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公开(公告)号：US4277283A
公开(公告)日：1981-07-07
申请号：US971829
申请日：1978-12-19
CPC分类号： C23C30/005 , C22C1/051 , C22C29/04 , C22C29/06
摘要： This invention relates to a sintered hard metal for cutting tools and having excellent wear resistance, resistance to thermal deformation, mechanical strength and the like. The present invention resides in the fact that the substrate metal consists of a rich content of the B-1 type hard phase and the surface thin layer consists of a rich content of the ordinary tungsten carbide. B-1 type crystal structure contains one or more Group IVa, Va and VIa metals, carbon, nitrogen and, moreover, tungsten. The thin layer structure has the layer of 5 to 200.mu. thickness on the surface thereof.
摘要翻译： 本发明涉及一种用于切割工具的烧结硬质金属，具有优异的耐磨性，耐热变形性，机械强度等。 本发明的目的在于，基底金属由丰富的B-1型硬质相组成，表面薄层由富含普通碳化钨组成。 B-1型晶体结构含有一种或多种IVa，Va和VIa族金属，碳，氮，以及钨。 薄层结构在其表面上具有5至200μm厚度的层。
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2.发明授权Surface-coated cemented carbide article and a process for the production thereof 失效表面硬化硬质合金制品及其制造方法
公开(公告)号：US4150195A
公开(公告)日：1979-04-17
申请号：US806880
申请日：1977-06-15
申请人： Masaaki Tobioka , Mitsuo Kodama , Minol Nakano , Takeshi Asai , Takaharu Yamamoto , Akio Hara
发明人： Masaaki Tobioka , Mitsuo Kodama , Minol Nakano , Takeshi Asai , Takaharu Yamamoto , Akio Hara
CPC分类号： B23B27/148 , B22F7/04 , C23C16/30 , C23C16/32 , C23C16/34 , C23C16/40 , C23C16/403 , C23C16/405 , C23C30/005 , Y10T428/12028 , Y10T428/12146 , Y10T428/12549 , Y10T428/12576
摘要： This invention relates to surface-coated cemented carbide articles having a monolayer or multilayer consisting of one or more materials selected from oxides, carbides, nitrides and mixtures or compounds thereof, the most interior layer, in contact with the surface of the cemented carbide substrate, consisting of one or more materials selected from carbides and carbonitrides of Group IVa, Va and VIa elements, wherein the thickness of a decarburized layer (.eta. phase) present between the cemented carbide substrate and most interior coating layer is 0.5 micron or less in a case where the curvature of the interface is zero and the lattice constant of the binder metal of the coated cemented carbide article, as a mean value from the interface to 50 microns, is not more than that of the iron group metal solid solution by 0.005 A or more.
摘要翻译： 本发明涉及具有由选自氧化物，碳化物，氮化物及其混合物或化合物的一种或多种材料组成的单层或多层的表面涂覆的硬质合金制品，与硬质合金基体的表面接触的最内层， 由选自Ⅳa族，Ⅴa和Ⅵa族元素的碳化物和碳氮化物的一种或多种材料组成，其中在硬质合金基底和最内部涂层之间存在的脱碳层（eta相）的厚度在0.5微米以下 其中界面的曲率为零，并且作为从界面到50微米的平均值的涂覆的硬质合金制品的粘合剂金属的晶格常数不大于铁族金属固溶体的晶格常数0.005A或 更多。
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公开(公告)号：US4279651A
公开(公告)日：1981-07-21
申请号：US974512
申请日：1978-12-28
CPC分类号： C22C29/00
摘要： The invention relates to a sintered hard metal having a high wear resistance and heat resistance as material for cutting tools and wear resistant tools and the method for producing the same. The sintered hard metal has a hard phase comprising a phase having a B-1 type crystal structure containing more than one kind of IVa, Va and VIa group metals in the Periodic Table and also the elements, carbon, nitrogen and oxygen and a WC phase, the hard phase and a bonding phase chiefly consisting of a ferrous metal which is sintered by a powder metallurgy technique, whereas the oxygen in particular is added thereto making it possible to obtain a sintered hard metal having said excellent properties.
