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    COMPOSITION FOR HYDROPHOBIC TREATMENT AND GLAZING
    3.
    发明申请
    COMPOSITION FOR HYDROPHOBIC TREATMENT AND GLAZING 有权
    组合物用于水处理和玻璃化

    公开(公告)号：US20090324968A1

    公开(公告)日：2009-12-31

    申请号：US12307927

    申请日：2007-07-10

    申请人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    发明人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    IPC分类号： B32B17/06 ,  C09D5/00

    CPC分类号： C07F7/0836 ,  C07F7/0838 ,  Y10T428/31612 ,  Y10T428/31663

    摘要： Hydrophobic treatment composition comprising one or more compounds, as a mixture, corresponding to the formula in which at least one R is a CaF2a+1 group, a being an integer, it being possible for another R to be an SiX3-bRCb1 group, b being 0, 1 or 2X being a hydrolysable group, such as alkoxy, hydroxyl or halo R1 being a hydrocarbon group, such as lower alkyl S is a hydrogen atom, an OH group, an alkyl group, in particular a lower alkyl group, such as CH3, or an OSiR2R3R4 group, R2, R3 and R4 being identical or different and consisting in particular of one of the abovementioned groups carried by an Si atom, such as (CH2)2—R, a hydrogen atom, an alkyl group or OSIR2R3R4, n is an integer≧1, the total number of Si atoms not exceeding 20. Process for treatment by this composition.Hydrophobic glass substrate thus obtained and its application, in particular as glazing.

    摘要翻译： 疏水性处理组合物，其包含一种或多种化合物，作为混合物，其中至少一个R为CaF 2 a + 1基团，a为整数，另外R为SiX 3-bRC b 1基团的式 0或1或2个X为可水解基团，例如烷氧基，羟基或卤素R 1为烃基，例如低级烷基S为氢原子，OH基团，烷基，特别是低级烷基， 例如CH 3或OSiR 2 R 3 R 4基团，R 2，R 3和R 4相同或不同，特别由上述基团之一由Si原子例如（CH 2）2 -R，氢原子，烷基 或OSIR2R3R4，n为整数> = 1，Si原子总数不超过20.用该组合物处理的方法。 这样得到的疏水玻璃基板及其应用，特别是玻璃。

    Method of Producing a Substrate Which is Coated With a Mesoporous Layer and Use Thereof in Ophthalmic Optics
    4.
    发明申请
    Method of Producing a Substrate Which is Coated With a Mesoporous Layer and Use Thereof in Ophthalmic Optics 有权
    产生介孔层的基板的制造方法及其在眼科用途中的应用

    公开(公告)号：US20080079894A1

    公开(公告)日：2008-04-03

    申请号：US11573137

    申请日：2005-05-03

    申请人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    发明人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    IPC分类号： C08J7/04 ,  G02C7/02

    CPC分类号： C09D183/04 ,  C09D183/02

    摘要： The invention relates to a method of producing a substrate which is coated with a mesoporous layer and to the use thereof in ophthalmic optics. The inventive method comprises the following steps consisting in: preparing a precursor sol containing (i) a precursor agent that is selected from compounds having formula M(X)4 (I), in which X is a hydrolysable group and M represents silicon or a tetravalent metal and mixtures thereof, (ii) at least one organic solvent, (iii) at least one pore-forming agent and (iv) water; depositing a film of the precursor sol on a main surface of the substrate; optionally consolidating the mesoporous structure of the deposited film; eliminating the pore-forming agent; and recovering the substrate coated with the mesoporous layer. The method is characterized in that: (i) the pore-forming agent is eliminated at a temperature of less than or equal to 150° C.; and (ii) the method comprises a step involving the introduction of at least one reactive agent bearing at least one hydrophobic group, before the deposition step (b) and/or after said step.

    摘要翻译： 本发明涉及一种制造涂覆有介孔层的基材的方法及其在眼科光学中的用途。 本发明的方法包括以下步骤：制备前体溶胶，所述前体溶胶含有（i）选自具有式M（X）4（I）的化合物的前体试剂，其中X是可水解基团，M代表硅或 四价金属及其混合物，（ii）至少一种有机溶剂，（iii）至少一种成孔剂和（iv）水; 在所述基板的主表面上沉积所述前体溶胶的膜; 可选地固结沉积膜的介孔结构; 消除造孔剂; 并回收涂有介孔层的基材。 该方法的特征在于：（i）在小于或等于150℃的温度下除去成孔剂; 和（ii）该方法包括在沉积步骤（b）和/或所述步骤之后引入至少一种带有至少一个疏水基团的反应剂的步骤。

