no nickel is present. The layer provides excellent corrosion protection. In a particular embodiment the layer is black, scratch-resistant in normal use, cannot be wiped off and is not sensitive to finger prints and is extremely suitable for decorative applications. The layers can be obtained electrolytically in a bath which comprises chromic acid and optionally phosphoric acid and sulfuric acid using reversed current in a given frequency range, a given range of current densities and a given range of ratios of cathodic to anodic pulse durations. In order to obtain the black layers the cathodic time duration is only a fraction of the anodic time duration.
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2.发明授权Metal article layered with a nickel-phosphorus alloy and a protective coating 失效用镍 - 磷合金层压的金属制品和保护涂层
公开(公告)号：US4497877A
公开(公告)日：1985-02-05
申请号：US491101
申请日：1983-05-03
CPC分类号： C25D11/36 , C25D11/38 , Y10S126/908 , Y10S428/926 , Y10S428/936 , Y10T428/12583 , Y10T428/1259 , Y10T428/12847 , Y10T428/12937 , Y10T428/12944 , Y10T428/261 , Y10T428/31678
摘要： A metal article which covered with a nickel-phosphorus alloy and which is covered on its outer surface with a protective layer which comprises CrPO.sub.4, Cr(OH).sub.3 and may also comprise Cr.sub.2 (SO.sub.4).sub.3 and in which no nickel is present. The layer provides an excellent corrosion protection. In a particular embodiment the layer is black, scratch-resistant in normal use, cannot be wiped off and is not sensitive to finger prints and is extremely suitable for decorative applications. The layers can be obtained electrolytically in a bath which comprises chromic acid and optionally reversed current in a given frequency range, a given range of current densities and a given range of ratios of cathodic to anodic pulse durations. In order to obtain the black layers the cathodic time duration is only a fraction of black layers the anodic time duration.
摘要翻译： 覆盖有镍 - 磷合金并且在其外表面上覆盖有包含CrPO 4，Cr（OH）3并且还可以包含Cr 2（SO 4）3并且其中不存在镍的保护层的金属制品。 该层提供了极好的防腐蚀性能。 在一个具体实施方案中，该层是黑色的，在正常使用中是耐刮擦的，不能被擦除并且对指纹不敏感，并且非常适用于装饰性应用。 这些层可以在包含铬酸和在给定频率范围内的给定范围的电流密度的给定范围以及阴极与阳极脉冲持续时间的给定范围的范围内的电镀中电解获得。 为了获得黑色层，阴极持续时间只是黑色层的一部分阳极时间。
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公开(公告)号：US4273625A
公开(公告)日：1981-06-16
申请号：US178045
申请日：1980-08-14
摘要： Treating objects of which at least the surface consists of tin in order to obtain a satisfactory corrosion resistance. To this end the objects are subjected in a tungstate solution of at least 0.02 M and having a pH of 4-11 alternately to a cathodic and an anodic polarity (so-called periodically reversed current). The frequency with which the current reverses must be between 0.2 and 2 Hz and the current density must be between 0.2 and 1 A/dm.sup.2, the ratio of the anodic to the cathodic density being from 0.5-1.
摘要翻译： 处理至少表面由锡组成的物体，以获得令人满意的耐腐蚀性。 为此，将物体在至少0.02M的钨酸盐溶液中交替地具有4-11的pH值至阴极和阳极极性（所谓的周期性反转电流）。 电流反转的频率必须在0.2和2Hz之间，电流密度必须在0.2和1A / dm2之间，阳极与阴极密度的比例为0.5-1。
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公开(公告)号：US4610933A
公开(公告)日：1986-09-09
申请号：US705758
申请日：1985-02-25
IPC分类号： C03B11/00 , B29C33/56 , B29D17/00 , C25D1/10 , G02B3/00 , G02B5/00 , G02B5/08 , G11B3/68 , G11B3/70
CPC分类号： B29D17/005 , B29C33/56 , G11B3/685 , B29L2011/00 , Y10T428/12576 , Y10T428/12993
摘要： A master suitable for the manufacture of electroplated negative metal copies. The master comprises a preform which on at least one side has a layer of electroplated aluminum. The surface has a precisely machined profile and is coated with a titanium nitride layer.
摘要翻译： 适用于制造电镀负极金属副本的主机。 主机包括在至少一侧上具有电镀铝层的预成型件。 表面具有精确加工的轮廓并且涂覆有氮化钛层。
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5.发明授权Optically readable information disc provided with a reflective optical structure 失效具有反射光学结构的光学可读信息盘
公开(公告)号：US4509161A
公开(公告)日：1985-04-02
申请号：US378570
申请日：1982-05-17
CPC分类号： G11B7/243 , G11B7/258 , Y10S430/146
摘要： An optically readable information disc having a reflective optical structure which comprises a reflective layer which is composed of a nitride, carbide or boride of a transition metal selected from the group consisting of titanium, zirconium, hafnium, vanadium, chromium, niobium, molybdenum, lanthanum, tantalum and tungsten.
摘要翻译： 一种具有反射光学结构的光学可读信息盘，其包括由选自钛，锆，铪，钒，铬，铌，钼，镧的过渡金属的氮化物，碳化物或硼化物构成的反射层 ，钽和钨。
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公开(公告)号：US4693769A
公开(公告)日：1987-09-15
申请号：US725868
申请日：1985-04-22
CPC分类号： B29C66/4724 , B29C45/00 , B29C65/08 , G09F7/16 , B29C2045/0041 , B29C2045/0086 , B29C66/73921 , Y10T156/108 , Y10T428/24736
摘要： The invention provides a method by means of which it becomes possible to produce emblems or wordmarks having three-dimensional symbols, both the front face and the raised side faces of which are metallized, while the substrate is not metallized. For that purpose, the symbols are injection molded with a carrier and they are not secured to a separately manufactured substrate until after the metallizing operation.
摘要翻译： 本发明提供了一种方法，通过该方法，可以产生具有三维符号的标志或符号，其前表面和凸起侧面均被金属化，同时基板未金属化。 为了这个目的，符号用载体注射成型，并且它们不固定到单独制造的基板上，直到金属化操作之后。
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7.发明授权
公开(公告)号：US5509958A
公开(公告)日：1996-04-23
申请号：US395743
申请日：1995-02-28
CPC分类号： C03C17/25 , H01J9/125 , C03C2217/228 , C03C2218/11 , C03C2218/113 , H01J2201/32 , H01J2209/012
摘要： A coating solution and a method of manufacturing a magnesium-oxide layer on a glass substrate. The layer obtained is characterized by a satisfactory adhesion and a high secondary electron emission coefficient. The curing temperature can remain below 250.degree. C., so that the method is suitable for the customary types of glass.Said coating solution comprising a solvent and partially acetylated and partially hydrolyzed Mg(OR).sub.2 of the formula Mg(OH).sub.x (OR).sub.y (OAc).sub.z.
摘要翻译： 一种涂布溶液和在玻璃基板上制造氧化镁层的方法。 所获得的层的特征在于令人满意的粘合力和高的二次电子发射系数。 固化温度可以保持在250℃以下，因此该方法适用于常规的玻璃类型。 所述涂覆溶液包含溶剂和式Mg（OH）x（OR）y（OAc）z的部分乙酰化和部分水解的Mg（OR）2。
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