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1.发明申请FLOW CELL FOR MEASURING ELECTROMAGNETIC RADIATION ABSORPTION SPECTRA IN A CONTINUOUSLY FLOWING IMMISCIBLE LIQUID(S) OR LIQUIDS WITH ENTRAINED GAS PHASES 有权用于测量电磁辐射吸收光谱的流动池在连续流动的可渗透液体（液体）或液体中与入口气相公开(公告)号：US20130061657A1
公开(公告)日：2013-03-14
申请号：US13231276
申请日：2011-09-13
申请人： Mark Erik Nelson , Arkady Samuilovich Dykman , Andrey Vladimirovich Zinenkov , Alexey Leonidovich Moskvin , Lubov Borisovna Drozdova
发明人： Mark Erik Nelson , Arkady Samuilovich Dykman , Andrey Vladimirovich Zinenkov , Alexey Leonidovich Moskvin , Lubov Borisovna Drozdova
CPC分类号： G01N21/85 , G01N21/05 , G01N21/645 , G01N30/74 , G01N2021/0346 , G01N2021/651 , G01N2021/8557 , G01N2201/08
摘要： An apparatus and method for spectral analysis of immiscible phases are disclosed. A flow cell for online absorption measurements of immiscible process phases can comprise: a body containing an inlet window and an outlet window in operable communication with a measurement instrument; and a series of partitions that divide the inside of the flow cell into three (3) or more vessels that have an inlet and an outlet, wherein the vessels are connected in series with one another. Optionally, the first vessel is equipped with a porous membrane to facilitate the separation of immiscible process phases.
摘要翻译： 公开了一种用于不混溶相的光谱分析的装置和方法。 用于不混溶过程相的在线吸收测量的流动池可以包括：主体，其包含与测量仪器可操作地连通的入口窗口和出口窗口; 以及将流动池内部分成具有入口和出口的三（3）个或更多个容器的一系列隔板，其中容器彼此串联连接。 任选地，第一容器装备有多孔膜以便于分离不混溶的工艺阶段。
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2.发明授权Flow cell for measuring electromagnetic radiation absorption spectra in a continuously flowing immiscible liquid(s) or liquids with entrained gas phases 有权用于测量连续流动的不混溶液体或带夹带气相的液体中的电磁辐射吸收光谱的流通池公开(公告)号：US08663562B2
公开(公告)日：2014-03-04
申请号：US13231276
申请日：2011-09-13
申请人： Mark Erik Nelson , Arkady Samuilovich Dykman , Andrey Vladimirovich Zinenkov , Alexey Leonidovich Moskvin , Lubov Borisovna Drozdova
发明人： Mark Erik Nelson , Arkady Samuilovich Dykman , Andrey Vladimirovich Zinenkov , Alexey Leonidovich Moskvin , Lubov Borisovna Drozdova
CPC分类号： G01N21/85 , G01N21/05 , G01N21/645 , G01N30/74 , G01N2021/0346 , G01N2021/651 , G01N2021/8557 , G01N2201/08
摘要： An apparatus and method for spectral analysis of immiscible phases are disclosed. A flow cell for online absorption measurements of immiscible process phases can comprise: a body containing an inlet window and an outlet window in operable communication with a measurement instrument; and a series of partitions that divide the inside of the flow cell into three (3) or more vessels that have an inlet and an outlet, wherein the vessels are connected in series with one another. Optionally, the first vessel is equipped with a porous membrane to facilitate the separation of immiscible process phases.