    Method of producing a substrate which is coated with a mesoporous layer and use thereof in ophthalmic optics
    5.
    发明授权
    Method of producing a substrate which is coated with a mesoporous layer and use thereof in ophthalmic optics 有权
    制备涂覆有介孔层的基材的方法及其在眼科光学中的用途

    公开(公告)号：US08182866B2

    公开(公告)日：2012-05-22

    申请号：US11573137

    申请日：2005-05-03

    申请人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    发明人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    IPC分类号： B05D5/06 ,  C09D183/02 ,  C09D183/04 ,  G02B1/04

    CPC分类号： C09D183/04 ,  C09D183/02

    摘要： The invention relates to a method of producing a substrate which is coated with a mesoporous layer and to the use thereof in ophthalmic optics. The inventive method comprises the following steps comprising: preparing a precursor sol containing (i) a precursor agent that is selected from compounds having formula M(X)4 (I), in which X is a hydrolysable group and M represents silicon or a tetravalent metal and mixtures thereof, (ii) at least one organic solvent, (iii) at least one pore-forming agent and (iv) water; depositing a film of the precursor sol on a main surface of the substrate; optionally consolidating the mesoporous structure of the deposited film; eliminating the pore-forming agent; and recovering the substrate coated with the mesoporous layer. The method is characterized in that: (i) the pore-forming agent is eliminated at a temperature of less than or equal to 150° C.; and (ii) the method comprises a step involving the introduction of at least one reactive agent bearing at least one hydrophobic group, before the deposition step and/or after said step.

    摘要翻译： 本发明涉及一种制造涂覆有介孔层的基材的方法及其在眼科光学中的用途。 本发明的方法包括以下步骤：制备前体溶胶，该前体溶胶含有（i）选自具有式M（X）4（I）的化合物的前体试剂，其中X是可水解基团，M代表硅或四价 金属及其混合物，（ii）至少一种有机溶剂，（iii）至少一种造孔剂和（iv）水; 在所述基板的主表面上沉积所述前体溶胶的膜; 可选地固结沉积膜的介孔结构; 消除造孔剂; 并回收涂有介孔层的基材。 该方法的特征在于：（i）在小于或等于150℃的温度下除去成孔剂; 和（ii）该方法包括在沉积步骤之前和/或在所述步骤之后引入至少一种带有至少一个疏水基团的活性剂的步骤。

    Methods for Making an Article Coated with a Photochromic Film and Use Thereof in Ophthalmological Optics
    8.
    发明申请
    Methods for Making an Article Coated with a Photochromic Film and Use Thereof in Ophthalmological Optics 审中-公开
    制造涂有光致变色膜的物品的方法及其在眼科学中的应用

    公开(公告)号：US20130108858A1

    公开(公告)日：2013-05-02

    申请号：US12278130

    申请日：2007-01-31

    申请人： John Biteau ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Muriel Matheron ,  Lorraine Raboin

    发明人： John Biteau ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Muriel Matheron ,  Lorraine Raboin

    IPC分类号： B32B3/26 ,  B05D3/06 ,  B05D3/02 ,  B05D3/10

    CPC分类号： G02B5/23 ,  C03C1/008 ,  C03C17/007 ,  C03C2217/425 ,  C03C2218/113 ,  C08J7/047 ,  C08J2483/00 ,  C09K9/02 ,  C09K2211/1029 ,  C09K2211/1033 ,  C09K2211/1088 ,  G03C1/73 ,  Y10T428/249953

    摘要： The present invention relates to a method for making a substrate coated with a mesoporous photochromic film, comprising: a) preparing a precursor sol of a mesoporous film comprising an inorganic precursor agent, at least one organic solvent, water, at least one pore-forming agent and one hydrophobic precursor agent bearing at least one hydrophobic group; b) depositing a film of the precursor sol onto a main surface of a substrate; c) removing the pore-forming agent from the film resulting from the previous step at a temperature ≦150° C.; d) impregnating the mesoporous film resulting from step c) with a solution comprising at least one photochromic agent. In an alternative embodiment, the photochromic agent is directly introduced into the precursor sol. In an alternative embodiment of the previous alternative embodiment, the precursor sol does not comprise any hydrophobic precursor agent but the photochromic film is made hydrophobic by a treatment subsequent to its preparation.

