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    Pyrocarbonic acid diesters and the preparation and use thereof
    1.
    发明授权
    Pyrocarbonic acid diesters and the preparation and use thereof 失效
    焦碳酸二酯及其制备及应用

    公开(公告)号：US06222047B1

    公开(公告)日：2001-04-24

    申请号：US09006360

    申请日：1998-01-13

    申请人： John Zambounis ,  Véronique Hall-Goulle

    发明人： John Zambounis ,  Véronique Hall-Goulle

    IPC分类号： C07D48704

    CPC分类号： C07D471/04 ,  C07D487/04 ,  C09B1/005 ,  C09B5/62 ,  C09B7/02 ,  C09B19/02 ,  C09B29/0037 ,  C09B47/16 ,  C09B47/26 ,  C09B48/00 ,  C09B57/004 ,  C09B57/04 ,  C09B69/08 ,  C09K9/02

    摘要： The invention relates to the preparation of pyrocarbonic acid diesters by an improved process and to the novel pyrocarbonic acid diesters prepared according to said process as well as to the use thereof. The core of the invention is a process for the preparation of a pyrocarbonic acid diester of formula (I) wherein R1 and R1′ are each independently of the other branched or straight-chain C1-C24alkyl, C3-C24alkenyl, C3-C24alkynyl, C4-C12cycloalkyl, C4-C12cycloalkenyl or C7-C24aralkyl, each of which is unsubstituted or substituted by one or more than one substituent which is inert under the reaction conditions, by reacting at least one ester carbonate of formula (II) with 40-50 mol % of a sulfochloride of formula (IV) in the presence of 0.8-5 mol % of a catalyst of formula (V) and with minor amounts of a heterocyclic aromatic amine in a nonpolar inert solvent, in which process the amount of heterocyclic aromatic amine is 1-3 mol % and the reaction is carried out in the temperature range from −10° C. to +25° C., all molar amounts being based on 100 mol % of ester carbonate of formula (II).

    摘要翻译： 本发明涉及通过改进的方法制备焦碳碳酸二酯，以及根据所述方法制备的新型热解碳酸二酯以及其用途。本发明的核心是制备焦碳碳酸二酯的方法 其中R 1和R 1'各自独立地为其它支链或直链C 1 -C 24烷基，C 3 -C 24烯基，C 3 -C 24炔基，C 4 -C 12环烷基，C 4 -C 12环烯基或C 7 -C 24芳烷基，其各自为未取代的 或由一个或多于一个在反应条件下为惰性的取代基取代，通过使至少一种式（II）的碳酸酯与40-50摩尔％的式（IV）的磺酰氯在0.8-5.0的存在下反应 摩尔％的式（V）催化剂和少量杂环芳族胺的非极性惰性溶剂，其中杂环芳族胺的量为1-3摩尔％，反应在温度范围内进行 从-1 0℃至+ 25℃，所有摩尔量均为100摩尔％的式（II）酯酸酯。

    Pyrocarbonic acid diesters and the preparation and use thereof
    2.
    发明授权
    Pyrocarbonic acid diesters and the preparation and use thereof 失效
    焦碳酸二酯及其制备及应用

    公开(公告)号：US06359122B1

    公开(公告)日：2002-03-19

    申请号：US09767313

    申请日：2001-01-23

    申请人： John Zambounis ,  Véronique Hall-Goulle

    发明人： John Zambounis ,  Véronique Hall-Goulle

    IPC分类号： C07D27304

    CPC分类号： C07D471/04 ,  C07D487/04 ,  C09B1/005 ,  C09B5/62 ,  C09B7/02 ,  C09B19/02 ,  C09B29/0037 ,  C09B47/16 ,  C09B47/26 ,  C09B48/00 ,  C09B57/004 ,  C09B57/04 ,  C09B69/08 ,  C09K9/02

