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公开(公告)号：US08197965B2
公开(公告)日：2012-06-12
申请号：US12201332
申请日：2008-08-29
申请人： Jun Tamura , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
发明人： Jun Tamura , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
CPC分类号： H01M4/8605 , H01M4/925 , H01M4/926 , H01M2004/8684 , H01M2008/1095
摘要： This invention provides an anode for a fuel cell which can realize stable output for a long period of time, and a fuel cell using the anode for a fuel cell. The anode for a fuel cell comprises an electrode catalyst layer, the electrode catalyst layer comprising a supported catalyst comprising an electroconductive carrier material and catalyst fine particles supported on the electroconductive carrier material, a proton conductive inorganic oxide, and a proton conductive organic polymer binder, the weight ratio between the supported catalyst (C) and the proton conductive inorganic oxide (SA), WSA/WC, being 0.06 to 0.38, the weight ratio between the proton conductive inorganic oxide (SA) and the proton conductive organic polymer binder (P), WP/WSA, being 0.125 to 0.5.
摘要翻译： 本发明提供一种能够长时间实现稳定输出的燃料电池用阳极和使用燃料电池用阳极的燃料电池。 用于燃料电池的阳极包括电极催化剂层，该电极催化剂层包含负载的催化剂，其包含导电载体材料和负载在导电载体材料上的催化剂细颗粒，质子传导性无机氧化物和质子传导性有机聚合物粘合剂， 载体催化剂（C）和质子传导性无机氧化物（SA）之间的重量比WSA / WC为0.06〜0.38，质子传导性无机氧化物（SA）与质子传导性有机聚合物粘合剂（P ），WP / WSA为0.125〜0.5。
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2.发明授权Catalyst, method for producing catalyst, membrane electrode assembly, and fuel cell 有权催化剂，催化剂生产方法，膜电极组件和燃料电池公开(公告)号：US08173306B2
公开(公告)日：2012-05-08
申请号：US12050497
申请日：2008-03-18
申请人： Itsuko Mizutani , Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
发明人： Itsuko Mizutani , Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
CPC分类号： C23C14/205 , B01J23/6486 , B01J23/6522 , B01J23/6527 , B01J37/0238 , B01J37/34 , H01M4/8621 , H01M4/8871 , H01M4/8878 , H01M4/8882 , H01M4/921 , H01M8/1011 , Y02E60/523 , Y02P70/56
摘要： A catalyst is provided and includes fine catalyst particles of a composition represented by formula (1): PtuRuxTayTz, in which T is at least one element selected from the group consisting of Hf, W, Ni, and V; u, x, y, and z are 10 to 98.9 atm %, 0.1 to 50 atm %, 0.5 to 35 atm %, and 0.5 to 35 atm %, respectively, or formula (2): PtuRuxTayTz, in which T is at least one element selected from the group consisting of Ct, Mo, Nb, Zr, and T; u, x, y, and z are 40 to 70 atm %, 0.1 to 50 atm %, 0.5 to 15 atm %, and 0.5 to 15 atm %, respectively.
摘要翻译： 提供了一种催化剂，其包括由式（1）表示的组合物的微细催化剂颗粒：PtuRuxTayTz，其中T是选自Hf，W，Ni和V中的至少一种元素; u，x，y和z分别为10〜98.9atm％，0.1〜50atm％，0.5〜35atm％，0.5〜35atm％，或式（2）：PtuRuxTayTz，其中T至少为 选自Ct，Mo，Nb，Zr和T的一种元素; u，x，y和z分别为40〜70atm％，0.1〜50atm％，0.5〜15atm％，0.5〜15atm％。
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3.发明授权Method for producing catalyst-layer-supporting substrate, method for producing membrane-electrode assembly and method for producing fuel cell 有权催化剂层支撑基板的制造方法，膜电极接合体的制造方法及燃料电池的制造方法公开(公告)号：US08128986B2
公开(公告)日：2012-03-06
申请号：US12051068
申请日：2008-03-19
申请人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
发明人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
CPC分类号： H01M4/921 , H01M4/881 , H01M4/8871 , H01M4/8878 , H01M4/926 , H01M8/1004 , H01M2008/1095 , Y02P70/56
摘要： A method for producing a catalyst-layer-supporting substrate includes a lamination step of forming a laminate of metal catalyst layers and mixture layers on a substrate by repeating a first step and a second step plural times alternatively; and an acid treatment step of subjecting the laminate to an acid treatment, wherein the first step is a step of sputtering or depositing the metal catalyst layer that comprises a catalyst, and the second step is a step of sputtering or depositing the mixture layer of carbon and metal, the metal of the mixture layer including at least one element M selected from the group consisting of Sn, Al, Cu and Zn.