    摘要翻译： 本发明涉及一种制备涂覆有介孔光致变色膜的基材的方法，包括：a）制备介孔膜的前体溶胶，所述介孔膜包含无机前体试剂，至少一种有机溶剂，水，至少一个成孔 剂和一种具有至少一个疏水基团的疏水性前体剂; b）将前体溶胶的膜沉积到基底的主表面上; c）在150℃的温度下从上一步骤得到的膜中除去造孔剂; d）用包含至少一种光致变色剂的溶液浸渍由步骤c）得到的介孔膜。 在替代实施方案中，将光致变色剂直接引入前体溶胶中。 在先前替代实施方案的替代实施方案中，前体溶胶不包含任何疏水性前体试剂，但是通过在其制备之后的处理使光致变色膜成为疏水性的。

    Hydrophobic treatment composition and glazing
    9.
    发明授权
    Hydrophobic treatment composition and glazing 有权
    疏水处理组合物和玻璃

    公开(公告)号：US08415016B2

    公开(公告)日：2013-04-09

    申请号：US12307927

    申请日：2007-07-10

    申请人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    发明人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    IPC分类号： B32B9/04

    CPC分类号： C07F7/0836 ,  C07F7/0838 ,  Y10T428/31612 ,  Y10T428/31663

    摘要： Hydrophobic treatment composition comprising one or more compounds, as a mixture, corresponding to the formula in which at least one R is a CaF2a+1 group, a being an integer, it being possible for another R to be an SiX3-bRC1b group, b being 0, 1 or 2 X being a hydrolysable group, such as alkoxy, hydroxyl or halo R1 being a hydrocarbon group, such as lower alkyl S is a hydrogen atom, an OH group, an alkyl group, in particular a lower alkyl group, such as CH3, or an OSiR2R3R4 group, R2, R3 and R4 being identical or different and consisting in particular of one of the abovementioned groups carried by an Si atom, such as (CH2)2—R, a hydrogen atom, an alkyl group or OSIR2R3R4, n is an integer≧1, the total number of Si atoms not exceeding 20. Process for treatment by this composition. Hydrophobic glass substrate thus obtained and its application, in particular as glazing.

    摘要翻译： 疏水性处理组合物，其包含一种或多种化合物，作为其中至少一个R为CaF 2 a + 1基团的化合物的混合物，a为整数，另外R可为SiX 3-bRC 1 b基团，b 0或1或2个X为可水解基团，例如烷氧基，羟基或卤素R 1为烃基，例如低级烷基S为氢原子，OH基团，烷基，特别是低级烷基， 例如CH 3或OSiR 2 R 3 R 4基团，R 2，R 3和R 4相同或不同，特别由上述基团之一由Si原子例如（CH 2）2 -R，氢原子，烷基 或OSIR2R3R4，n为1以上的整数，Si原子数不超过20个。 这样得到的疏水玻璃基板及其应用，特别是玻璃。

    METHOD FOR THE LOW-TEMPERATURE PREPARATION OF ELECTRICALLY CONDUCTIVE MESOSTRUCTURED COATINGS
    10.
    发明申请
    METHOD FOR THE LOW-TEMPERATURE PREPARATION OF ELECTRICALLY CONDUCTIVE MESOSTRUCTURED COATINGS 审中-公开
    电导体结构涂层低温制备方法

    公开(公告)号：US20130078458A1

    公开(公告)日：2013-03-28

    申请号：US13702043

    申请日：2011-05-26

    申请人： Claudine Biver ,  Sandrine Duluard ,  Joëlle Corde ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Sandrine Perruchas

    发明人： Claudine Biver ,  Sandrine Duluard ,  Joëlle Corde ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Sandrine Perruchas

    IPC分类号： B05D3/06

    CPC分类号： B05D3/065 ,  C23C18/1225 ,  C23C18/1254 ,  C23C18/1295 ,  C23C18/14 ,  C23C18/1603 ,  C23C18/165 ,  C23C18/1667 ,  C23C18/42 ,  Y10T428/265

    摘要： The present invention relates to a method for manufacturing mesostructural coatings comprising electrically conductive structures formed of metal nanoparticles. Said method includes the steps that involve: a) depositing on a substrate, a first layer consisting of a silica material, mesostructured by a structuring agent, and a photocatalytic material: b) depositing on the first layer, a second layer of a mesostructural silica material, said second layer being free of photocatalytic material: c) consolidating the first and second layers at at temperature between 50° C. and 250° C.; and d) placing the consolidating coating in contact with a solution that contains and irradiatting coating with a radiation that enables the photocatalytic material to be activated. Said method is characterized in that it includes no heat treatment at a temperature greater than 250° C.

    摘要翻译： 本发明涉及包含由金属纳米颗粒形成的导电结构的介观涂层的制造方法。 所述方法包括以下步骤：a）沉积在基材上，由由结构化剂介孔结构的二氧化硅材料和光催化材料组成的第一层，和b）在第一层上沉积第二层中等结构二氧化硅 所述第二层不含光催化材料：c）在50℃和250℃之间的温度下固化第一层和第二层; 以及d）将固结涂层与含有能够使光催化材料活化的辐射的包含和照射涂层的溶液接触。 所述方法的特征在于它不包括在大于250℃的温度下的热处理