摘要翻译： 公开了一种用于不混溶相的光谱分析的装置和方法。 用于不混溶过程相的在线吸收测量的流动池可以包括：主体，其包含与测量仪器可操作地连通的入口窗口和出口窗口; 以及将流动池内部分成具有入口和出口的三（3）个或更多个容器的一系列隔板，其中容器彼此串联连接。 任选地，第一容器装备有多孔膜以便于分离不混溶的工艺阶段。
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3.发明授权Transparent and high-heat polycarbonate-polysiloxane copolymers and transparent blends with polycarbonate and a process for preparing same 有权透明和高热聚碳酸酯 - 聚硅氧烷共聚物和与聚碳酸酯的透明共混物及其制备方法公开(公告)号：US07232865B2
公开(公告)日：2007-06-19
申请号：US10797418
申请日：2004-03-10
申请人： James Louis DeRudder , Niles Richard Rosenquist , Gary Charles Davis , Matthew Robert Pixton , Mark Erik Nelson , Zhaohui Su
发明人： James Louis DeRudder , Niles Richard Rosenquist , Gary Charles Davis , Matthew Robert Pixton , Mark Erik Nelson , Zhaohui Su
IPC分类号： C08F20/00
CPC分类号： C08L83/10 , C08G64/186 , C08G64/24 , C08G77/448 , C08L69/00 , C08L2666/02 , C08L2666/18
摘要： A method is provided for making siloxane polycarbonate copolymers and blends of other polycarbonates with such copolymers wherein the copolymers and blends have excellent transparency and physical characteristic.
摘要翻译： 提供了制备硅氧烷聚碳酸酯共聚物和其它聚碳酸酯与这种共聚物的共混物的方法，其中共聚物和共混物具有优异的透明度和物理特性。
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4.发明授权Copolyestercarbonates derived from dimer acids and method for their preparation 有权衍生自二聚酸的共聚酯碳酸酯及其制备方法公开(公告)号：US06433127B1
公开(公告)日：2002-08-13
申请号：US09745169
申请日：2000-12-20
IPC分类号： C08G6400
CPC分类号： C08G63/64
摘要： Copolyestercarbonates comprising carbonate structural units derived from at least one dihydroxyaromatic compound, preferably bisphenol A, and ester units derived from a dihydroxyaromatic compound and a composition comprising at least one C36 dimer acid may be prepared by an interfacial phosgenation method conducted at a pH in the range of about 9-11. The copolyestercarbonates have properties which are often superior to those of corresponding polymers prepared, for example, from dodecanedioic acid.
摘要翻译： 包含衍生自至少一种二羟基芳族化合物，优选双酚A的碳酸酯结构单元和衍生自二羟基芳族化合物的酯单元和包含至少一种C36二聚酸的组合物的共聚酯碳酸酯可以通过在pH范围内进行的界面光气化方法 约9-11。 共聚酯碳酸酯具有通常优于由例如十二烷二酸制备的相应聚合物的性质。
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公开(公告)号：US20100145103A1
公开(公告)日：2010-06-10
申请号：US12633737
申请日：2009-12-08
申请人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
发明人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
IPC分类号： C07C45/78
摘要： A method for purifying a crude acetone raw material containing low molecular weight impurities using three columns in sequence is disclosed. The method comprises the steps of feeding the crude acetone raw material into a first column; adding an alkaline reagent and an oxidative reagent into the first column; feeding the first bottom fraction to a second rectification column; optionally adding an alkaline reagent to the second column above the charge point of the bottom fraction; separating a purified acetone from the high molecular weight impurities and removing the purified acetone as a top fraction by distillation in the second column, thereby forming a second bottom fraction comprising an acetone mixture comprising high molecular weight impurities; feeding the second bottom fraction comprising the acetone mixture to a third rectification column; removing a top fraction from the third column; and returning the top fraction removed from the third column to the first column, wherein the second rectification column is operated at atmospheric pressure, and wherein the purified acetone has an acetaldehyde level of less than 5 ppm and a KT-Test time of greater than 11 hours, as measured by the SABIC KT-Test method.
摘要翻译： 公开了一种使用三列依次纯化含有低分子量杂质的粗丙酮原料的方法。 该方法包括将粗丙酮原料进料到第一塔中的步骤; 在第一塔中加入碱性试剂和氧化试剂; 将第一底部馏分送入第二精馏塔; 任选地在底部馏分的充电点上方的第二塔中加入碱性试剂; 将纯化的丙酮与高分子量杂质分离，并在第二塔中通过蒸馏除去纯化的丙酮作为顶级馏分，由此形成包含含有高分子量杂质的丙酮混合物的第二塔底馏分; 将包含丙酮混合物的第二底部馏分进料至第三精馏塔; 从第三列移除顶部馏分; 并将从第三塔取出的顶馏分返回到第一塔，其中第二精馏塔在大气压下运行，其中纯化丙酮的乙醛水平小于5ppm，KT-测试时间大于11 小时，由SABIC KT-Test方法测量。
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公开(公告)号：US6096900A
公开(公告)日：2000-08-01
申请号：US418871
申请日：1999-10-15
IPC分类号： C07D209/48
CPC分类号： C07D209/48
摘要： A method for the solventless synthesis of a phthalimide or phthalimide mixture is provided comprising contacting at least one amine reactant and at least one anhydride reactant in a solventless environment at a first temperature sufficient to allow the reactants to at least partially condense; and increasing the temperature to a second temperature sufficient to melt the reaction mixture, thereby allowing the reaction to go essentially to completion and form the reaction product.
