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公开(公告)号：US07049394B2
公开(公告)日：2006-05-23
申请号：US10638484
申请日：2003-08-12
CPC分类号： C08J3/124 , C08J2325/00
摘要： The present invention provides a method for producing a free flowing and/or non clumping resin that includes prior to drying, shrinking the resin under agitation. In one variant of the invention, the is a resin used in solid phase synthesis of peptides. In another aspect the invention provides a process of making a peptide using the free flowing resin described herein, and a polypeptide made using the process. Various therapeutics are then be made using the polypepdite.
摘要翻译： 本发明提供一种自由流动和/或非聚集树脂的制造方法，其包括在干燥之前，在搅拌下使树脂收缩。 在本发明的一个变体中，它是用于固相合成肽的树脂。 在另一方面，本发明提供了使用本文所述的自由流动树脂制备肽的方法，以及使用该方法制备的多肽。 然后使用多肽制备各种治疗剂。
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公开(公告)号：US06939923B2
公开(公告)日：2005-09-06
申请号：US10636186
申请日：2003-08-07
摘要： A method for functionalizing a crosslinked polymer bead. The method comprises the steps of: (a) swelling the bead in a first solvent or solvent mixture to a volume from 200% to 310% of its volume when dry; and (b) contacting the bead with a functionalizing reagent in a second solvent or solvent mixture capable of swelling the bead to a volume from 200% to 310% of its volume when dry.
摘要翻译： 交联聚合物珠粒官能化的方法。 该方法包括以下步骤：（a）在干燥时将珠粒在第一溶剂或溶剂混合物中溶胀至其体积的200％至310％; 和（b）当干燥时，将珠粒与官能化试剂接触在能够使珠粒膨胀至其体积的200％至310％的体积的第二溶剂或溶剂混合物中。
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公开(公告)号：US07232849B2
公开(公告)日：2007-06-19
申请号：US10636148
申请日：2003-08-07
IPC分类号： C08F2/18
CPC分类号： C08F2/18
摘要： A crosslinked polymeric bead comprising a polymer having from 0.5 mole percent to 2 mole percent crosslinker. The bead has a diameter no greater than 200 μm, no void spaces having a diameter greater than 5 μm, and less than 5 weight percent of organic extractables.
摘要翻译： 一种交联聚合物珠，其包含具有0.5摩尔％至2摩尔％交联剂的聚合物。 胎圈具有不大于200μm的直径，没有直径大于5μm的孔隙空间和小于5重量％的有机可提取物。
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公开(公告)号：US20070287760A1
公开(公告)日：2007-12-13
申请号：US11449427
申请日：2006-06-08
IPC分类号： C08J9/28
CPC分类号： C08J9/286 , C08J2203/14 , C08J2333/08 , Y10T428/2982
摘要： A method for producing a macroporous acrylic resin in an aqueous suspension from a C1-C4 alkyl acrylate, an organic solvent and a crosslinker.
摘要翻译： 一种从C 1 -C 4烷基丙烯酸酯，有机溶剂和交联剂制备水性悬浮液中的大孔丙烯酸树脂的方法。
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公开(公告)号：US09447215B2
公开(公告)日：2016-09-20
申请号：US13218926
申请日：2011-08-26
申请人： James Charles Bohling , Steven James Broadwater , Arnold Stan Brownell , John William Hook, III , Reginald T. Smart
发明人： James Charles Bohling , Steven James Broadwater , Arnold Stan Brownell , John William Hook, III , Reginald T. Smart
IPC分类号： C08F30/02 , C08F220/18 , C08F297/02 , C08F297/04 , C08F2/00 , C08F2/22 , C08F265/06 , C09C1/00 , C09D7/12 , C08F220/06 , C08F220/36 , C08F230/02
CPC分类号： C08F220/18 , C08F2/001 , C08F2/22 , C08F220/06 , C08F220/36 , C08F230/02 , C08F265/06 , C08F297/02 , C08F297/026 , C08F297/04 , C09C1/0084 , C09D7/62
摘要： This invention provides a multistage emulsion polymer including, as copolymerized units: from 0.5% to 5%, by weight P-acid monomer, based on the weight of the emulsion polymer; from 0% to 0.05% by weight multiethylenically unsaturated monomer, based on the weight of the emulsion polymer; and at least one second monoethylenically unsaturated monomer; the emulsion polymer having a calculated Tg of from −20° C. to 50° C.; the emulsion polymer is formed by the “pulsed” addition of 75% to 100% of the P-acid monomer during a stage including from 10% to 50% of the total monomer weight, preferably added during the relatively early stages of the polymerization. A multistage polymer/TiO2 composite particle and an aqueous coating composition including the composite particle are also provided.
