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    Coating apparatus, method of coating glass, compounds and compositions for coating glasss and coated glass substrates
    1.
    发明授权
    Coating apparatus, method of coating glass, compounds and compositions for coating glasss and coated glass substrates 失效
    涂布装置，玻璃涂覆方法，用于涂覆玻璃和涂覆的玻璃基板的化合物和组合物

    公开(公告)号：US5356718A

    公开(公告)日：1994-10-18

    申请号：US17930

    申请日：1993-02-16

    申请人： Patricia R. Athey ,  Douglas S. Dauson ,  David E. Lecocq ,  George A. Neuman ,  John F. Sopko ,  Royann L. Stewart-Davis

    发明人： Patricia R. Athey ,  Douglas S. Dauson ,  David E. Lecocq ,  George A. Neuman ,  John F. Sopko ,  Royann L. Stewart-Davis

    IPC分类号： B32B9/00 ,  B32B17/06 ,  C03C17/00 ,  C03C17/23 ,  C03C17/245 ,  C03C17/30 ,  C03C17/34 ,  C07C7/04 ,  C23C16/40 ,  C23C16/44 ,  C23C16/453 ,  C23C16/455 ,  C23C16/54

    CPC分类号： C03C17/245 ,  C03C17/002 ,  C03C17/2453 ,  C03C17/3417 ,  C23C16/401 ,  C23C16/4412 ,  C23C16/453 ,  C23C16/545 ,  C03C2217/211 ,  C03C2217/212 ,  C03C2217/213 ,  C03C2217/215 ,  C03C2217/216 ,  C03C2217/218 ,  C03C2217/219 ,  C03C2217/228 ,  C03C2217/23 ,  C03C2217/241 ,  C03C2217/244 ,  C03C2218/152

    摘要： An apparatus for coating a glass ribbon has an exhaust on each side of a coating unit at different distances therefrom. With this arrangement, portions of the ribbon upstream and downstream of the coating unit are exposed to coating vapors from the coating unit for different periods of time. A coating mixture includes tin containing precursors and a silicon containing precursor. The silicon containing precursor has the structural formula ##STR1## where R.sub.1 is a group which does not have an oxygen available to form a peroxide, R.sub.2 is a functional group giving the silicon containing precursor the ability to be easily converted to silicon oxide coating, R.sub.3 is a bridging group to provide for multiple silicon atoms and R.sub.4 completes the bonding on the foundation silicon atom. An accelerant e.g. a phosphorus containing precursor may be used with the metal containing precursors to increase the deposition rate of the coating. The coating deposited on the glass has regions of continuously varying weight percent of silicon oxide and tin oxide as the distance from the glass-coating interface increases, with the surface of the coating farthest from the glass-coating interface being predominantly tin oxide. The regions within the coating provide the coating with different indices of refraction to eliminate iridescence resulting from increased thickness of the tin oxide at the outer coating surface and to provide the coated glass article with a neutral color. When phosphorus is used as the accelerant, the percent of crystallinity is reduced and approaches O, thereby reducing or eliminating the coating haze.

    摘要翻译： 用于涂覆玻璃带的设备在与其不同的距离处的涂布单元的每一侧上具有排气。 通过这种布置，涂层单元的上游和下游的部分部分暴露于来自涂覆单元的涂覆蒸气不同的时间段。 涂料混合物包括含锡前体和含硅前体。 含硅前体具有结构式“IMAGE”，其中R1是不具有可用于形成过氧化物的氧的基团，R2是赋予含硅前体的能够容易地转化为氧化硅涂层的功能，R3 是提供多个硅原子的桥接基团，R4完成了在基础硅原子上的键合。 加速剂例如 可以将含磷前体与含金属的前体一起使用以增加涂层的沉积速率。 随着玻璃 - 涂层界面的距离增加，沉积在玻璃上的涂层具有连续变化重量百分比的氧化硅和氧化锡的区域，其中最远离玻璃 - 涂层界面的涂层的表面主要是氧化锡。 涂层中的区域为涂层提供不同的折射率，以消除由外涂层表面上的氧化锡厚度增加而产生的虹彩，并为涂覆的玻璃制品提供中性色。 当磷用作促进剂时，结晶度的百分比降低并接近O，从而减少或消除涂层雾度。

