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    Process for preparing thiophenols and novel thiophenols
    1.
    发明授权
    Process for preparing thiophenols and novel thiophenols 失效
    制备苯硫酚和新型苯硫酚的方法

    公开(公告)号：US4980510A

    公开(公告)日：1990-12-25

    申请号：US219103

    申请日：1988-07-14

    申请人： Hermann Hagemann ,  Klaus Sasse ,  Reiner Fischer

    发明人： Hermann Hagemann ,  Klaus Sasse ,  Reiner Fischer

    IPC分类号： C07D239/47 ,  A01N43/54 ,  C07B45/06 ,  C07C319/02 ,  C07C323/22 ,  C07C323/62 ,  C07C323/65 ,  C07D213/72 ,  C07D239/38 ,  C07D239/46

    CPC分类号： C07D239/47 ,  A01N43/54 ,  C07B45/06 ,  C07C323/00

    摘要： Thiophenols of the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 independently of each other each stand for hydrogen, halogen, nitro, alkyl, alkoxy, alkylthio, alkoxyalkyl, alkylthioalkyl, haloalkyl, haloalkoxy or alkylcarboxyl, optionally substituted aryl or optionally substituted hetaryl,R.sup.5 stands for alkyl, alkoxyalkyl, alkylthioalkyl, haloalkyl, alkenyl, haloalkenyl, optionally substituted aryl or optionally substituted hetaryl, andX stands for carbonyl, sulphinyl or sulphonyl can be obtained by reacting halobenzenes of the formula ##STR2## in which Hal stands for halogen, first with sodium hydrogen sulphide or sodium sulphide in the presence of a diluent to form compounds of the formula ##STR3## and then adding an acid to form the thiophenol, some of the thiophenols are novel and all can be used to form aryethioaminopyridides which are employed as herbicides.

    摘要翻译： 其中R 1，R 2，R 3和R 4各自独立地表示氢，卤素，硝基，烷基，烷氧基，烷硫基，烷氧基烷基，烷硫基烷基，卤代烷基，卤代烷氧基或烷基羧基，任选取代的芳基或任选地 取代的杂芳基，R5代表烷基，烷氧基烷基，烷硫基烷基，卤代烷基，烯基，卤代烯基，任选取代的芳基或任选取代的杂芳基，X代表羰基，亚磺酰基或磺酰基可以通过将式 代表卤素，首先用硫酸氢钠或硫化钠在稀释剂存在下形成式“IMAGE”的化合物，然后加入酸形成苯硫酚，一些苯硫酚是新颖的，都可用于形成 用作除草剂的芳硫氨基吡啶。

    Pyrimidyl-thio-carboxanilides
    4.
    发明授权
    Pyrimidyl-thio-carboxanilides 失效

    公开(公告)号：US4765824A

    公开(公告)日：1988-08-23

    申请号：US934064

    申请日：1986-11-21

    申请人： Klaus Sasse ,  Reiner Fischer ,  Hermann Hagemann ,  Hans-Joachim Santel ,  Robert R. Schmidt ,  Robert H. Strang

    发明人： Klaus Sasse ,  Reiner Fischer ,  Hermann Hagemann ,  Hans-Joachim Santel ,  Robert R. Schmidt ,  Robert H. Strang

