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1.发明授权Nitrogen-mediated manufacturing method of transition metal-carbon nanotube hybrid materials 有权过渡金属 - 碳纳米管混合材料的氮介导制造方法公开(公告)号：US07897131B2
公开(公告)日：2011-03-01
申请号：US11878155
申请日：2007-07-20
申请人： Jeung-Ku Kang , Seong-Ho Yang , Hyun-Seok Kim , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Shin , Jun-Hyeon Bae
发明人： Jeung-Ku Kang , Seong-Ho Yang , Hyun-Seok Kim , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Shin , Jun-Hyeon Bae
CPC分类号： B82Y40/00 , B01J21/185 , B01J23/75 , B01J23/755 , B01J37/0203 , B01J37/16 , B82Y30/00 , C01B3/0021 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30449 , H01J2201/30469 , Y02E60/325
摘要： The present invention relates to a method for manufacturing a transition metal-carbon nanotube hybrid material using nitrogen as a medium. The present invention is characterized in that nitrogen-added carbon nanotube is grown in the presence of metal catalyst particles by reacting an hydrocarbon gas with a nitrogen gas by a chemical vapor deposition (CVD) and a transition metal-carbon nanotube hybrid material where a transition metal is uniformly attached to the entire carbon nanotube structure in which nitrogen with a great chemical reactivity is added as heterogeneous elements is chemically manufactured. Therefore, the present invention does not use an acid treatment required to attach transition-metal atoms to the carbon-nanotube, a surface treating process using a surfactant and the like and an inhibitor for preventing the coagulation of the transition metal so that a simplification of the process is obtained and the method is an environment-friendly method. The transition metal-carbon nanotube hybrid material manufactured by the above can be applied variously as a hydrogen storage material, a catalyst material, an electric field emission device and an electrode material.
摘要翻译： 本发明涉及使用氮作为介质制造过渡金属 - 碳纳米管混合材料的方法。 本发明的特征在于，通过化学气相沉积（CVD）和过渡金属 - 碳纳米管混合材料使碳氢化合物气体与氮气反应，在金属催化剂颗粒的存在下生长氮添加碳纳米管，其中过渡 金属均匀地附着在整个碳纳米管结构上，其中加入具有大的化学反应性的氮作为异质元素是化学制造的。 因此，本发明不使用将过渡金属原子附着在碳纳米管上所需的酸处理，使用表面活性剂等的表面处理方法和防止过渡金属凝结的抑制剂， 获得该过程，并且该方法是环境友好的方法。 由上述制造的过渡金属 - 碳纳米管混合材料可以用作储氢材料，催化剂材料，电场发射装置和电极材料。
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2.发明申请Nitrogen-mediated manufacturing method of transition metal-carbon nanotube hybrid materials 有权过渡金属 - 碳纳米管混合材料的氮介导制造方法公开(公告)号：US20080102015A1
公开(公告)日：2008-05-01
申请号：US11878155
申请日：2007-07-20
申请人： Jeung-Ku Kang , Seong-Ho Yang , Hyun-Seok Kim , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Shin , Jun-Hyeon Bae
发明人： Jeung-Ku Kang , Seong-Ho Yang , Hyun-Seok Kim , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Shin , Jun-Hyeon Bae
IPC分类号： C01B21/00
CPC分类号： B82Y40/00 , B01J21/185 , B01J23/75 , B01J23/755 , B01J37/0203 , B01J37/16 , B82Y30/00 , C01B3/0021 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30449 , H01J2201/30469 , Y02E60/325
摘要： The present invention relates to a method for manufacturing a transition metal-carbon nanotube hybrid material using nitrogen as a medium. The present invention is characterized in that nitrogen-added carbon nanotube is grown in the presence of metal catalyst particles by reacting an hydrocarbon gas with a nitrogen gas by a chemical vapor deposition (CVD) and a transition metal-carbon nanotube hybrid material where a transition metal is uniformly attached to the entire carbon nanotube structure in which nitrogen with a great chemical reactivity is added as heterogeneous elements is chemically manufactured. Therefore, the present invention does not use an acid treatment required to attach transition-metal atoms to the carbon-nanotube, a surface treating process using a surfactant and the like and an inhibitor for preventing the coagulation of the transition metal so that a simplification of the process is obtained and the method is an environment-friendly method. The transition metal-carbon nanotube hybrid material manufactured by the above can be applied variously as a hydrogen storage material, a catalyst material, an electric field emission device and an electrode material.