    Aqueous suspension for pyrolytic spray coating
    2.
    发明授权
    Aqueous suspension for pyrolytic spray coating 有权
    用于热解喷涂的水悬浮液

    公开(公告)号：US08197940B2

    公开(公告)日：2012-06-12

    申请号：US12179669

    申请日：2008-07-25

    申请人： John F. Sopko ,  Patricia R. Athey

    发明人： John F. Sopko ,  Patricia R. Athey

    IPC分类号： B32B15/00

    CPC分类号： C03C17/25 ,  C03C2217/217 ,  C03C2217/219 ,  C03C2217/23 ,  C03C2218/112

    摘要： The durability of a transparent pyrolytic spray applied coating is improved by providing a spray solution of metal acetylacetonates having different particle size distribution. More particularly, the particle size distribution of each of the metal acetylacetonates is a function of its melting temperature, and optionally of its melting temperature and solubility.

    摘要翻译： 通过提供具有不同粒度分布的金属乙酰丙酮化物的喷雾溶液来改善透明热解喷涂涂层的耐久性。 更具体地，每个金属乙酰丙酮化物的粒度分布是其熔融温度，以及任选其熔融温度和溶解度的函数。

    AQUEOUS SUSPENSION FOR PYROLYTIC SPRAY COATING
    3.
    发明申请
    AQUEOUS SUSPENSION FOR PYROLYTIC SPRAY COATING 有权
    水性喷雾涂料的水性悬浮液

    公开(公告)号：US20100021746A1

    公开(公告)日：2010-01-28

    申请号：US12179669

    申请日：2008-07-25

    申请人： John F. Sopko ,  Patricia R. Athey

    发明人： John F. Sopko ,  Patricia R. Athey

    IPC分类号： C23C14/54 ,  B01F13/00

    CPC分类号： C03C17/25 ,  C03C2217/217 ,  C03C2217/219 ,  C03C2217/23 ,  C03C2218/112

    摘要： The durability of a transparent pyrolytic spray applied coating is improved by providing a spray solution of metal acetylacetonates having different particle size distribution. More particularly, the particle size distribution of each of the metal acetylacetonates is a function of its melting temperature, and optionally of its melting temperature and solubility.

    摘要翻译： 通过提供具有不同粒度分布的金属乙酰丙酮化物的喷雾溶液来改善透明热解喷涂涂层的耐久性。 更具体地，每个金属乙酰丙酮化物的粒度分布是其熔融温度，以及任选其熔融温度和溶解度的函数。

    Compounds and compositions for coating glass with silicon oxide
    5.
    发明授权
    Compounds and compositions for coating glass with silicon oxide 失效
    用氧化硅涂覆玻璃的化合物和组合物

    公开(公告)号：US5599387A

    公开(公告)日：1997-02-04

    申请号：US472589

    申请日：1995-06-07

    申请人： George A. Neuman ,  Patricia R. Athey ,  Royann L. Stewart-Davis

    发明人： George A. Neuman ,  Patricia R. Athey ,  Royann L. Stewart-Davis

    IPC分类号： C03C17/00 ,  C03C17/245 ,  C03C17/34 ,  C23C16/40 ,  C23C16/44 ,  C23C16/453 ,  C23C16/54 ,  C09D5/00

    CPC分类号： C03C17/002 ,  C03C17/245 ,  C03C17/2453 ,  C03C17/3417 ,  C23C16/401 ,  C23C16/402 ,  C23C16/4412 ,  C23C16/453 ,  C23C16/545 ,  C03C2217/211 ,  C03C2217/212 ,  C03C2217/213 ,  C03C2217/215 ,  C03C2217/216 ,  C03C2217/218 ,  C03C2217/219 ,  C03C2217/228 ,  C03C2217/23 ,  C03C2217/241 ,  C03C2217/244 ,  C03C2218/152

