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    Composition of matter comprising more than 50% trans, trans-.DELTA.-damascone for augmenting or enhancing the aroma and taste of a smoking tobacco
    4.
    发明授权
    Composition of matter comprising more than 50% trans, trans-.DELTA.-damascone for augmenting or enhancing the aroma and taste of a smoking tobacco 失效
    包含超过50％反式，反式 - DELTA-马斯克酮用于增强或增强吸烟烟草的香气和味道的物质组成

    公开(公告)号：US4211242A

    公开(公告)日：1980-07-08

    申请号：US851727

    申请日：1977-11-15

    申请人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Richard A. Wilson ,  Frederick L. Schmitt ,  Manfred H. Vock ,  Edward J. Granda ,  Joacquin Vinals ,  Jacob Kiwala ,  William L. Schreiber

    发明人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Richard A. Wilson ,  Frederick L. Schmitt ,  Manfred H. Vock ,  Edward J. Granda ,  Joacquin Vinals ,  Jacob Kiwala ,  William L. Schreiber

    IPC分类号： A23L27/20 ,  A23L27/29 ,  A24B3/12 ,  A24B15/34 ,  A61K8/00 ,  A61K8/35 ,  A61Q11/00 ,  A61Q13/00 ,  C07C45/67 ,  C07C45/69 ,  C07C45/72 ,  C07C49/543 ,  C07C49/573 ,  C07C67/00 ,  C07C401/00 ,  C07C403/00 ,  C07C403/16 ,  C11B9/00

    CPC分类号： C11D3/0084 ,  A24B15/34 ,  C07C403/16 ,  C07C45/67 ,  C07C45/69 ,  C07C45/72 ,  C07C49/543 ,  C07C49/573 ,  C11B9/0034 ,  C07B2200/09 ,  C07C2101/16

    摘要： Described is a process for augmenting or enhancing the aroma and taste of a smoking tobacco comprising adding to said smoking tobacco an organoleptic property modifying quantity of a composition of matter comprising more than 50% trans,trans-.DELTA.-damascone and in addition a process for augmenting or enhancing the aroma and taste of a smoking tobacco comprising adding to said smoking tobacco in an organoleptic property modifying quantity a product produced according to the process of (i) reacting 1-alpha-acetyl-2-alpha,6,6-trimethyl-3-cyclohexene with strong base in aqueous ethanol at reflux thereby producing 1-alpha-acetyl-2-beta,6,6-trimethyl-3-cyclohexene; (ii) reacting the 1-alpha-acetyl-2-beta,6,6-trimethyl-3-cyclohexene with n-methyl aniline Grignard thereby forming a first organometallic compound; (iii) reacting said first organometallic compound with acetaldehyde thereby forming a second organometallic compound; (iv) reacting said second organometallic compound with acid in order to hydrolyze said second organometallic compound thereby forming a hydroxy ketone having the structure: ##STR1## in admixture with other compounds; (v) dehydrating said hydroxy ketone in admixture with other compounds thereby forming a mixture having a major proportion of trans, trans-.DELTA.-damascone having the structure: ##STR2## in admixture with cis, trans-.DELTA.-damascone having the structure: ##STR3## and in admixture with other compounds; and in addition smoking tobacco products containing same.

    摘要翻译： 描述了一种用于增强或增强吸烟烟草的香气和味道的方法，包括向所述吸烟烟草中添加包含超过50％反式，反式 - △ - 马斯酮酮的物质组合物的感官特性改性量，另外还包括 增加或增强烟草的香气和味道，其包括向所述吸烟烟草中加入感官特性调节量，根据以下方法生产的产物：（i）使1-α-乙酰基-2-α，6,6-三甲基 -3-环己烯与强碱在乙醇水溶液中反应，从而产生1-α-乙酰基-2-β，6,6-三甲基-3-环己烯; （ii）使1-α-乙酰基-2-β6,6-三甲基-3-环己烯与正甲基苯胺格氏试剂反应，从而形成第一有机金属化合物; （iii）使所述第一有机金属化合物与乙醛反应，从而形成第二有机金属化合物; （iv）使所述第二有机金属化合物与酸反应以水解所述第二有机金属化合物，从而形成具有以下结构的羟基酮：与其它化合物混合; （v）使所述羟基酮与其它化合物混合，从而形成具有以下结构的具有以下结构的具有以下结构的反式，反式 - 三氯乙酸 - 马来酰肼的主要比例的混合物：＆lt; IMAGE＆gt;与具有以下结构的顺式，反式 - IMAGE>并与其他化合物混合; 以及含有相同烟草制品的烟草制品。

    Process for augmenting or enhancing aroma or taste of smoking tobacco and smoking tobacco article using aldehyde composition
    5.
    发明授权
    Process for augmenting or enhancing aroma or taste of smoking tobacco and smoking tobacco article using aldehyde composition 失效
    使用醛组合物增强或增强吸烟烟草和烟草制品的香气或味道的方法

