摘要:
The present invention provides a process for the production of glyoxals which comprises effecting the oxidative dehydrogenation of a glycol at a temperature of 400.degree. to 700.degree. C. in the presence of a silver-based catalyst composed of silver and at least one element selected from the group consisting of gold, platinum, rhodium and palladium, and phosphorus or a phosphorus compound, as well as such catalysts. These process and catalysts make it possible to produce high-quality glyoxals in high yield and with industrial advantages while minimizing the contents of unreacted raw material and reaction intermediates such as glycolaldehyde and acetol.
摘要:
There is disclosed a process for producing silanes by reducing polyhalosilane with a mixture of alkyl aluminum hydride and trialkyl aluminum, in which a treatment for reducing the content of trialkyl aluminum in the mixture is lowered to 10 mol. % or less of alkyl aluminum hydride prior to the reduction reaction.As to methods for reducing the content of trialkyl aluminum in the mixture, there are provided, for example, distillation, recrystallization, separation by complex formation, pyrolysis of trialkyl aluminum and decomposition by hydrogenation of trialkyl aluminum.
摘要:
There is disclosed a process for producing germanes by reducing germanium halide with a mixture of alkylaluminum hydride and trialkylaluminum, in which a treatment for reducing the content of trialkylaluminum in the mixture to 10 mol. % or less relative to the alkylaluminum hydride is carried out prior to the reduction reaction. As to the treatment for reducing the content of trialkylaluminum in the mixture, there are provided, for example, distillation, recrystallization, complex formation followed by separation, pyrolysis and decomposition by hydrogenation and addition of alkylaluminum halide to said mixture.
摘要:
Sinterable crystalline aluminum nitride powder is produced by reacting alkyl aluminum with ammonia in a gas phase to produce an amorphous aluminum nitride presursor powder, and subjecting the precursor powder to a primary calcination in a reducing gas containing at least 20% (vol.) ammonia at 600.degree. C. to 1300.degree. C., and then subjecting the calcined aluminum nitride to a secondary calination in an inert gas or a reducing gas at 1400.degree.-1750.degree. C.
摘要:
A method for preparing high-purity aluminum nitride having high thermal conductivity and heat resistance for aluminum nitride substrates, which comprises the steps of reacting an organic aluminum compound with an aminotriazine in a solvent to obtain an aluminum nitride precursor, separating the precursor from the solvent, and heating the precursor at a temperature of 600.degree. C. or more in a reducing atmosphere and/or a non-oxidizing atmosphere. An aluminum nitride sinter is prepared by, if necessary, adding a sintering auxiliary to the above aluminum nitride powder, molding the powder into a desired shape, and then sintering the molded material at a temperature of 1,600.degree. to 2,000.degree. C. in a non-oxidizing atmosphere.
摘要:
A method for preparing high-purity aluminum nitride having high thermal conductivity and heat resistance for aluminum nitride substrates, which comprises the steps of reacting an organic aluminum compound with an aminotriazine in a solvent to obtain an aluminum nitride precursor, separating the precursor form the solvent, and heating the precursor at a temperature of 600.degree. C. or more in a reducing atmosphere and/or a non-oxidizing atmosphere. An aluminum nitride sinter is prepared by, if necessary, adding a sintering auxiliary to the above aluminum nitride powder, molding the powder into a desired shape, and then sintering the molded material at a temperature of 1,600.degree. to 2,000.degree. C. in a non-oxidizing atmosphere.
摘要:
An electronic device including: a thin-film substrate having a front surface being formed with electronic circuits; an adhesive layer comprising an adhesive material applied to a back surface of the thin-film substrate, the adhesive material having an elasticity modulus being in a range of 1.0×103 to 2.1×104 Pa at 80° C.; and a flexible substrate having a front surface being bonded to the back surface of the thin-film substrate with the adhesive layer.
摘要:
According to an embodiment, a tracking drive type solar power generation apparatus (1) includes a tracking control portion (20) having a tilt drive portion (21) that controls the tilt position of a module panel (10) (a driving solar cell module (12) and juxtaposition solar cell modules (13) supported by main beam members 22), a swivel drive portion (25) that controls the swivel position of the module panel (10), and a tracking control base (20c) to which the tilt drive portion (21) and the swivel drive portion (25) are integrally connected. The driving solar cell module (12) includes, in a middle thereof in a length direction, inside a bottom plate portion (14b) thereof, a tilt drive housing portion (17) in which the tilt drive portion (21) is housed. A tilt rotation axis (21s) serving as the center of rotation of the tilt drive portion (21) is disposed on the same side with respect to the bottom plate portion (14b) as the center of gravity (CG) of the driving solar cell module (12).
摘要:
Disclosed is a key generator, which assures the security of a key by preventing a circuit designer and other persons from readily knowing the value of the key. Random number generator circuits (51, 52, 53 and so on) generate random numbers respectively in accordance with different clocks (CLK1, CLK2, CLK3, and so on). An arithmetic circuit (59) operates on the random numbers generated from the random number generator circuits (51, 52, 53 and so on) to generate an N-bit random number RA as the output from a random number generator (50). This N-bit random number is RA acquired via a key selector (43), and latched into a key register (45) in accordance with an acquisition enable signal EN from a timing monitoring counter (47), which is driven by a clock CLKA other than clocks CLK1, CLK2, CLK3, and so on, to obtain a hardware key, which is a unique secret key.
摘要:
A liquid crystal display, and a method of manufacturing the same, the display including a substrate; a pixel electrode on the substrate; a pixel isolator surrounding the pixel electrode, the pixel isolator being formed by an insulator. The display also includes a liquid crystal layer on the pixel electrode surrounded by the pixel isolator; a common electrode on the liquid crystal layer; and a counter substrate on the common electrode.