摘要翻译： 本发明提供了一种多级乳液聚合物，其包含基于乳液聚合物的重量的共聚单元：0.5％至5％重量的P酸单体; 基于乳液聚合物的重量，0％至0.05％重量的多烯属不饱和单体; 和至少一种第二单烯属不饱和单体; 所述乳液聚合物的计算Tg为-20℃至50℃; 乳液聚合物通过在包含总单体重量的10％至50％的阶段中“脉冲”加入75％至100％的P酸单体形成，优选在聚合的相对早期阶段加入。 还提供了多级聚合物/ TiO 2复合颗粒和包含复合颗粒的水性涂料组合物。
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公开(公告)号：US07074736B2
公开(公告)日：2006-07-11
申请号：US09973261
申请日：2001-10-09
IPC分类号： C08F6/64
CPC分类号： C08F10/00 , B01J31/06 , B01J31/2295 , B01J31/38 , C08F4/65908 , C08F4/65912 , C08F4/65925 , C08F110/02 , Y10S526/943 , C08F4/02 , C08F4/65916 , C08F4/027 , C08F2500/24
摘要： A hydrozirconated matrix for the production of polyolefins is disclosed. The hydrozirconated matrix is prepared from the reaction of an organozirconium composition and an olefin based material. A process is described for using the hydrozirconated matrix to prepare a range of polyolefin products.
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公开(公告)号：US08710133B2
公开(公告)日：2014-04-29
申请号：US13218977
申请日：2011-08-26
申请人： James Charles Bohling , John William Hook, III , Melinda H. Keefe , Arthur Grigorievich Kravchenko , Jeffrey J. Moretti , Judith Niece Varner
发明人： James Charles Bohling , John William Hook, III , Melinda H. Keefe , Arthur Grigorievich Kravchenko , Jeffrey J. Moretti , Judith Niece Varner
CPC分类号： C08K3/22
摘要： This invention provides a method for forming a stable aqueous composition including composite particles by admixing TiO2 particles and adsorbing emulsion polymer particles at or below the critical composite ratio to an equilibrated viscosity range of from 200 cps to 4000 cps. Also provided is a method for forming a stable aqueous composition including composite particles by admixing TiO2 particles and adsorbing emulsion polymer particles at a mixing intensity of greater than 2 hp/kgal. A method for providing a coating including composite particles is also included.
摘要翻译： 本发明提供了一种通过混合TiO 2颗粒并将临界复合比等于或低于临界复合比的乳液聚合物颗粒与200cps至4000cps的平衡粘度范围形成包含复合颗粒的稳定含水组合物的方法。 还提供了通过混合TiO 2颗粒并以大于2hp / kgal的混合强度吸附乳液聚合物颗粒来形成包含复合颗粒的稳定含水组合物的方法。 还包括提供包括复合颗粒的涂层的方法。
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公开(公告)号：US20120058278A1
公开(公告)日：2012-03-08
申请号：US13218977
申请日：2011-08-26
申请人： James Charles Bohling , John William Hook, III , Melinda H. Keefe , Arthur Grigorievich Kravchenko , Jeffrey J. Moretti , Judith Niece Varner
发明人： James Charles Bohling , John William Hook, III , Melinda H. Keefe , Arthur Grigorievich Kravchenko , Jeffrey J. Moretti , Judith Niece Varner
IPC分类号： B05D3/02 , C08K3/22 , C09D143/02
CPC分类号： C08K3/22
摘要： This invention provides a method for forming a stable aqueous composition including composite particles by admixing TiO2 particles and adsorbing emulsion polymer particles at or below the critical composite ratio to an equilibrated viscosity range of from 200 cps to 4000 cps. Also provided is a method for forming a stable aqueous composition including composite particles by admixing TiO2 particles and adsorbing emulsion polymer particles at a mixing intensity of greater than 2 hp/kgal. A method for providing a coating including composite particles is also included.