摘要翻译： 本发明涉及使用氮作为介质制造过渡金属 - 碳纳米管混合材料的方法。 本发明的特征在于，通过化学气相沉积（CVD）和过渡金属 - 碳纳米管混合材料使碳氢化合物气体与氮气反应，在金属催化剂颗粒的存在下生长氮添加碳纳米管，其中过渡 金属均匀地附着在整个碳纳米管结构上，其中加入具有大的化学反应性的氮作为异质元素是化学制造的。 因此，本发明不使用将过渡金属原子附着在碳纳米管上所需的酸处理，使用表面活性剂等的表面处理方法和防止过渡金属凝结的抑制剂， 获得该过程，并且该方法是环境友好的方法。 由上述制造的过渡金属 - 碳纳米管混合材料可以用作储氢材料，催化剂材料，电场发射装置和电极材料。
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3.发明申请Carbonnitride nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pore thereof 有权碳纳米管在其茎上具有纳米尺寸的孔，其制备方法和孔的尺寸和数量的控制方法公开(公告)号：US20090004091A1
公开(公告)日：2009-01-01
申请号：US11819700
申请日：2007-06-28
申请人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
发明人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
IPC分类号： C01C3/00
CPC分类号： C01B21/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2006/14 , C01P2006/16 , C23C16/347 , Y10S977/734
摘要： Disclosed are carbon nitride (C1-xNx) nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pores thereof.The present invention further has an object of providing the C1-xNx nanotube with pores having the size of not more than 1 nm over structure of the nanotube and a method for preparing the same.Another object of the present invention is to provide the control method of the size and quantity of pores with size of not more than 1 nm in the preparation of the C1-xNx nanotube with the pores over structure of the nanotube.The present invention can produce the C1-xNx nanotube with nano-sized pores by reacting hydrocarbon gas and nitrogen gas through plasma CVD in the presence of metal catalyst particles, wherein x ranges from 0.001 to 0.2.
摘要翻译： 公开了其茎上具有纳米尺寸孔的碳氮化物（C1-xNx）纳米管及其孔的尺寸和数量的制备方法和控制方法。 本发明的目的还在于提供具有尺寸不超过纳米管结构的1nm以上的孔的C1-xNx纳米管及其制备方法。 本发明的另一个目的是提供在制备具有纳米管结构的孔的C1-xNx纳米管的尺寸不超过1nm的孔的尺寸和数量的控制方法。 本发明可以在金属催化剂颗粒存在的情况下通过等离子体CVD与烃气体和氮气反应来生产具有纳米尺寸孔的C1-xNx纳米管，其中x为0.001至0.2。
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4.发明申请Carbonnitride nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pore thereof 有权碳纳米管在其茎上具有纳米尺寸的孔，其制备方法和孔的尺寸和数量的控制方法公开(公告)号：US20100015031A1
公开(公告)日：2010-01-21
申请号：US12457082
申请日：2009-06-01
申请人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
发明人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
IPC分类号： C01B21/00
CPC分类号： C01B21/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2006/14 , C01P2006/16 , C23C16/347 , Y10S977/734
摘要： Disclosed are carbon nitride (C1-xNx) nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pores thereof.The present invention further has an object of providing the C1-xNx nanotube with pores having the size of not more than 1 nm over structure of the nanotube and a method for preparing the same.Another object of the present invention is to provide the control method of the size and quantity of pores with size of not more than 1 nm in the preparation of the C1-xNx nanotube with the pores over structure of the nanotube.The present invention can produce the C1-xNx nanotube with nano-sized pores by reacting hydrocarbon gas and nitrogen gas through plasma CVD in the presence of metal catalyst particles, wherein x ranges from 0.001 to 0.2.