摘要翻译： 一种催化剂层支撑基板的制造方法包括层叠工序，通过重复第一工序和第二工序，在基板上形成金属催化剂层和混合层的层叠体; 以及对该层压体进行酸处理的酸处理工序，其中，第一工序是溅射或沉积包含催化剂的金属催化剂层的工序，第二工序是溅射或沉积碳化物层 和金属，所述混合物层的金属包括从由Sn，Al，Cu和Zn组成的组中选择的至少一种元素M。
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4.发明授权公开(公告)号：US07579298B2
公开(公告)日：2009-08-25
申请号：US11534804
申请日：2006-09-25
申请人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
发明人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
CPC分类号： H01M4/921 , B01J23/626 , H01M4/8605 , H01M4/926 , H01M8/1007
摘要： Catalysts contain noble metal-containing particles that has a composition except oxygen represented by a formula PtXRuYAZSnS and exhibits a mean particle diameter of from 0.5 nm to 10 nm, both inclusively. A is at least one element selected from a group consisting of Rh, Au, Pd, Ir and Os, and X, Y, Z and S are atomic ratios satisfying relations 30≦X ≦70, 30≦Y≦70, 0≦Z≦40, 0.5≦S≦8 and X+Y+Z+S=100.
摘要翻译： 催化剂含有含有由式PtXRuYAZSnS表示的氧以外的组成的含贵金属的颗粒，其平均粒径均包含0.5nm至10nm。 A是选自Rh，Au，Pd，Ir和Os中的至少一种元素，X，Y，Z和S是满足关系式30 <= X <=70,30≤Y≤70的原子比 ，0 <= Z <= 40，0.5 <= S <= 8，X + Y + Z + S = 100。
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5.发明授权Catalyst for polymer solid electrolyte fuel cell, membrane electrode assembly, and fuel cell 有权用于聚合物固体电解质燃料电池，膜电极组件和燃料电池的催化剂公开(公告)号：US08080347B2
公开(公告)日：2011-12-20
申请号：US12049739
申请日：2008-03-17
申请人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Itsuko Mizutani , Yoshihiko Nakano
发明人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Itsuko Mizutani , Yoshihiko Nakano
CPC分类号： H01M8/1004 , H01M4/921 , H01M4/925
摘要： There is provided a catalyst for a fuel cell, which simultaneously realizes excellent catalytic activity and catalytic stability. The catalyst for a fuel cell comprises a fine particle of a metal represented by formula: PtxRuySizT1u wherein T1 represents at least one element selected from the group consisting of nickel (Ni), tungsten (W), vanadium (V), and molybdenum (Mo); x=30 to 90 atomic %; y=0 to 50 atomic %; z=0.5 to 20 atomic %; and u=0.5 to 40 atomic %, or comprises a fine particle of a metal represented by formula: PtxRuySizT2u wherein T2 represents at least one element selected from the group consisting of hafnium (Hf), tin (Sn), zirconium (Zr), niobium (Nb), titanium (Ti), tantalum (Ta), chromium (Cr), and aluminum (Al); x=30 to 90 atomic %; y=0 to 50 atomic %; z=0.5 to 20 atomic %; and u=0.5 to 40 atomic %.
