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    Process for producing terephthalic acid
    1.
    发明授权
    Process for producing terephthalic acid 有权
    对苯二甲酸生产方法

    公开(公告)号：US08884055B2

    公开(公告)日：2014-11-11

    申请号：US13155553

    申请日：2011-06-08

    Applicant: Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    Inventor： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina I. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC: C07C51/16 ,  C07C51/265

    CPC classification number: C07C51/265 ,  C07C51/42 ,  Y02P20/52 ,  Y02P20/542 ,  C07C63/26

    Abstract: A solid terephthalic acid composition and a process for producing terephthalic acid from para-xylene. The process comprises forming a mixture comprising the para-xylene, a solvent, a bromine source, and a catalyst; and oxidizing the para-xylene by contacting the mixture with an oxidizing agent at oxidizing conditions to produce a solid oxidation product comprising terephthalic acid, para-toluic acid, 4-carboxybenzaldehyde. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an dialkyl imidazolium ionic liquid; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium. The solid terephthalic acid composition comprises, less than about 4,000 ppm-wt 4-carboxybenzaldehyde content, and more than about 2,000 ppm-wt a para-toluic acid.

    Abstract translation: 固体对苯二甲酸组合物和由对二甲苯生产对苯二甲酸的方法。 该方法包括形成包含对二甲苯，溶剂，溴源和催化剂的混合物; 并通过在氧化条件下将氧化剂与氧化剂接触来氧化对二甲苯以产生包含对苯二甲酸，对甲苯甲酸，4-羧基苯甲醛的固体氧化产物。 溶剂包括具有1至7个碳原子的羧酸和二烷基咪唑鎓离子液体; 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。 固体对苯二甲酸组合物包含小于约4,000ppm重量的4-羧基苯甲醛含量和大于约2,000ppm重量的对甲苯甲酸。

    PROCESS FOR OXIDIZING ALKYL AROMATIC COMPOUNDS
    3.
    发明申请
    PROCESS FOR OXIDIZING ALKYL AROMATIC COMPOUNDS 有权
    用于氧化烷基芳族化合物的方法

    公开(公告)号：US20120004449A1

    公开(公告)日：2012-01-05

    申请号：US13155519

    申请日：2011-06-08

    Applicant: Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina L. Kuznetsova ,  Bair S. Bal'zhinimaev

    Inventor： Alakananda Bhattacharyya ,  Joseph A. Kocal ,  Joel T. Walenga ,  Nikolay Y. Adonin ,  Nina L. Kuznetsova ,  Bair S. Bal'zhinimaev

    IPC: C07C51/265 ,  C07C51/42 ,  C07C51/16

    CPC classification number: C07C51/265 ,  C07C63/16 ,  C07C63/24 ,  C07C63/26 ,  C07C63/06

    Abstract: A process and a mixture for oxidizing an alkyl-aromatic compound comprises forming a mixture comprising the alkyl-aromatic compound, a solvent, a bromine source, and a catalyst; and contacting the mixture with an oxidizing agent at oxidizing conditions to produce an oxidation product comprising at least one of an aromatic aldehyde, an aromatic alcohol, an aromatic ketone, and an aromatic carboxylic acid. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an ionic liquid selected from the group consisting of an imidazolium ionic liquid, a pyridinium ionic liquid, a phosphonium ionic liquid, a tetra alkyl ammonium ionic liquid, and combinations thereof. The catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium.

    Abstract translation: 用于氧化烷基 - 芳族化合物的方法和混合物包括形成包含烷基 - 芳族化合物，溶剂，溴源和催化剂的混合物; 以及在氧化条件下使所述混合物与氧化剂接触以产生包含芳族醛，芳族醇，芳族酮和芳族羧酸中的至少一种的氧化产物。 溶剂包括具有1至7个碳原子的羧酸和选自咪唑鎓离子液体，吡啶鎓离子液体，鏻离子液体，四烷基铵离子液体及其组合的离子液体。 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。

    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS
    4.
    发明申请
    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS 有权
    用于连续生成聚合物的催化方法

    公开(公告)号：US20110313210A1

    公开(公告)日：2011-12-22

    申请号：US13193227

    申请日：2011-07-28

    Applicant: Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    Inventor： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    IPC: C07C31/20

    CPC classification number: C07C29/132 ,  C10G3/44 ,  C10G3/46 ,  C10G3/48 ,  C10G3/52 ,  C10G3/56 ,  C10G2300/1014 ,  Y02P20/52 ,  Y02P30/20 ,  C07C31/202 ,  C07C31/205

    Abstract: A catalytic process for generating at least one polyol from a feedstock comprising cellulose is performed in a continuous manner. The process involves, contacting, continuously, hydrogen, water, and a feedstock comprising cellulose, with a catalyst to generate an effluent stream comprising at least one polyol, water, hydrogen, and at least one co-product. The water, hydrogen, and at least one co-product are separated from the effluent stream and recycled to the reaction zone. The polyol is recovered from the effluent stream.