    IPC分类号： A01N43/54 ,  C07D239/38 ,  C07D401/12 ,  C07D403/12 ,  A01N43/48 ,  C07D239/02

    CPC分类号： C07D401/12 ,  A01N43/54 ,  C07D239/38 ,  C07D403/12

    摘要： A pyrimidyl-thio-carboxanilide of the formula (I), ##STR1## in which R.sup.1 represents hydrogen or halogen, alkyl, alkoxy or alkylthio having 1 to 6 carbon atoms in each case, trifluoromethyl, or phenyl which is unsubstituted or mono- or poly-substituted, identically or differently, by halogen, methyl, ethyl, methoxy or trifluoromethyl,R.sup.2 represents hydrogen, halogen, alkyl having 1 to 6 carbon atoms or trifluoromethyl,R.sup.3 represents halogen, methyl or methoxy,n represents an integer 0, 1 or 2, andZ represents the radical ##STR2## where X represents oxygen or sulphur,R.sup.4 represents hydrogen or hydroxyl, alkyl or alkoxy having 1 to 6 carbon atoms in each case, alkenyl or alkynyl having 3 to 6 carbon atoms in each case, with the proviso that R.sup.4 does not represent hydrogen when X represents oxygen,R.sup.5 represents hydrogen, halogen or alkyl having 1 to 6 carbon atoms which is unsubstituted or mono- or poly-substituted by halogen orR.sup.4 and R.sup.5, together with the carbon atom and the nitrogen atom to which they are bonded, form a 3- to 8-membered heterocyclic ring which is unsubstituted or mono- or poly-substituted, identically or differently, by halogen, methyl or ethyl and which may contain one or more double bonds,R.sup.6 and R.sup.7, independently of one another, represent halogen or alkyl having 1 to 6 carbon atoms which is unsubstituted or mono- or poly-substituted by halogen,R.sup.6 and R.sup.7, together with the carbon atom to which they are bonded, form a 3- to 8-membered ring which may also contain oxygen and/or sulphur atoms as ring members in addition to carbon, and which is unsubstituted or mono- or poly-substituted by halogen, methyl or ethyl and which may contain one or more double bonds, andR.sup.8 represents hydrogen, alkyl having 1 to 6 carbon atoms, which is unsubstituted or mono- or poly-substituted by halogen, alkenyl or alkynyl having 3 to 6 carbon atoms in each case, processes for their preparation, herbicidal compositions and methods for combating weeds using such pyrimidyl-thio-carboxanilides.

    Process for the preparation of 4-mercaptobenzonitriles, and 4-mercaptobenzonitriles
    5.
    发明授权
    Process for the preparation of 4-mercaptobenzonitriles, and 4-mercaptobenzonitriles 失效
    制备4-巯基苯腈和4-巯基苯腈的方法

    公开(公告)号：US4841089A

    公开(公告)日：1989-06-20

    申请号：US937935

    申请日：1986-12-04

    申请人： Hermann Hagemann ,  Klaus Sasse

    发明人： Hermann Hagemann ,  Klaus Sasse

    IPC分类号： C07D239/38 ,  C07C67/00 ,  C07C313/00 ,  C07C319/14 ,  C07C323/62 ,  C07D213/70

    CPC分类号： C07C323/00

    摘要： 4-Mercaptobenzonitriles are prepared by reacting the appropriate 4-halogenobenzonitrile with sodium sulfide or sodium hydrogen sulfide in the presence of an inert organic solvent, and subsequently acidifying. The 4-mercaptobenzonitriles thus accessible are new, with the exception of the unsubstituted 4-mercaptobenzonitrile, and can be used as intermediates for the preparation of nematic liquid-crystalline products, herbicides and plant-growth regulators.

    摘要翻译： 通过在惰性有机溶剂的存在下使合适的4-卤代苄腈与硫化钠或硫化氢钠反应，然后酸化制备4-巯基苯腈。 因此可以使用的4-巯基苯腈是新的，除了未取代的4-巯基苄腈，可以用作制备向列型液晶产品，除草剂和植物生长调节剂的中间体。

    Herbicidal 2-[4-substituted carboxyamino-phenyl mercapto)]-subsituted pyrimidines
    7.
    发明授权
    Herbicidal 2-[4-substituted carboxyamino-phenyl mercapto)]-subsituted pyrimidines 失效
    除草剂2- [4-取代羧基氨基 - 苯基巯基]] - 取代的嘧啶