摘要翻译： 公开了其茎上具有纳米尺寸孔的碳氮化物（C1-xNx）纳米管及其孔的尺寸和数量的制备方法和控制方法。 本发明的目的还在于提供具有尺寸不超过纳米管结构的1nm以上的孔的C1-xNx纳米管及其制备方法。 本发明的另一个目的是提供在制备具有纳米管结构的孔的C1-xNx纳米管的尺寸不超过1nm的孔的尺寸和数量的控制方法。 本发明可以在金属催化剂颗粒存在的情况下通过等离子体CVD与烃气体和氮气反应来生产具有纳米尺寸孔的C1-xNx纳米管，其中x为0.001至0.2。
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公开(公告)号：US07563425B2
公开(公告)日：2009-07-21
申请号：US11819700
申请日：2007-06-28
申请人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
发明人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
CPC分类号： C01B21/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2006/14 , C01P2006/16 , C23C16/347 , Y10S977/734
摘要： Disclosed are carbon nitride (C1-xNx) nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pores thereof.The present invention further has an object of providing the C1-xNx nanotube with pores having the size of not more than 1 nm over structure of the nanotube and a method for preparing the same.Another object of the present invention is to provide the control method of the size and quantity of pores with size of not more than 1 nm in the preparation of the C1-xNx nanotube with the pores over structure of the nanotube.The present invention can produce the C1-xNx nanotube with nano-sized pores by reacting hydrocarbon gas and nitrogen gas through plasma CVD in the presence of metal catalyst particles, wherein x ranges from 0.001 to 0.2.
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6.发明授权Carbonnitride nanotubes with nano-sized pores on their stems, their preparation method and control method of size and quantity of pore thereof 有权碳纳米管在其茎上具有纳米尺寸的孔，其制备方法和孔的尺寸和数量的控制方法公开(公告)号：US07850940B2
公开(公告)日：2010-12-14
申请号：US12457082
申请日：2009-06-01
申请人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
发明人： Jeung-Ku Kang , Jai-Young Lee , Hyun-Seok Kim , Seong-Ho Yang , Kyu-Sung Han , Se-Yun Kim , Jung-Woo Lee , Weon-Ho Sin
IPC分类号： C01B31/00
CPC分类号： C01B21/0605 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2006/14 , C01P2006/16 , C23C16/347 , Y10S977/734
摘要： The present application provides a C1-xNx nanotube with pores having nano-sized diameter ranging from 5 to 10 Å, where x ranges from 0.001 to 0.2, and a method for controlling the size and quantity of pores in said nanotube by reacting hydrocarbon gas, nitrogen gas, and oxygen gas or hydrogen gas together in the presence of metal catalyst and by controlling the concentration of nitrogen gas.
摘要翻译： 本申请提供了一种C1-xNx纳米管，其具有范围为5至10埃的纳米尺寸直径的孔，其中x为0.001至0.2，以及通过使烃气体反应来控制所述纳米管中的孔的尺寸和数量的方法， 氮气和氧气或氢气一起在金属催化剂的存在下并通过控制氮气的浓度。
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7.发明申请公开(公告)号：US20090098402A1
公开(公告)日：2009-04-16
申请号：US12000375
申请日：2007-12-12
申请人： Jeung-Ku Kang , Augustine Saji , Jung-Woo Lee , Weon-Ho Shin , Kyu-Sung Han , Jung-Hoon Choi
发明人： Jeung-Ku Kang , Augustine Saji , Jung-Woo Lee , Weon-Ho Shin , Kyu-Sung Han , Jung-Hoon Choi
CPC分类号： B01J23/74 , B01J21/185 , B01J35/10 , B01J37/0238 , B01J37/349 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/18 , Y10S977/775 , Y10S977/777 , Y10T428/12014
摘要： Disclosed are a nanocrater catalyst in metal nanoparticles with a nanocrater form of hole structure in center of the catalyst which is useful for manufacturing nano-sized materials and/or articles with desired structure and characteristics, a preparation method thereof including a plasma etching and chemical etching process (“PTCE process”), and nano-sized materials and/or articles manufactured by using the nanocrater catalyst in metal nanoparticles.
