Compositions containing 2-acetyl-1-pyrroline
    3.
    发明授权
    Compositions containing 2-acetyl-1-pyrroline 失效
    含有2-乙酰基-1-吡咯啉的组合物

    公开(公告)号:US5512290A

    公开(公告)日:1996-04-30

    申请号:US364310

    申请日:1994-12-27

    摘要: A powder-form composition of 2-acetyl-1-pyrroline incorporated with a support of maltodextrin and/or cyclodextrin. The composition is prepared by hydrolyzing a 2-(1-alkoxyethenyl)-1-pyrroline with an acid to obtain a reaction medium, adding an equimolar amount of a base to the reaction medium to obtain a neutralized reaction medium containing 2-acetyl-1-pyrroline, combining maltodextrin and/or cyclodextrin with the neutralized reaction medium to obtain a support solution and freeze-drying the support solution to obtain the composition.

    摘要翻译: 加入麦芽糖糊精和/或环糊精的载体的2-乙酰基-1-吡咯啉的粉末状组合物。 通过用酸水解2-(1-烷氧基乙烯基)-1-吡咯啉来制备组合物以获得反应介质,向反应介质中加入等摩尔量的碱,得到中和的含有2-乙酰基-1 - 吡咯啉,将麦芽糖糊精和/或环糊精与中和的反应介质结合,得到载体溶液并冷冻干燥载体溶液以获得组合物。

    Anisotropic compounds having nematic phase and liquid crystal mixtures
    7.
    发明授权
    Anisotropic compounds having nematic phase and liquid crystal mixtures 失效
    具有向列相和液晶混合物的各向异性化合物

    公开(公告)号:US5179101A

    公开(公告)日:1993-01-12

    申请号:US477490

    申请日:1990-02-09

    摘要: Anisotropic compounds having a nematic phase have the formula ##STR1## wherein A is a cyclic radical selected from the group consisting of ##STR2## Z is selected from the group consisting of a single bond, a --CH2CH2-- group, a methyleneoxy group and an oxymethylene group,n is 1 or 2,p is 0, 1, or 2,r is 0 or 1,X is selected from the group consisting of fluorine, chlorine, bromine, iodine, nitrile and methyl,R.sup.1 and R.sup.2 are selected from the group consisting of hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.1 -C.sub.12 -alkoxy, C.sub.1 -C.sub.12 -alkanoyloxy and C.sub.1 -C.sub.12 -alkylamino and cyclic groups of the formulas ##STR3## wherein R.sup.3 through R.sup.6 are selected from the group consisting of hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.1 -C.sub.12 -alkoxy, C.sub.1 -C.sub.12 -alkanoyloxy, and C.sub.1 -C.sub.12 -alkylamino, and Z.sup.2 through Z.sup.6 represent a Z group, with the provisos that:(A) none of the above aromatic radicals (10), (11), (13), (14) or (15) is directly bonded to the C-atom of a methyleneoxy or oxymethylene group; and(B) at least one X group is methyl when only one or none of the groups R.sup.1 and R.sup.2 is a cyclic radical of formulas (13) or (16), A has the formula (12), Z is a single bond, and any of Z.sup.3 or Z.sup.6, if present, is a single bond.Compounds having the defined lateral substituents on the rings have a reduced tendency to form smectic phases as compared with the compounds not having such lateral substituents.

    摘要翻译: 具有向列相的各向异性化合物具有式(1)其中A是选自下列的环状基团:(1)Z(Z)选自 n是1或2,p是0,1或2,r是0或1,X选自由以下组成的组: 氟,氯,溴,碘,腈和甲基,R 1和R 2选自氢,C 1 -C 12 - 烷基,C 1 -C 12 - 烷氧基,C 1 -C 12 - 烷酰氧基和C 1 -C 12烷基氨基和环基 (16)其中R 3至R 6选自氢,C 1 -C 12 - 烷基,C 1 -C 12 - 烷基,(C 1 -C 12)烷基, 烷氧基,C 1 -C 12烷酰氧基和C 1 -C 12烷基氨基,Z 2至Z 6表示Z基团,条件是:(A)上述芳族基团(10),(11),(13), (14)或(15)直接键合到亚甲基氧基的C原子上 氧亚甲基; 和(B)至少一个X基团是甲基,当基团R 1和R 2中的一个或没有一个是式(13)或(16)的环基时,A具有式(12),Z是单键, Z 3或Z 6中的任何一个(如果存在)是单键。 与不具有这种侧面取代基的化合物相比,在环上具有限定的侧面取代基的化合物具有降低的形成近晶相的倾向。

    Food flavorant preparation via bioconversion of elemental sulphur
    9.
    发明授权
    Food flavorant preparation via bioconversion of elemental sulphur 失效
    通过元素硫生物转化的食品调味剂制剂

    公开(公告)号:US5948453A

    公开(公告)日:1999-09-07

    申请号:US756497

    申请日:1996-11-26

    IPC分类号: A23L27/21 C12P11/00 B32B3/14

    CPC分类号: C12P11/00 A23L27/215

    摘要: A flavorant agent is prepared by incubating a medium of baker's yeast, elemental sulfur and a reducing sugar to obtain a reaction medium from which hydrogen sulfide gas evolves and then the reaction medium is treated with heat to obtain the flavorant agent. A further flavorant agent is obtained by separating the supernatant of the reaction medium from reaction medium residue, and the reaction medium or supernatant may be mixed with a flavor precursor material and heated to obtain a flavorant composition.

    摘要翻译: 通过培养面包酵母,元素硫和还原糖的培养基来制备调味剂,以获得产生硫化氢气体的反应介质,然后加热处理反应介质以获得风味剂。 通过将反应介质的上清液从反应介质残留物中分离得到另外的调味剂,并且将反应介质或上清液与调味剂前体材料混合并加热以获得食用香料组合物。