    公开(公告)号：US4797146A

    公开(公告)日：1989-01-10

    申请号：US937940

    申请日：1986-12-04

    申请人： Klaus Sasse ,  Hermann Hagemann ,  Hans-Joachim Santel ,  Robert R. Schmidt

    发明人： Klaus Sasse ,  Hermann Hagemann ,  Hans-Joachim Santel ,  Robert R. Schmidt

    IPC分类号： A01N43/54 ,  C07D239/38 ,  C07D405/12 ,  C07D239/02 ,  A01N43/48

    CPC分类号： C07D405/12 ,  A01N43/54 ,  C07D239/38

    摘要： Herbicidally, fungicidally and insecticidally active pyrimidylmercapto-acylanilides of the formula ##STR1## in which R.sup.1 represents methyl or ethyl,R.sup.2 represents halogen, methyl or ethyl,R.sup.3 represents hydrogen or methyl,R.sup.4 represents hydrogen, methyl or methoxy,n represents 0, 1 or 2,R.sup.5 represents hydrogen, halogen, cyano, optionally substituted alkyl having 1 to 6 carbon atoms, optionally substituted aryl, optionally substituted aralkyl or the --OR.sup.8 or --SO.sub.m --R.sup.8 radicals, whereR.sup.8 represents optionally substituted alkyl having 1 to 6 carbon atoms or optionally substituted aryl andm represents 0, 1 or 2, andR.sup.6 and R.sup.7, independently of one another, represent halogen or optionally substituted alkyl having 1 to 6 carbon atoms orR.sup.5 and R.sup.6, together with the neighboring carbon atom, represent an optionally substituted, saturated or unsaturated ring, which has 3 to 8 ring members and which can also contain oxygen and sulphur atoms in addition to carbon atoms, orR.sup.6 and R.sup.7, together with the neighboring carbon atom, represent an optionally substituted saturated or unsaturated ring which has 3 to 8 ring carbon atoms.

    摘要翻译： 甲基或乙基，R 3表示氢或甲基，R 4表示氢，甲基或甲氧基，n表示0,1或2，其中R1表示甲基或乙基，R2表示卤素，甲基或乙基，R4表示氢，甲基或甲氧基， 或2，R 5表示氢，卤素，氰基，任选取代的具有1至6个碳原子的烷基，任选取代的芳基，任选取代的芳烷基或-OR 8或-SO m -R 8基团，其中R 8表示任选取代的具有1至6个碳原子的烷基 原子或任选取代的芳基，m表示0,1或2，R 6和R 7彼此独立地表示卤素或任选取代的具有1至6个碳原子的烷基或R 5和R 6与相邻碳原子一起表示 任选取代的，饱和或不饱和的环，其具有3至8个环成员，并且除了碳原子之外还可含有氧和硫原子，或R6和R7以及t 他相邻的碳原子表示任选取代的饱和或不饱和的环，其具有3至8个环碳原子。

    Pyridylthio-acylanilide herbicides
    8.
    发明授权
    Pyridylthio-acylanilide herbicides 失效
    吡啶硫基酰基酰苯胺除草剂

    公开(公告)号：US4898608A

    公开(公告)日：1990-02-06

    申请号：US38700

    申请日：1987-04-15

    申请人： Klaus Sasse ,  Reiner Fischer ,  Hans-Joachim Santel ,  Robert R. Schmidt

    发明人： Klaus Sasse ,  Reiner Fischer ,  Hans-Joachim Santel ,  Robert R. Schmidt

    IPC分类号： C07D213/84 ,  A01N43/40 ,  C07D213/70 ,  C07D213/85 ,  C07D401/12 ,  C07D405/12

    CPC分类号： C07D213/70 ,  A01N43/40 ,  C07D213/85 ,  C07D401/12 ,  C07D405/12

    摘要： Novel herbicidally active pyridylthio-acylanilides of the formula ##STR1## in which R.sup.1, R.sup.2 and R.sup.3, independently of one another, represent hydrogen, halogen, cyano or trifluoromethyl or alkyl, alkoxy and alkylthio having 1 to 4 carbon atoms in each case,R.sup.4 represents halogen, methyl or methoxy,n represents a number 0, 1 or 2,z represents the group (Ia) ##STR2## or the group (Ib) ##STR3## where X represents oxygen, sulphur, an N--R.sup.10 or N--O--R.sup.11 group, or X and R.sup.g tpgether represent the ##STR4## radical, and the other radicals can have various meanings. Intermediates of the formulae ##STR5## are also new.