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公开(公告)号：US08058479B2
公开(公告)日：2011-11-15
申请号：US12633737
申请日：2009-12-08
申请人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
发明人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
IPC分类号： C07C45/78
摘要： A method for purifying a crude acetone raw material containing low molecular weight impurities using three columns in sequence is disclosed. The method comprises the steps of feeding the crude acetone raw material into a first column; adding an alkaline reagent and an oxidative reagent into the first column; feeding the first bottom fraction to a second rectification column; optionally adding an alkaline reagent to the second column above the charge point of the bottom fraction; separating a purified acetone from the high molecular weight impurities and removing the purified acetone as a top fraction by distillation in the second column, thereby forming a second bottom fraction comprising an acetone mixture comprising high molecular weight impurities; feeding the second bottom fraction comprising the acetone mixture to a third rectification column; removing a top fraction from the third column; and returning the top fraction removed from the third column to the first column, wherein the second rectification column is operated at atmospheric pressure, and wherein the purified acetone has an acetaldehyde level of less than 5 ppm and a KT-Test time of greater than 11 hours, as measured by the SABIC KT-Test method.
摘要翻译： 公开了一种使用三列依次纯化含有低分子量杂质的粗丙酮原料的方法。 该方法包括将粗丙酮原料进料到第一塔中的步骤; 在第一塔中加入碱性试剂和氧化试剂; 将第一底部馏分送入第二精馏塔; 任选地在底部馏分的充电点上方的第二塔中加入碱性试剂; 将纯化的丙酮与高分子量杂质分离，并在第二塔中通过蒸馏除去纯化的丙酮作为顶级馏分，由此形成包含含有高分子量杂质的丙酮混合物的第二塔底馏分; 将包含丙酮混合物的第二底部馏分进料至第三精馏塔; 从第三列移除顶部馏分; 并将从第三塔取出的顶馏分返回到第一塔，其中第二精馏塔在大气压下运行，其中纯化丙酮的乙醛水平小于5ppm，KT-测试时间大于11 小时，由SABIC KT-Test方法测量。
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8.发明授权Diaminoalkyl quaternary ammonium salts and method for their preparation and use 失效二氨基烷基季铵盐及其制备和使用方法
公开(公告)号：US5821322A
公开(公告)日：1998-10-13
申请号：US851260
申请日：1997-05-05
申请人： Daniel Joseph Brunelle , Peter David Phelps , Eugene Pauling Boden , Mark Erik Nelson , Larry Ivis Flowers , Paul Dean Sybert , Erik Hendrick Adriaan Capelle
发明人： Daniel Joseph Brunelle , Peter David Phelps , Eugene Pauling Boden , Mark Erik Nelson , Larry Ivis Flowers , Paul Dean Sybert , Erik Hendrick Adriaan Capelle
IPC分类号： C07D295/02 , B01J31/02 , C07B61/00 , C07C68/02 , C07C69/96 , C07C209/12 , C07C211/63 , C07D295/13 , C08G64/22 , C08G64/24 , C08G64/00
CPC分类号： C07D295/13 , C07C211/63 , C08G64/24
摘要： Diaminoalkyl quaternary ammonium salts are prepared by the reaction of alkyl halides with tertiary diamines having C.sub.2-20 primary alkyl radicals attached to nitrogen and an alkyl radical between the two nitrogen atoms in which at least three carbon atoms separate said nitrogen atoms. Said salts are preferably substantially free from corresponding diamines. They are useful as catalysts for interfacial polycarbonate preparation by the reaction of phosgene with at least one dihydroxyaromatic compound. Polycarbonate preparation using such catalysts is economical in phosgene consumption, is accompanied by a rapid conversion of chloroformate groups to desirable species and affords a product with a very low proportion of unreacted dihydroxyaromatic compound.