    摘要： Silicon compounds useful as coating reactants for the chemical vapor deposition of silicon oxide are disclosed, along with compounds useful as accelerants to increase the deposition rate of silicon oxide. The silicon-containing precursor comprises the structural formula ##STR1## wherein R.sup.1 is an alkyl, alkenyl, alkynyl or aryl radical which may be substituted, and R.sub.2 is a functional group which increases the reactivity of the silicon compound by withdrawing electron density away from the silicon atom, such as hydrogen, halogen, alkenyl, alkynyl, halogenated alkyl and perhalogenated alkyl radicals. The accelerant is a compound selected to take advantage of the partial positive charge on the silicon atom. Such accelerant compounds include Lewis acids and bases; water; ozone; trivalent compounds of nitrogen, boron and phosphorus; tetravalent compounds of sulfur and selenium; pentavalent compounds of phosphorus and a variety of metal compounds. Also disclosed are compositions including an additional metal-containing coating precursor, such as an organotin compound, to deposit another metal oxide along with silicon oxide.

    摘要翻译： 公开了可用作氧化硅的化学气相沉积的涂料反应物的硅化合物，以及可用作增加氧化硅沉积速率的促进剂的化合物。 含硅前体包括结构式：其中R 1是可以被取代的烷基，链烯基，炔基或芳基，R 2是通过将电子密度从 硅原子，例如氢，卤素，烯基，炔基，卤代烷基和全卤代烷基。 促进剂是选择用于利用硅原子上的部分正电荷的化合物。 这种促进剂化合物包括路易斯酸和碱; 水; 臭氧; 氮，硼和磷的三价化合物; 硫和硒的四价化合物; 五价磷化合物和各种金属化合物。 还公开了包含另外的含金属的涂层前体，例如有机锡化合物，以沉积另外的金属氧化物和氧化硅的组合物。

    Coated substrates that include an undercoating
    6.
    发明授权
    Coated substrates that include an undercoating 有权
    涂层底物包括底漆

    公开(公告)号：US07431992B2

    公开(公告)日：2008-10-07

    申请号：US10914356

    申请日：2004-08-09

    申请人： Luke A. Kutilek ,  Caroline Harris ,  Patricia R. Athey ,  Songwei Lu

    发明人： Luke A. Kutilek ,  Caroline Harris ,  Patricia R. Athey ,  Songwei Lu

    IPC分类号： B32B9/00

    CPC分类号： C03C17/3417 ,  C03C17/3435

    摘要： A coated substrate is disclosed. The coated substrate includes a substrate; an undercoating having one or more materials selected from tin oxide, silica, titania, alumina, zirconia, zinc oxide and alloys and mixtures thereof nitrides of titanium, zirconium, hafnium, silicon, aluminum and mixtures thereof, and oxy-nitrides of titanium, zirconium, hafnium, silicon, aluminum and mixtures thereof overlaying at least a portion of the substrate; and a functional coating overlaying at least a portion of the undercoating. As a result of the undercoating, the coated substrate can exhibit improved properties such as improved aesthetic properties, increased durability, photocatalytic activity, mechanical durability, etc.

    摘要翻译： 公开了涂覆的基材。 被覆基板包括基板; 具有选自氧化锡，二氧化硅，二氧化钛，氧化铝，氧化锆，氧化锌及其混合物中的一种或多种材料的底涂层及其混合物钛，锆，铪，硅，铝及其混合物的氮化物，钛，锆的氧化物 ，铪，硅，铝及其混合物，覆盖至少一部分基底; 以及覆盖所述底涂层的至少一部分的功能性涂层。 作为底涂层的结果，涂布的基材可以表现出改善的性能，例如改善的美学性能，增加的耐久性，光催化活性，机械耐久性等。