摘要翻译： 提供了一种用于燃料电池的催化剂，其同时实现优异的催化活性和催化稳定性。 用于燃料电池的催化剂包括由式PtxRuySizT1u表示的金属微粒，其中T1表示选自镍（Ni），钨（W），钒（V）和钼（Mo）中的至少一种元素 ）; x = 30〜90原子％ y = 0〜50原子％ z = 0.5〜20原子％ 并且u = 0.5〜40原子％，或者包含由式PtxRuySizT2u表示的金属微粒，其中，T2表示选自铪（Hf），锡（Sn），锆（Zr）， 铌（Nb），钛（Ti），钽（Ta），铬（Cr）和铝（Al）; x = 30〜90原子％ y = 0〜50原子％ z = 0.5〜20原子％ u = 0.5〜40原子％。
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6.发明申请CATALYST, METHOD FOR PRODUCING CATALYST, MEMBRANE ELECTRODE ASSEMBLY, AND FUEL CELL 有权催化剂，催化剂生产方法，膜电极组件和燃料电池公开(公告)号：US20080233465A1
公开(公告)日：2008-09-25
申请号：US12050497
申请日：2008-03-18
申请人： Itsuko Mizutani , Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
发明人： Itsuko Mizutani , Wu Mei , Taishi Fukazawa , Takahiro Sato , Yoshihiko Nakano
IPC分类号： H01M4/92 , B01J23/26 , B01J23/28 , B01J23/30 , B01J23/46 , C23C14/16 , C23C14/34 , C23C26/00
CPC分类号： C23C14/205 , B01J23/6486 , B01J23/6522 , B01J23/6527 , B01J37/0238 , B01J37/34 , H01M4/8621 , H01M4/8871 , H01M4/8878 , H01M4/8882 , H01M4/921 , H01M8/1011 , Y02E60/523 , Y02P70/56
摘要： A catalyst is provided and includes fine catalyst particles of a composition represented by formula (1): PtuRuxTayTz, in which T is at least one element selected from the group consisting of Hf, W, Ni, and V; u, x, y, and z are 10 to 98.9 atm %, 0.1 to 50 atm %, 0.5 to 35 atm %, and 0.5 to 35 atm %, respectively, or formula (2): PtuRuxTayTz, in which T is at least one element selected from the group consisting of Ct, Mo, Nb, Zr, and T; u, x, y, and z are 40 to 70 atm %, 0.1 to 50 atm %, 0.5 to 15 atm %, and 0.5 to 15 atm %, respectively
摘要翻译： 提供了一种催化剂，并且包括由式（1）表示的组合物的细小催化剂颗粒：Pt z，其中T是选自Hf，W，Ni和V中的至少一种元素; u，x，y和z分别为10〜98.9atm％，0.1〜50atm％，0.5〜35atm％，0.5〜35atm％，或式（2）：Pt 其中T是选自Ct，Mo，Nb，Zr中的至少一种元素，其中T是选自Ct，Mo，Nb，Zr中的至少一种元素 ， 和T; u，x，y，z分别为40〜70atm％，0.1〜50atm％，0.5〜15atm％，0.5〜15atm％
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公开(公告)号：US20060210864A1
公开(公告)日：2006-09-21
申请号：US11374325
申请日：2006-03-14
申请人： Tomoko Eguchi , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
发明人： Tomoko Eguchi , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
CPC分类号： H01M4/90 , H01M4/9075 , H01M4/921 , H01M4/925 , H01M8/1011 , H01M2004/8689 , Y02E60/523
摘要： Disclosed is a catalyst, including a catalyst particle containing at least one component selected from the group consisting of gold, platinum and an gold alloy, the gold alloy containing gold and at least one element selected from transition metal elements of the fourth period, fifth period and sixth period of the Periodic Table, and a catalyst carrier carrying the catalyst particle and containing a perovskite type oxide represented by general formula (1) given below: A(1-x)BxTiOy (1) where the element A is at least one element selected from the group consisting of Ca, Sr and Ba, the element B is at least one element selected from the group consisting of La, Nd, Sm, Eu, Gd, Dy, Ho, Er, Tm, Yb, and Lu, the molar ratio x satisfies 0
摘要翻译： 公开了一种催化剂，其包括含有选自金，铂和金合金中的至少一种成分的催化剂颗粒，含有金的金合金和选自第四周期的第五期的过渡金属元素中的至少一种元素 和第六周期，以及载有催化剂颗粒并含有由下式给出的通式（1）表示的钙钛矿型氧化物的催化剂载体：<？in-line-formula description =“In-line formula”end =“ （1-x）B
（1）<βin-line-formula description =“In-line-formula description” 线型“end =”tail“？>其中元素A为选自Ca，Sr和Ba中的至少一种元素，元素B为选自La，Nd，Sm中的至少一种元素 ，Eu，Gd，Dy，Ho，Er，Tm，Yb和Lu，摩尔比x满足0 -
8.发明授权Process for producing membrane electrode assembly, and fuel cell using the membrane electrode assembly produced by the process 有权用于生产膜电极组件的方法，以及使用通过该方法生产的膜电极组件的燃料电池公开(公告)号：US07931935B2
公开(公告)日：2011-04-26
申请号：US12049770
申请日：2008-03-17
申请人： Masaaki Yamamoto , Wu Mei , Tsuyoshi Kobayashi , Taishi Fukazawa , Itsuko Mizutani , Yoshihiko Nakano
发明人： Masaaki Yamamoto , Wu Mei , Tsuyoshi Kobayashi , Taishi Fukazawa , Itsuko Mizutani , Yoshihiko Nakano
CPC分类号： H01M8/1004 , C23C14/185 , H01M4/8878 , H01M4/8882 , H01M4/921 , H01M8/1011 , Y02E60/366 , Y02E60/523 , Y02P70/56
摘要： This invention provides a process for producing a membrane electrode assembly which has high and stable catalytic activity, and suppressed deterioration in catalytic activity during operation, and can prevent a deterioration in performance attributable to a structural factor of the membrane electrode assembly. The process comprises the step of, after the washing/removing step, drying the catalyst electrode in an atmosphere having a lower oxygen partial pressure than the air. The anode/cathode is a covered catalyst electrode having a structure formed by supporting/depositing a catalytically active material composed mainly of platinum/ruthenium subjected to the potential holding step, the washing/removing step, and the drying step, on a porous electroconductive carrier to cover at least a part of the porous electroconductive carrier with the ion conductive material.