摘要翻译： 二氨基烷基季铵盐通过烷基卤与与氮连接的具有C2-20伯烷基的叔二胺和两个氮原子之间的烷基与其中至少三个碳原子分开所述氮原子的烷基反应来制备。 所述盐优选基本上不含相应的二胺。 它们可用作通过光气与至少一种二羟基芳族化合物反应的界面聚碳酸酯制备的催化剂。 使用这种催化剂的聚碳酸酯制备在光气消耗中是经济的，伴随着氯甲酸酯基团快速转化为所需物质并提供具有非常低比例的未反应的二羟基芳族化合物的产物。
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公开(公告)号：US08741109B2
公开(公告)日：2014-06-03
申请号：US12633746
申请日：2009-12-08
申请人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
发明人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
摘要： A method for purifying a crude acetone raw material containing low molecular weight impurities using two columns is disclosed. Crude acetone raw material is fed into a first column; adding an alkaline reagent and an oxidative agent into the first column to form high molecular weight impurities; removing a top fraction from the first column by distillation to form bottom fraction containing an acetone mixture containing high molecular weight impurities; feeding the bottom fraction containing the acetone mixture obtained to a second rectification column at a charge point on the column; adding an alkaline reagent to the second column above the charge point of the bottom fraction fed; and separating a purified acetone from the high molecular weight impurities and removing the purified acetone as a top fraction by distillation in the second column, wherein the second rectification column is operated at atmospheric pressure.
摘要翻译： 公开了使用两列纯化含有低分子量杂质的粗丙酮原料的方法。 将粗丙酮原料送入第一塔; 向第一塔中加入碱性试剂和氧化剂以形成高分子量杂质; 通过蒸馏从顶部馏分中除去顶部馏分以形成含有含有高分子量杂质的丙酮混合物的底部馏分; 将所获得的含有丙酮混合物的塔底馏分在柱上的充电点向第二精馏塔进料; 向供给的底部馏分的充电点以上的第二塔加入碱性试剂; 并将纯化的丙酮与高分子量杂质分离，并在第二塔中通过蒸馏除去纯化的丙酮作为顶级馏分，其中第二精馏塔在大气压下运行。
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公开(公告)号：US20100140075A1
公开(公告)日：2010-06-10
申请号：US12633746
申请日：2009-12-08
申请人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
发明人： Mark Erik Nelson , Andrey Yurievich Sokolov , Ilya Yurievich Krupenko , Valery Yurievich Aristovich
摘要： A method for purifying a crude acetone raw material containing low molecular weight impurities using two columns is disclosed. The method comprises the steps of feeding the crude acetone raw material into a first column; adding an alkaline reagent and an oxidative agent into the first column to form high molecular weight impurities; removing a top fraction from the first column by distillation to form bottom fraction comprising an acetone mixture comprising high molecular weight impurities; feeding the bottom fraction comprising the acetone mixture obtained to a second rectification column at a charge point on the column; adding an alkaline reagent to the second column above the charge point of the bottom fraction fed; and separating a purified acetone from the high molecular weight impurities and removing the purified acetone as a top fraction by distillation in the second column, wherein the second rectification column is operated at atmospheric pressure.
摘要翻译： 公开了使用两列纯化含有低分子量杂质的粗丙酮原料的方法。 该方法包括将粗丙酮原料进料到第一塔中的步骤; 向第一塔中加入碱性试剂和氧化剂以形成高分子量杂质; 通过蒸馏从顶部馏分中除去顶部馏分以形成包含含有高分子量杂质的丙酮混合物的底馏分; 将所获得的包含丙酮混合物的塔底馏分在柱上的充电点进料至第二精馏塔; 向供给的底部馏分的充电点以上的第二塔加入碱性试剂; 并将纯化的丙酮与高分子量杂质分离，并在第二塔中通过蒸馏除去纯化的丙酮作为顶级馏分，其中第二精馏塔在大气压下运行。
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