    Abstract translation: 以包含纤维素的原料生成至少一种多元醇的催化方法是以连续方式进行的。 该方法包括使含有纤维素的氢，水和原料与催化剂连续地接触，以产生包含至少一种多元醇，水，氢和至少一种共同产物的流出物流。 将水，氢和至少一种副产物与流出物流分离并再循环至反应区。 从流出物流中回收多元醇。

    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS
    5.
    发明申请
    CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS 有权

    公开(公告)号：US20110313209A1

    公开(公告)日：2011-12-22

    申请号：US13193200

    申请日：2011-07-28

    Applicant: Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    Inventor： Tom N. Kalnes ,  John Q. Chen ,  Joseph A. Kocal

    IPC: C07C29/74

    CPC classification number: C07C29/132 ,  C07C31/20

    Abstract: A catalytic process for generating at least one polyol from a feedstock comprising cellulose is performed in a continuous manner. The process involves, contacting, continuously, hydrogen, water, and a feedstock comprising cellulose, with a catalyst to generate an effluent stream comprising at least one polyol, water, hydrogen, and at least one co-product. The water, hydrogen, and at least one co-product are separated from the effluent stream and recycled to the reaction zone. The polyol is recovered from the effluent stream.

    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME
    7.
    发明申请
    LOW OXYGEN BIOMASS-DERIVED PYROLYSIS OILS AND METHODS FOR PRODUCING THE SAME 有权
    低氧生物质衍生的热解油及其生产方法

    公开(公告)号：US20110201855A1

    公开(公告)日：2011-08-18

    申请号：US12707433

    申请日：2010-02-17

    Applicant: Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    Inventor： Richard Marinangeli ,  Timothy A. Brandvold ,  Joseph A. Kocal

    IPC: C10G1/00

    CPC classification number: C10G3/44 ,  C10G3/45 ,  C10G3/47 ,  C10G3/48 ,  C10G3/49 ,  C10G2400/30 ,  Y02E50/14 ,  Y02P30/20

    Abstract: Low oxygen biomass-derived pyrolysis oils and methods for producing them from carbonaceous biomass feedstock are provided. The carbonaceous biomass feedstock is pyrolyzed in the presence of a catalyst comprising base metal-based catalysts, noble metal-based catalysts, treated zeolitic catalysts, or combinations thereof to produce pyrolysis gases. During pyrolysis, the catalyst catalyzes a deoxygenation reaction whereby at least a portion of the oxygenated hydrocarbons in the pyrolysis gases are converted into hydrocarbons. The oxygen is removed as carbon oxides and water. A condensable portion (the vapors) of the pyrolysis gases is condensed to low oxygen biomass-derived pyrolysis oil.

    Abstract translation: 提供了低氧生物质衍生的热解油及其从碳质生物质原料生产它们的方法。 在含有贱金属基催化剂，贵金属基催化剂，经处理的沸石催化剂或其组合的催化剂存在下，碳质生物质原料热解产生裂解气。 在热解期间，催化剂催化脱氧反应，由此将热解气体中的至少一部分氧化烃转化成烃。 作为碳氧化物和水除去氧气。 热解气体的可冷凝部分（蒸汽）被冷凝成低氧生物质衍生的裂解油。

    Metal cation-modified alkylation catalysts
    10.
    发明授权
    Metal cation-modified alkylation catalysts 失效
    金属阳离子改性烷基化催化剂

    公开(公告)号：US5739074A

    公开(公告)日：1998-04-14

    申请号：US453044

    申请日：1995-05-30

    Applicant: Joseph A. Kocal ,  Anil R. Oroskar

    Inventor： Joseph A. Kocal ,  Anil R. Oroskar

    IPC: B01J23/02 ,  B01J23/04 ,  B01J27/08 ,  C07C2/58 ,  B01J27/135

    CPC classification number: B01J23/02 ,  B01J23/04 ,  B01J27/08 ,  C07C2/58 ,  C07C2521/02 ,  C07C2521/04 ,  C07C2521/06 ,  C07C2521/12 ,  C07C2523/42 ,  C07C2523/44 ,  C07C2523/46 ,  C07C2523/755 ,  C07C2527/125 ,  C07C2527/126

    Abstract: A catalytic composite of a refractory inorganic oxide whose bound surface hydroxyl group has reacted with a Friedel-Crafts type metal halide and whose acidity has been modified by the deposition of a monovalent metal cation, especially an alkali metal cation, or alkaline earth metal cation shows superior selectivity and a significantly decreased cracking tendency relative to similar catalysts without the monovalent metal or alkaline earth metal cation. The resulting alkylate from an isobutane-butene feedstock shows a substantial increase in research octane number relative to the alkylate formed by a similar catalyst which has not been so modified by an alkali or alkaline earth metal cation.

    Abstract translation: 结合表面羟基与Friedel-Crafts型金属卤化物反应并且酸性已经通过沉积一价金属阳离子，特别是碱金属阳离子或碱土金属阳离子而改性的耐火无机氧化物的催化复合物显示出 优异的选择性和相对于没有一价金属或碱土金属阳离子的类似催化剂显着降低的开裂趋势。 从异丁烷 - 丁烯原料得到的烷基化物相对于由未被碱金属或碱土金属阳离子改性的类似催化剂形成的烷基化物，研究辛烷值显着增加。

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