PREPARING POLYESTER ALCOHOLS
    10.
    发明申请
    PREPARING POLYESTER ALCOHOLS 审中-公开
    制备聚酯醇

    公开(公告)号:US20120059143A1

    公开(公告)日:2012-03-08

    申请号:US13227068

    申请日:2011-09-07

    IPC分类号: C08G63/80 C08G63/668

    摘要: The subject of the present invention is a process for preparing polyester alcohols by condensation of polytetrahydrofuran with aromatic dicarboxylic acids and/or their anhydrides in the presence of a transesterification catalyst in a multi-stage operation at different pressure levels with at least one reaction stage at atmospheric pressure and at least one reaction stage at reduced pressure, where distillate is removed from the reaction system, which process comprises heating the reaction mixture in two or more phases in the atmospheric-pressure reaction stage wherein the heating phases are interrupted by at least one phase in which the temperature is kept constant.

    摘要翻译: 本发明的主题是通过在不同压力水平的多级操作中在酯交换催化剂存在下,将聚四氢呋喃与芳族二羧酸和/或它们的酸酐缩合制备聚酯醇的方法,其中至少一个反应阶段在 大气压力和至少一个反应阶段,其中从反应体系中除去馏出物,该方法包括在大气压反应阶段中将反应混合物加热至两相或更多阶段,其中加热阶段被至少一个 温度保持恒定的相。