    摘要翻译： 式（I）的新型除草活性吡啶硫基 - 酰基酰苯胺，其中R 1，R 2和R 3彼此独立地代表氢，卤素，氰基或三氟甲基或每个具有1至4个碳原子的烷基，烷氧基和烷硫基 情况下，R 4表示卤素，甲基或甲氧基，n表示数字0,1或2，z表示基团（Ia）（Ia）或基团（Ib）其中X表示氧， 硫，N-R10或NO-R11基团，或X和Rg共表示基团，其他基团可以具有各种含义。 公式和的中间体也是新的。

    Pesticidal substituted aminophenyl carbamates
    10.
    发明授权
    Pesticidal substituted aminophenyl carbamates 失效
    农药取代氨基苯基氨基甲酸酯

    公开(公告)号：US5260474A

    公开(公告)日：1993-11-09

    申请号：US852484

    申请日：1992-03-16

    申请人： Bernd-Wieland Kruger ,  Klaus Sasse ,  Peter Heitkamper ,  Klaus Konig ,  Wilhelm Brandes ,  Gerd Hanssler ,  Albrecht Marhold

    发明人： Bernd-Wieland Kruger ,  Klaus Sasse ,  Peter Heitkamper ,  Klaus Konig ,  Wilhelm Brandes ,  Gerd Hanssler ,  Albrecht Marhold

    IPC分类号： C07C205/26 ,  C07C205/37 ,  C07C275/34 ,  C07D307/08 ,  C07D319/06 ,  C07C271/28 ,  C07C271/48

    CPC分类号： C07D307/08 ,  C07C205/26 ,  C07C205/37 ,  C07C275/34 ,  C07D319/06

    摘要： Fungicidal substituted aminophenyl carbamates of the formula ##STR1## in which X represents --CO--NR.sup.8 R.sup.9 ; --CO--OR.sup.9 ; --CO--SR.sup.9 ; --CO--R.sup.10 ; --SO.sub.2 R.sup.9 or hydrogen, in whichR.sup.8 represents hydrogen or alkyl,R.sup.9 represents optionally substituted aryl, optionally substituted aralkyl, optionally substituted alkyl, alkenyl, halogenoalkenyl, or in each case optionally substituted cycloalkyl, cycloalkenyl or cycloalkylalkyl, and R.sup.10 has the meaning of R.sup.9 or represents an optionally substituted heterocyclic ring,Y.sup.1 to Y.sup.4 are identical or different and represent hydrogen, halogen, nitro, cyano, alkyl, halogenoalkyl, alkoxy, halogenoalkoxy, alkylthio, alkylsulfonyl or halogenoalkylthio,R.sup.1 to R.sup.7 are identical or different and represent hydrogen, alkyl, halogenoalkyl or alkoxyalkyl,n represents 0 or 1, andZ represents alkyl, halogenoalkyl or a ##STR2##

    摘要翻译： 其中X表示-CO-NR8R9的式（I）的杀真菌取代的氨基苯基氨基甲酸酯; -CO-OR9; -CO-SR9; -CO-R10; -SO 2 R 9或氢，其中R 8表示氢或烷基，R 9表示任选取代的芳基，任选取代的芳烷基，任选取代的烷基，烯基，卤代烯基，或在每种情况下任选取代的环烷基，环烯基或环烷基烷基，R 10具有R 9 或表示任选取代的杂环，Y 1至Y 4相同或不同，表示氢，卤素，硝基，氰基，烷基，卤代烷基，烷氧基，卤代烷氧基，烷硫基，烷基磺酰基或卤代烷硫基，R 1至R 7相同或不同， 烷基，卤代烷基或烷氧基烷基，n表示0或1，Z表示烷基，卤代烷基或者“IMAGE”