    公开(公告)号：US4627449A

    公开(公告)日：1986-12-09

    申请号：US754122

    申请日：1985-07-12

    申请人： Jacob Kiwala ,  Braja D. Mookherjee ,  Robert W. Trenkle

    发明人： Jacob Kiwala ,  Braja D. Mookherjee ,  Robert W. Trenkle

    IPC分类号： A24B15/32 ,  A24B3/12 ,  A24B15/30

    CPC分类号： A24B15/32

    摘要： Described is a method for augmenting or enhancing the aroma or taste of smoking tobacco or smoking tobacco articles by adding to smoking tobacco or to at least one section of the smoking tobacco article, e.g., the paper, the filter or the body of tobacco, a mixture consisting essentially of:(a) from about 0.5 up to about 7% by weight of said composition of n-hexanal;(b) from about 5 up to about 21% by weight of said composition of n-octanal;(c) from about 30 up to about 80% by weight of said composition of n-nonanal;(d) from 0 up to about 40% by weight of said composition of n-decanal;(e) from 0 up to about 7% by weight of said composition of n-tetradecanal;(f) from about 7 up to about 12% by weight of said composition of n-heptanal;(g) from 0 up to about 12% by weight of said composition of n-undecanal; and(h) from 0 up to about 12% by weight of said composition of n-dodecanal. Particularly, on smoking the side stream is modified and masked. The smokey, phenolic, cresolic odor is covered and the aroma in the environment around the smoked cigarette is clean and slightly citrusy.

    摘要翻译： 描述了通过添加到吸烟烟草或吸烟烟草制品的至少一个部分（例如纸张，过滤器或烟草体）来增强或增强吸烟烟草或吸烟烟草制品的香味或味道的方法， 混合物基本上由以下组成：（a）约0.5至约7重量％的所述组合物的正己醛; （b）所述组合物的约5至约21重量％的正辛醛; （c）所述组合物的约30至约80重量％的正壬醛; （d）所述组合物的正癸醛的0至约40重量％; （e）所述组合物的重量的0至约7％的正十四烷醛; （f）约7至约12重量％的所述组合物的正庚醛; （g）所述组合物的重量为0至约12％的正十一烷醛; 和（h）所述组合物的正十二烷醛的0至约12重量％。 特别地，在吸烟时，侧流被修改和掩蔽。 熏烟，酚醛，芳香气味被覆盖，烟熏香烟周围的香气清洁，略带柑橘。

    6-Hydroxy-2,6-dimethylheptanal, organoleptic uses thereof and processes for preparing the same
    8.
    发明授权
    6-Hydroxy-2,6-dimethylheptanal, organoleptic uses thereof and processes for preparing the same 失效
    6-羟基-2,6-二甲基庚醛，其感官用途及其制备方法

    公开(公告)号：US4287133A

    公开(公告)日：1981-09-01

    申请号：US169900

    申请日：1980-07-17

    申请人： Mark A. Sprecker ,  Robert W. Trenkle ,  Braja D. Mookherjee ,  Manfred H. Vock ,  Joaquin F. Vinals ,  Jacob Kiwala ,  Frederick L. Schmitt

    发明人： Mark A. Sprecker ,  Robert W. Trenkle ,  Braja D. Mookherjee ,  Manfred H. Vock ,  Joaquin F. Vinals ,  Jacob Kiwala ,  Frederick L. Schmitt

    IPC分类号： C07C45/54 ,  C07C45/56 ,  C07C45/64 ,  C07C47/19 ,  C11B9/00 ,  C07C141/10

    CPC分类号： C11B9/0015 ,  C07C45/54 ,  C07C45/56 ,  C07C45/64 ,  C07C47/19

    摘要： Described is the compound 6-hydroxy-2,6-dimethylheptanal and methods for preparing foodstuffs, flavoring compositions for foodstuffs, tobacco compositions, flavoring compositions for tobacco, perfume compositions, ingredients for perfume compositions, perfumed articles and ingredients for perfumed articles by including said 6-hydroxy-2,6-dimethylheptanal therein in order to produce:(a) In food flavorings, sweet, green, melon-like, tropical fruit-like, seedy and raspberry aromas and/or tastes;(b) In perfumes, sweet, green, melony, floral and muguet-like aromas; and(c) In tobaccos, sweet, fruity-melon-like, peach-like, and floral aromas prior to and on smoking in the main stream and in the sidestream in smoking tobaccos and the same aroma and taste nuances in the filter.Processes for synthesizing the 6-hydroxy-2,6-dimethylheptanal by hydrolysis of 2,6-dimethyl-5-heptenal are also described.

    摘要翻译： 描述了化合物6-羟基-2,6-二甲基庚醛以及制备食品的方法，用于食品的调味组合物，烟草组合物，烟草调味组合物，香料组合物，香料组合物成分，香料制品和用于香料制品的成分，包括所述 6-羟基-2,6-二甲基庚醛，以产生：（a）在食品香料中，甜味，绿色，瓜类，热带水果样，种子和覆盆子香气和/或口味; （b）香水，甜，绿，香，香，香，香; 和（c）在主烟道和吸烟烟草之间的吸烟之前和烟草中的烟草，甜味，水果瓜状，桃子状和花香味，以及过滤器中相同的香气和味道细微差别。 还描述了通过2,6-二甲基-5-庚烯醛水解合成6-羟基-2,6-二甲基庚醛的方法。