    摘要： The invention relates to the preparation of pyrocarbonic acid diesters by an improved process and to the novel pyrocarbonic acid diesters prepared according to said process as well as to the use thereof. The core of the invention is a process for the preparation of a pyrocarbonic acid diester of formula (I) wherein R1 and R1′ are each independently of the other branched or straight-chain C1-C24alkyl, C3-C24alkenyl, C3-C24alkynyl, C4-C12cycloalkyl, C4-C12cycloalkenyl or C7-C24aralkyl, each of which is unsubstituted or substituted by one or more than one substituent which is inert under the reaction conditions, by reacting at least one ester carbonate of formula (II)  with 40-50 mol % of a sulfochloride of formula (IV)  in the presence of 0.8-5 mol % of a catalyst of formula (V) and with minor amounts of a heterocyclic aromatic amine in a nonpolar inert solvent, in which process the amount of heterocyclic aromatic amine is 1-3 mol % and the reaction is carried out in the temperature range from −10° C. to +25° C., all molar amounts being based on 100 mol % of ester carbonate of formula (II).

    摘要翻译： 本发明涉及通过改进的方法制备焦碳碳酸二酯，以及根据所述方法制备的新型热解碳酸二酯以及其用途。本发明的核心是制备焦碳碳酸二酯的方法 其中R 1和R 1'各自独立地为其它支链或直链C 1 -C 24烷基，C 3 -C 24烯基，C 3 -C 24炔基，C 4 -C 12环烷基，C 4 -C 12环烯基或C 7 -C 24芳烷基，其各自为未取代的 或由一个或多于一个在反应条件下为惰性的取代基取代，通过使至少一种式（II）的碳酸酯与40-50摩尔％的式（IV）的磺酰氯在0.8-5.0的存在下反应 摩尔％的式（V）催化剂和少量杂环芳族胺的非极性惰性溶剂，其中杂环芳族胺的量为1-3摩尔％，反应在温度范围内进行 从 -10℃至+ 25℃，所有摩尔量基于100摩尔％的式（II）的碳酸酯酯。

    Curable mixtures based on epoxy resins comprising imidazoles
    3.
    发明授权
    Curable mixtures based on epoxy resins comprising imidazoles 有权
    基于包含咪唑的环氧树脂的可固化混合物

    公开(公告)号：US06455662B2

    公开(公告)日：2002-09-24

    申请号：US09728991

    申请日：2000-12-04

    申请人： Véronique Hall-Goulle

    发明人： Véronique Hall-Goulle

    IPC分类号： B32B2738

    CPC分类号： C07D233/54 ,  Y10T428/31511 ,  Y10T428/31515

    摘要： Curable mixtures suitable for the manufacture of moldings, coatings and foams comprises a) an epoxy resin having more than one 1,2-epoxy group per molecule, b) as curing catalyst, an imidazole compound of formula I wherein R1, R2 and R3 are each independently of the others a hydrogen atom, a halogen atom, alkyl having from 1 to 20 carbon atoms, alkoxy having from 1 to 20 carbon atoms, unsubstituted or halo-, nitro-, C1-4alkyl- or C1-4alkoxy-substituted aralkyl having from 7 to 20 carbon atoms, or unsubstituted or halo-, nitro-, C1-4alkyl- or C1-4alkoxy-substituted aryl having from 6 to 20 carbon atoms, and R4 is alkyl having from 1 to 20 carbon atoms, alkenyl having from 2 to 20 carbon atoms, alkynyl having from 2 to 20 carbon atoms, unsubstituted or halo-, nitro-, C1-4alkyl- or C1-4alkoxy-substituted aralkyl having from 7 to 20 carbon atoms or unsubstituted or halo-, nitro-, C1-4alkyl- or C1-4alkoxy-substituted aryl having from 6 to 20 carbon atoms; and c) curing agent such as dicyadiamide or an anhydride.

    摘要翻译： 适用于制造模制品，涂料和泡沫的可固化混合物包括：a）每分子具有多于一个1,2-环氧基的环氧树脂，b）作为固化催化剂，式I的咪唑化合物，其中R 1，R 2和R 3各自独立地为 的其它物质为氢原子，卤素原子，具有1-20个碳原子的烷基，具有1-20个碳原子的烷氧基，未取代的或卤素，硝基 - ，C 1-4烷基 - 或C 1-4烷氧基取代的芳烷基，其具有 7至20个碳原子，或未取代或卤代，硝基，C 1-4烷基或C 1-4烷氧基取代的具有6至20个碳原子的芳基，R 4为具有1至20个碳原子的烷基，具有2个 至20个碳原子，具有2至20个碳原子的炔基，未取代的或具有7至20个碳原子的未取代或卤代，硝基 - ，C 1-4烷基 - 或C 1-4烷氧基取代的芳烷基或未取代或卤代 - 硝基 - ， - 具有6至20个碳原子的4-烷基 - 或C 1-4烷氧基取代的芳基; 和c）固化剂如双氰胺或酐。

