Wool-like polyester filament and preparing method thereof

    公开(公告)号:US11091587B2

    公开(公告)日:2021-08-17

    申请号:US17042127

    申请日:2019-10-28

    摘要: A type of wool-like polyester filament and preparing method thereof are disclosed. The preparing method is manufacturing filament from a modified polyester through a POY process and a successive DTY processes, wherein the modified polyester is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, 1,4-butanediol, fluorinated dicarboxylic acid, tert-butyl branched hexanediol and 2,5,6,6-tetramethyl-2,5-heptanediol. The obtained fiber has a dye uptake of 90.32-93.27% and a K/S value of 22.15-23.42 when dyed at 100° C., and has an intrinsic viscosity drop of 17-20% when stored at 25° C. and R.H. 65% for 60 months. This invention features a method with ease of application and a product with good dyeing and degradation performance.

    Feather-like polyester fiber and preparing method thereof

    公开(公告)号:US10961641B2

    公开(公告)日:2021-03-30

    申请号:US17042957

    申请日:2019-10-28

    摘要: A type of feather-like polyester fiber and a preparing method thereof are disclosed. The preparing method is to manufacture filament from a modified polyester through a POY process with a four-fold flat spinneret and a successive DTY processes, wherein said modified polyester is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, ethylene glycol, main-chain silicated diol and fluorinated dicarboxylic acid, and the spinneret is the one set with four-fold flat shaped orifices. The obtained fiber has a dye uptake of 89.6-93.7% when dyed at 130° C., and has an intrinsic viscosity drop of 13-20% when stored at 25° C. and R.H. 65% for 60 months. This invention is simple to apply and features a product with good dyeing and degradation performance.

    Modified polyester and its preparation method

    公开(公告)号:US10465041B2

    公开(公告)日:2019-11-05

    申请号:US16322948

    申请日:2017-06-26

    摘要: A method for preparing the modified polyester. The modified polyester segments include terephthalic acid segment, ethylene glycol diol segment and branched diol segment, in which the branched diol segment refers to a diol segment in which a branch is located on a non-terminal carbon in the glycol segment and the branch is a linear carbon chain having 5 to 10 carbon atoms. The method includes preparing terephthalic acid glycol ester through the esterification of terephthalic acid and branched diol using the concentrated sulfuric acid as the catalyst. Then get ethylene terephthalate through the esterification of terephthalic acid and ethylene glycol. After stirring and mixing the two, the modified polyester can be obtained through polycondensation reaction of a low vacuum stage and a high vacuum stage using the catalyst and stabilizer.

    Semi-dull polyester drawn yarns and preparing method thereof

    公开(公告)号:US11788212B2

    公开(公告)日:2023-10-17

    申请号:US17042129

    申请日:2019-10-29

    摘要: A type of semi-dull polyester drawn yarns and preparing method thereof are disclosed. The preparing method is to melt spinning a modified polyester with FDY technique, wherein the modified polyester is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, ethylene glycol, main chain silicated diol, fluorinated dicarboxylic acid, matting agent and doped Bi2O3, in which the main chain silicated diol could be dimethylsiloxane diol, dimethyldiphenyldisiloxane glycol or tetramethyldisiloxane diol, and in which the fluorinated dicarboxylic acids could be 2,2-difluoro-1,3-malonic acid, 2,2-difluoro-1,4-succinic acid, 2,2-difluoro-1,5-glutaric acid or 2,2,3,3-tetrafluoro-1,4-succinic acid. The obtained fiber has a dye uptake of 87.5-91.8% when dyed at 120° C., and has an intrinsic viscosity drop of 18-26% when stored at 25° C. and R.H. 65% for 60 months. This invention features a method with ease of application and a product with good dyeing and degradation performance.

    Degradable polyester fiber and its preparation method

    公开(公告)号:US11686018B2

    公开(公告)日:2023-06-27

    申请号:US17789218

    申请日:2020-06-11

    摘要: A degradable polyester fiber and its preparation method are disclosed. The preparation method is to cool a PET melt dispersing with doped ZrO2 powder by ring-blowing after extruded from a trilobal spinneret hole on a spinneret, and manufacture a fully drawn yarn (FDY) according to an FDY process with the PET melt, then the degradable polyester fiber is prepared after a relaxation heat treatment. The trilobal spinneret hole on the spinneret has three leaves with unequal lengths and angles, and all the trilobal spinneret holes are distributed in concentric circles, with a center line of the leaf opposite to the smallest angle in each trilobal spinneret hole passing through the center of the circle, and pointing away from the center of the circle. The process is simple, and the obtain fiber has good performances in degradation and elasticity.