摘要翻译： 本发明提供了一种通过混合TiO 2颗粒并将临界复合比等于或低于临界复合比的乳液聚合物颗粒与200cps至4000cps的平衡粘度范围形成包含复合颗粒的稳定含水组合物的方法。 还提供了通过混合TiO 2颗粒并以大于2hp / kgal的混合强度吸附乳液聚合物颗粒来形成包含复合颗粒的稳定含水组合物的方法。 还包括提供包括复合颗粒的涂层的方法。
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公开(公告)号：US20120058277A1
公开(公告)日：2012-03-08
申请号：US13218926
申请日：2011-08-26
申请人： James Charles Bohling , Steven James Broadwater , Arnold Stan Brownell , John William Hook, III , Reginald T. Smart
发明人： James Charles Bohling , Steven James Broadwater , Arnold Stan Brownell , John William Hook, III , Reginald T. Smart
IPC分类号： C08K3/22 , B05D3/10 , C09D143/02 , C09D147/00 , C08F230/02 , C08F236/20
CPC分类号： C08F220/18 , C08F2/001 , C08F2/22 , C08F220/06 , C08F220/36 , C08F230/02 , C08F265/06 , C08F297/02 , C08F297/026 , C08F297/04 , C09C1/0084 , C09D7/62
摘要： This invention provides a multistage emulsion polymer including, as copolymerized units: from 0.5% to 5%, by weight P-acid monomer, based on the weight of the emulsion polymer; from 0% to 0.05% by weight multiethylenically unsaturated monomer, based on the weight of the emulsion polymer; and at least one second monoethylenically unsaturated monomer; the emulsion polymer having a calculated Tg of from −20° C. to 50° C.; the emulsion polymer is formed by the “pulsed” addition of 75% to 100% of the P-acid monomer during a stage including from 10% to 50% of the total monomer weight, preferably added during the relatively early stages of the polymerization. A multistage polymer/TiO2 composite particle and an aqueous coating composition including the composite particle are also provided.
摘要翻译： 本发明提供了一种多级乳液聚合物，其包含基于乳液聚合物的重量的共聚单元：0.5％至5％重量的P酸单体; 基于乳液聚合物的重量，0％至0.05％重量的多烯属不饱和单体; 和至少一种第二单烯属不饱和单体; 所述乳液聚合物的计算Tg为-20℃至50℃; 乳液聚合物通过在包含总单体重量的10％至50％的阶段中“脉冲”加入75％至100％的P酸单体形成，优选在聚合的相对早期阶段加入。 还提供了多级聚合物/ TiO 2复合颗粒和包含复合颗粒的水性涂料组合物。
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10.发明授权公开(公告)号：US08877852B2
公开(公告)日：2014-11-04
申请号：US11998911
申请日：2007-12-03
申请人： James Charles Bohling , Matthew Stewart Gebhard , Thomas Glenn Madle , Alvin Michael Maurice , Robert Joseph Pafford, IV , William Douglas Rohrbach
发明人： James Charles Bohling , Matthew Stewart Gebhard , Thomas Glenn Madle , Alvin Michael Maurice , Robert Joseph Pafford, IV , William Douglas Rohrbach
IPC分类号： C08L43/02 , C08K9/00 , C08F2/22 , C08F230/02 , C08F220/14 , C08F220/18 , C08F220/06
CPC分类号： C08F2/22 , C08F220/06 , C08F220/14 , C08F220/18 , C08F230/02
摘要： An organic polymer including internal pendant phosphorous acid groups at a level of >0.25% phosphorus by weight based on the weight of said organic polymer, the phosphorus acid groups being separated from the backbone of the organic polymer by no more than 2 alkylene glycol units, the organic polymer having an acid number of from 100 to 1,000, and a Mw of from 1,000 to 75,000, wherein the organic polymer has been formed by emulsion polymerization from at least one ethylenically unsaturated monomer is provided. Compositions further including an emulsion polymer including from 0.05% to 2% phosphorous, present as pendant phosphorous acid groups, by weight based on the weight of the emulsion polymer, and, optionally, an inorganic particle are also provided as are processes related to the compositions.
摘要翻译： 一种有机聚合物，包括基于所述有机聚合物的重量，重量百分比> 0.25重量％的内侧亚磷酸基团，磷酸基与有机聚合物的主链分开不超过2个亚烷基二醇单元， 提供酸值为100至1,000，Mw为1,000至75,000的有机聚合物，其中通过至少一种烯键式不饱和单体的乳液聚合形成有机聚合物。 还包括基于乳液聚合物的重量，以及任选的无机颗粒，包含以重量计，作为侧基亚磷酸基团存在的0.05％至2％的磷的乳液聚合物，以及任选的无机颗粒， 。
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