    Process for preparing fine pigment dispersions
    4.
    发明授权
    Process for preparing fine pigment dispersions 失效
    制备精细颜料分散体的方法

    公开(公告)号：US06211347B1

    公开(公告)日：2001-04-03

    申请号：US09539912

    申请日：2000-03-30

    申请人： Werner Sieber ,  Véronique Hall-Goulle

    发明人： Werner Sieber ,  Véronique Hall-Goulle

    IPC分类号： C09B6720

    CPC分类号： G03F1/56 ,  C09B29/338 ,  C09B33/153 ,  C09B35/035 ,  C09B67/0077 ,  G03F7/0007 ,  G03F7/105

    摘要： Preparation of pigment dispersions by a1) subjecting a mixture A comprising a latent pigment and a polymer to thermal, chemical or photolytic treatment and b) then adding a solvent, or a2) subjecting a mixture B comprising a latent pigment, a polymer and a solvent to thermal, chemical or photolytic treatment, new pigment dispersions and new latent pigments, their use in the process according to the invention for preparing the fine pigment dispersions and the use of the dispersions according to the invention for pigmenting high molecular mass material, including color filters.

    摘要翻译： 颜料分散体的制备通过a）将包含潜在颜料和聚合物的混合物A进行热，化学或光解处理，b）然后加入溶剂，或a）使包含潜在颜料，聚合物和溶剂的混合物B经热处理， 化学或光解处理，新颜料分散体和新的潜在颜料，它们在根据本发明用于制备细颜料分散体的方法中的用途以及使用根据本发明的分散体用于着色高分子量材料（包括滤色器）。

    TRANSPARENT COLOURANTS AND COLOURANT COMPOSITIONS, AND THEIR USE
    7.
    发明申请
    TRANSPARENT COLOURANTS AND COLOURANT COMPOSITIONS, AND THEIR USE 有权
    透明的富钴和钴合金组合物及其使用

    公开(公告)号：US20100021831A1

    公开(公告)日：2010-01-28

    申请号：US12527042

    申请日：2008-02-13

    申请人： Véronique Hall-Goulle

    发明人： Véronique Hall-Goulle

    IPC分类号： G03F1/00 ,  C07C49/303 ,  G03F7/004

    CPC分类号： C09B1/585 ,  C09B67/0033

    摘要： The invention relates to a colourant composition comprising in a weight ratio of from 99:1 to 10:90, preferably a weight ratio of from 95:5 to 30:70, particularly preferred a weight ratio of from 95:5 to 50:50, a pigment of average particle size from 10 to 200 nm and a 1- or 2-phenylthio-substituted anthraquinones of greenish-yellow colour hue, lacking electron-rich N(III), O(II) and further S(II) substituents on the anthraquinone ring. The compositions are particularly useful in patterned colour filters. Compounds wherein the 1- or 2-phenylthio group is substituted by SOR10, SO2R10, SO3R10, SO2NR11R12, CN, COR10, COOR10 or CONR11R12, or the anthraquinone group is substituted by SO2NR11R12 are also claimed, with a few exceptions. The invention also relates to a compound of Formula (III) or (IV), wherein at least one of R1, R2 and R3 is SOR10, SO2R10, SO3R10, SO2NR11R12, CN or COR10, or at least one of R7, R8 and R9 is SO2NR11R12, with the proviso that R3 is not SO2NH2.