摘要翻译： 本发明提供了具有高且稳定的催化活性的电极组件的制造方法，抑制了操作时的催化活性的劣化，能够防止膜电极接合体的结构因素引起的性能的劣化。 该方法包括以下步骤：在洗涤/除去步骤之后，在氧气分压低于空气的气氛中干燥催化剂电极。 阳极/阴极是具有通过在多孔导电载体上负载/沉积主要由经受电位保持步骤的铂/钌，洗涤/去除步骤和干燥步骤的催化活性材料形成的结构的被覆催化剂电极 用离子导电材料覆盖多孔导电载体的至少一部分。
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公开(公告)号：US07862932B2
公开(公告)日：2011-01-04
申请号：US12423313
申请日：2009-04-14
申请人： Tomoko Eguchi , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
发明人： Tomoko Eguchi , Yoshihiko Nakano , Wu Mei , Taishi Fukazawa
CPC分类号： H01M4/90 , H01M4/9075 , H01M4/921 , H01M4/925 , H01M8/1011 , H01M2004/8689 , Y02E60/523
摘要： Disclosed is a catalyst, including a catalyst particle containing at least one component selected from the group consisting of gold, platinum and an gold alloy, the gold alloy containing gold and at least one element selected from transition metal elements of the fourth period, fifth period and sixth period of the Periodic Table, and a catalyst carrier carrying the catalyst particle and containing a perovskite type oxide represented by general formula (1) given below: A(1-x)BxTiOy (1) where the element A is at least one element selected from the group consisting of Ca, Sr and Ba, the element B is at least one element selected from the group consisting of La, Nd, Sm, Eu, Gd, Dy, Ho, Er, Tm, Yb, and Lu, the molar ratio x satisfies 0
摘要翻译： 公开了一种催化剂，其包括含有选自金，铂和金合金中的至少一种成分的催化剂颗粒，含有金的金合金和选自第四周期的第五期的过渡金属元素中的至少一种元素 和第六周期，以及载有催化剂颗粒并含有下列通式（1）表示的钙钛矿型氧化物的催化剂载体：A（1-x）BxTiOy（1）其中元素A为至少一种 元素B选自由La，Nd，Sm，Eu，Gd，Dy，Ho，Er，Tm，Yb和Lu组成的组中的至少一种元素， 摩尔比x满足0
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公开(公告)号：US07727930B2
公开(公告)日：2010-06-01
申请号：US11737393
申请日：2007-04-19
申请人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Itsuko Mizutani , Tsuyoshi Kobayashi , Yoshihiko Nakano
发明人： Wu Mei , Taishi Fukazawa , Takahiro Sato , Itsuko Mizutani , Tsuyoshi Kobayashi , Yoshihiko Nakano
CPC分类号： H01M4/921 , B82Y30/00 , H01M4/926 , H01M8/1004 , H01M2008/1095 , Y02P70/56
摘要： A catalyst includes a conductive carrier and catalyst particles. The catalyst particles are supported on the conductive carrier and have a composition represented by formula 1, below. An area of a peak derived from a metal bond of a T-element is 15% or more of an area of a peak derived from an oxygen bond of the T-element in a spectrum obtained by X-ray photoelectron spectroscopic method. PtxRuyTz (1) where the T-element is at least one element selected from the group consisting of V, Nb and Hf, x is 30 to 60 at. %, y is 20 to 50 at. % and z is 5 to 50 at. %.
摘要翻译： 催化剂包括导电载体和催化剂颗粒。 催化剂颗粒负载在导电载体上，并具有由下式1表示的组成。 衍生自T元件的金属键的峰的面积是通过X射线光电子分光法获得的光谱中由T元素的氧键衍生的峰的面积的15％以上。 PtxRuyTz（1）其中T元素是选自V，Nb和Hf中的至少一种元素，x为30至60at。 ％，y为20至50 at。 ％，z为5〜50at。 ％。
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