摘要翻译： 本发明涉及具有高耐磨性和耐热性的烧结硬金属作为切削工具和耐磨工具的材料及其制造方法。 烧结硬质金属具有包含在周期表中含有多于一种IVa，Va和VIa族金属的B-1型晶体结构的相的硬相以及元素，碳，氮和氧以及WC相 硬质相和主要由通过粉末冶金技术烧结的黑色金属组成的结合相，特别是加入氧，使得可以获得具有优异性能的烧结硬质金属。
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公开(公告)号：US4169913A
公开(公告)日：1979-10-02
申请号：US882893
申请日：1978-03-01
CPC分类号： B23B27/148 , C23C14/06 , C23C30/00 , Y10S428/911 , Y10T428/24983 , Y10T428/31
摘要： There is provided a coated tool steel having a tool steel substrate and at least one layer of a hard film overcoated on the substrate. The film consists of a B-1 type solid solution selected from carbides, nitrides and carbonitrides of at least one of titanium, zirconium or hafnium, and the breadth of the peak, at half maximum intensity, of Cu-K.alpha. diffraction from the (200) plane of the film, being not less than 0.4 degree on a 2 .theta. scale. The invention further provides a machine tool having at least one cutting part thereof formed from the coated tool steel described above. The coated steel provided herein has excellent wear resistance.
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公开(公告)号：US5480601A
公开(公告)日：1996-01-02
申请号：US355814
申请日：1994-12-14
CPC分类号： C22C29/06 , B22F3/12 , B22F3/1208 , B23K35/327 , B23K35/406 , B22F2998/00
摘要： Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult of shaping or moulding by conventional process such as wire-drawing, rolling or extrusion of powder material and are difficult of machining or processing after the powder material is sintered.
摘要翻译： 一种细长烧结制品的制造方法，其特征在于包括将粉末材料填充到管中，对填充有粉末材料的管进行塑性变形，以及加热填充有粉末材料的管以烧结和/或烧结粉末 材料。 本发明的方法有利地适用于陶瓷线或棒的生产，特别是所谓的新陶瓷或微细陶瓷，烧结合金或它们的组合，其难以通过常规方法成形或成型，例如拉丝，轧制 或粉末材料的挤出，并且在粉末材料烧结后难以进行机械加工或加工。
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公开(公告)号：US4746563A
公开(公告)日：1988-05-24
申请号：US729973
申请日：1985-05-02
申请人： Minoru Nakano , Masaaki Tobioka
发明人： Minoru Nakano , Masaaki Tobioka
IPC分类号： C23C16/30 , B23P15/28 , C23C16/32 , C23C16/34 , C23C16/36 , C23C16/40 , C23C30/00 , B32B7/02 , B24D3/02 , B32B9/00 , C23C16/00
CPC分类号： C23C30/005 , Y10S428/932 , Y10T428/12576 , Y10T428/24975 , Y10T428/24983
摘要： Multilayer coated cemented carbides excellent in wear resistance and toughness are provided comprising a substrate of cemented carbide, an inner layer contacted with the surface of the substrate, and an outer layer contacted with the inner layer, the inner layer being a single layer and/or laminated layers consisting of at least one member selected from the group consisting of carbides, nitrides, carbonitrides, carboxynitrides, oxynitrides, boronitrides and borocarbonitrides of Ti, and the outer layer being a multilayer with a total thickness of 5 to 20 .mu.m, consisting of a plurality of Al.sub.2 O.sub.3 layer each having a thickness of 0.01 to 2 .mu.m, each consisting of an Al.sub.2 O.sub.3 film in which titanium oxide is dissolved or at most 30 vol % of titanium oxide is coexistent and being respectively divided by interlayers each having a thickness of 0.01 to 2 .mu.m and each consisting of at least one member of the group consisting of TiC, TiN, TiCN, TiCNO, TiNO, Ti oxides Ti(B, N), Ti(B, N, C), SiC, AlN and AlON.