    摘要翻译： 本发明涉及一种着色剂组合物，其包含重量比为99:1至10:90，优选95:5至30:70的重量比，特别优选的重量比为95:5至50:50 ，平均粒度为10〜200nm的颜料和绿黄色色调的1-或2-苯硫基取代的蒽醌，缺乏富电子的N（III），O（II）和另外的S（II）取代基 在蒽醌环上。 组合物在图案化滤色器中特别有用。 除了少数例外，还要求保护由SOR10，SO2R10，SO3R10，SO2NR11R12，CN，COR10，COOR10或CONR11R12或被SO2NR11R12取代的蒽醌基的化合物。 本发明还涉及式（III）或（IV）的化合物，其中R1，R2和R3中的至少一个是SOR10，SO2R10，SO3R10，SO2NR11R12，CN或COR10，或R7，R8和R9中的至少一个 是SO 2 NR 11 R 12，条件是R 3不是SO 2 NH 2。

    Pigmented vitreous material
    8.
    发明授权
    Pigmented vitreous material 失效
    着色玻璃质材料

    公开(公告)号：US06737533B2

    公开(公告)日：2004-05-18

    申请号：US10335727

    申请日：2003-01-02

    申请人： Véronique Hall-Goulle ,  Zhimin Hao

    发明人： Véronique Hall-Goulle ,  Zhimin Hao

    IPC分类号： C07D48702

    CPC分类号： C07D409/12 ,  C03C14/008 ,  C03C17/007 ,  C03C17/009 ,  C03C17/28 ,  C03C2214/17 ,  C03C2214/32 ,  C03C2217/485 ,  C03C2218/113 ,  C07D209/46 ,  C07D487/04 ,  C07D493/04 ,  Y10T428/10 ,  Y10T428/1095 ,  Y10T428/131

    摘要： The present application relates to a process for the manufacture of pigmented vitreous materials, as well as to pigmented vitreous materials, characterized by the use of soluble pigment precursors and preferably the absence of significant amounts of dispersants. These pigmented vitreous materials can be used as coloured materials for any known purposes. Soluble pigment precursors comprising a partial structure: are also claimed, wherein X1 is an aromatic or heteroaromatic ring, B is hydrogen or a group of the formula: but at least one group B is not hydrogen, and L is a solubilizing group.

    摘要翻译： 本申请涉及一种用于制备着色玻璃质材料的方法，以及着色的玻璃质材料，其特征在于使用可溶性颜料前体，优选不存在显着量的分散剂。 这些着色的玻璃质材料可以用作任何已知目的的有色材料。 还要求保护含有部分结构的可溶性颜料前体，其中X1是芳族或杂芳族环，B是氢或下列基团：但至少一个B不是氢，L是增溶基团。

    Photoactivatable nitrogen-containing bases based on alpha-amino ketones
    10.
    发明授权
    Photoactivatable nitrogen-containing bases based on alpha-amino ketones 失效
    基于α-氨基酮的可光活化含氮碱

    公开(公告)号：US06410628B1

    公开(公告)日：2002-06-25

    申请号：US09880212

    申请日：2001-06-13

    申请人： Véronique Hall-Goulle ,  Sean Colm Turner

    发明人： Véronique Hall-Goulle ,  Sean Colm Turner

    IPC分类号： C08L9106

    CPC分类号： C08L91/06 ,  B33Y70/00 ,  C07D487/04 ,  C08K5/17

    摘要： The invention relates to organic compounds having a molecular weight of less than 1000 comprising at least one structural unit of the formula (I) in which R1 is an aromatic or heteroaromatic radical which is capable of absorbing light in the wavelength range from 200 to 650 nm and in doing so brings about cleavage of the adjacent carbon-nitrogen bond. The compounds represent photoinitiators for base-catalyzable reactions. Other subjects of the invention are base-polymerizable or crosslinkable compositions comprising compounds having a structural unit of the formula I, a method of implementing photochemically induced, base-catalyzed reactions, and the use of the compounds as photoinitiators for base-catalyzed reactions.

    摘要翻译： 本发明涉及分子量小于1000的有机化合物，其包含至少一种式（I）的结构单元，其中R 1是能够吸收200至650nm波长范围内的光的芳族或杂芳族基团 并且这样做导致相邻碳 - 氮键的裂解。化合物表示用于碱可催化反应的光引发剂。 本发明的其它主题是包含具有式I结构单元的化合物的碱可聚合或可交联组合物，实施光化学诱导的碱催化反应的方法，以及该化合物作为碱式催化反应的光引发剂的用途。