摘要翻译： 公开了一种在催化剂中心具有纳米级形式的孔结构的金属纳米颗粒中的纳米尺寸催化剂，其可用于制造具有所需结构和特性的纳米尺寸材料和/或制品，其制备方法包括等离子体蚀刻和化学蚀刻 工艺（“PTCE工艺”）以及通过在金属纳米颗粒中使用纳米级催化剂制造的纳米尺寸的材料和/或制品。
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8.发明授权公开(公告)号：US08137760B2
公开(公告)日：2012-03-20
申请号：US12000375
申请日：2007-12-12
申请人： Jeung-Ku Kang , Augustine Saji , Jung-Woo Lee , Weon-Ho Shin , Kyu-Sung Han , Jung-Hoon Choi
发明人： Jeung-Ku Kang , Augustine Saji , Jung-Woo Lee , Weon-Ho Shin , Kyu-Sung Han , Jung-Hoon Choi
IPC分类号： H05H1/00
CPC分类号： B01J23/74 , B01J21/185 , B01J35/10 , B01J37/0238 , B01J37/349 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/18 , Y10S977/775 , Y10S977/777 , Y10T428/12014
摘要： Disclosed are a nanocrater catalyst in metal nanoparticles with a nanocrater form of hole structure in center of the catalyst which is useful for manufacturing nano-sized materials and/or articles with desired structure and characteristics, a preparation method thereof including a plasma etching and chemical etching process (“PTCE process”), and nano-sized materials and/or articles manufactured by using the nanocrater catalyst in metal nanoparticles.
摘要翻译： 公开了一种在催化剂中心具有纳米级形式的孔结构的金属纳米颗粒中的纳米尺寸催化剂，其可用于制造具有所需结构和特性的纳米尺寸材料和/或制品，其制备方法包括等离子体蚀刻和化学蚀刻 工艺（“PTCE工艺”）以及通过在金属纳米颗粒中使用纳米级催化剂制造的纳米尺寸的材料和/或制品。
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公开(公告)号：US20110256316A1
公开(公告)日：2011-10-20
申请号：US13140879
申请日：2009-02-03
申请人： Jeung-Ku Kang , Kyung-Min Choi , Jung-Hoon Choi , Weon-Ho Shin , Jung-Woo Lee , Hyung-Mo Jeong
发明人： Jeung-Ku Kang , Kyung-Min Choi , Jung-Hoon Choi , Weon-Ho Shin , Jung-Woo Lee , Hyung-Mo Jeong
CPC分类号： B81C1/00031 , B82Y30/00 , B82Y40/00 , C01B32/174
摘要： Disclosed is a method for patterning a nanomaterial using solution evaporation. More particularly, the method for patterning a nanomaterial using solution evaporation includes; coating the nanomaterial with a polymer material and uniformly dispersing the coated nanomaterial in a solvent to prepare a solution containing the nanomaterial, and pouring the nanomaterial-containing solution on a substrate, enabling the nanomaterial to be patterned after evaporation of the solvent.
摘要翻译： 公开了使用溶液蒸发来对纳米材料进行图案化的方法。 更具体地，使用溶液蒸发来构图纳米材料的方法包括： 用聚合物材料涂覆纳米材料，并将涂覆的纳米材料均匀分散在溶剂中以制备含有纳米材料的溶液，并将含纳米材料的溶液倾倒在基材上，使纳米材料在蒸发溶剂后进行图案化。
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公开(公告)号：US08758852B2
公开(公告)日：2014-06-24
申请号：US13140879
申请日：2009-02-03
申请人： Jeung-Ku Kang , Kyung-Min Choi , Jung-Hoon Choi , Weon-Ho Shin , Jung-Woo Lee , Hyung-Mo Jeong
发明人： Jeung-Ku Kang , Kyung-Min Choi , Jung-Hoon Choi , Weon-Ho Shin , Jung-Woo Lee , Hyung-Mo Jeong
CPC分类号： B81C1/00031 , B82Y30/00 , B82Y40/00 , C01B32/174
摘要： Disclosed is a method for patterning a nanomaterial using solution evaporation. More particularly, the method for patterning a nanomaterial using solution evaporation includes; coating the nanomaterial with a polymer material and uniformly dispersing the coated nanomaterial in a solvent to prepare a solution containing the nanomaterial, and pouring the nanomaterial-containing solution on a substrate, enabling the nanomaterial to be patterned after evaporation of the solvent.
摘要翻译： 公开了使用溶液蒸发来对纳米材料进行图案化的方法。 更具体地，使用溶液蒸发来构图纳米材料的方法包括： 用聚合物材料涂覆纳米材料，并将涂覆的纳米材料均匀分散在溶剂中以制备含有纳米材料的溶液，并将含纳米材料的溶液倾倒在基材上，使纳米材料在蒸发溶剂后进行图案化。
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