摘要翻译： 提供耐磨性和韧性优异的多层涂层胶结碳化物，其包括硬质合金基材，与基材表面接触的内层和与内层接触的外层，内层为单层和/或 由选自碳化物，氮化物，碳氮化物，羧基氮化物，氧氮化物，硼氮化物和硼碳氮化物中的至少一种的Ti组成的层叠层，外层为总厚度为5至20μm的多层，由 多个Al 2 O 3层，各自具有0.01至2μm的厚度，每个Al 2 O 3层由其中溶解有氧化钛的Al 2 O 3膜或至多30vol％的氧化钛共存并分别由具有厚度为 0.01〜2μm，分别由TiC，TiN，TiCN，TiCNO，TiNO，Ti氧化物Ti（B，N），Ti（B，N，C），SiC，AlN 和Alon。
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公开(公告)号：US5252288A
公开(公告)日：1993-10-12
申请号：US883368
申请日：1992-05-15
CPC分类号： B22F3/12 , B22F3/1208 , B23K35/327 , B23K35/406 , C22C29/06 , B22F2998/00
摘要： Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult to shape or mold by conventional process such as wire-drawing, rolling or extrusion of powder material which is difficult to mold and machine after the powder material is sintered.
摘要翻译： 一种细长烧结制品的制造方法，其特征在于包括将粉末材料填充到管中，对填充有粉末材料的管进行塑性变形，以及加热填充有粉末材料的管以烧结和/或烧结粉末 材料。 本发明的方法有利地适用于陶瓷线或棒的生产，特别是所谓的新陶瓷或微细陶瓷，烧结合金或它们的组合，其难以通过常规方法如拉丝，轧制形成或模制 或挤出粉末材料，在粉末材料烧结后难以模塑和机械加工。
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公开(公告)号：US4900628A
公开(公告)日：1990-02-13
申请号：US76721
申请日：1987-07-22
申请人： Akihiko Ikegaya , Masaaki Tobioka
发明人： Akihiko Ikegaya , Masaaki Tobioka
IPC分类号： C30B25/02
CPC分类号： C30B25/02 , C30B29/04 , Y10T428/30
摘要： The present invention relates to gaseous phase synthesized diamond and a method of synthesizing the same. In order to obtain crystalline diamond having remarkably high completeness and hardly containing carbon having a construction other than that of diamond, raw material gases are thermally activated by a thermoelectron-radiating material heated at an extremely high temperature, the thermoelectron-radiating material being connected to a negative pole while a substrate to be coated is connected to a positive pole, by the use of a direct current power source, a plasma being formed between the thermoelectron-radiating material and the substrate by applying a direct current voltage, and a diamond film having an average particle size of 2 microns or less, compression residual stress and electric resistance of 10.sup.8 ohm.cm or more being formed on the substrate by using the activation by the thermoelectron-radiating material together with the activation by the formation of DC plasma.In addition, homogeneous diamond particles uniform in shape can be obtained by using this method.
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9.发明授权
公开(公告)号：US5266389A
公开(公告)日：1993-11-30
申请号：US691020
申请日：1991-06-27
申请人： Naoya Omori , Kazuo Yamagata , Toshio Nomura , Masaaki Tobioka
发明人： Naoya Omori , Kazuo Yamagata , Toshio Nomura , Masaaki Tobioka
IPC分类号： C23C14/06
CPC分类号： C23C14/0641 , C23C14/0635 , C23C14/0664 , Y10T428/24975
摘要： A surface-coated hard material for a cutting tool or wear resistance tool is provided which is excellent in wear resistance, deposition resistance and breakage resistance and exhibits good cutting performances for a long time, as a cutting tool or a wear resistance tool, in not only a low speed cutting but also a high speed cutting, and in which a layer consisting of a carbide, nitride or carbonitride of Ti, Zr or Hf and a layer consisting of a carbide, nitride or carbonitride of Al are alternately laminated to form at least 10 hard coating layers.
摘要翻译： PCT No.PCT / JP90 / 01258 Sec。 371日期1991年6月27日 102（e）1991年6月27日PCT PCT 1990年9月28日PCT公布。 第WO91 / 05076号公报 日本1991年04月18日提供了一种用于切削工具或耐磨工具的表面涂层硬质材料，其耐磨性，耐沉积性和耐断裂性优异，长时间显示出良好的切割性能，作为切削工具或 耐磨工具，不仅是低速切削而且是高速切削，其中由Ti，Zr或Hf的碳化物，氮化物或碳氮化物组成的层和由碳化物，氮化物或碳氮化物组成的层 Al交替层压以形成至少10个硬涂层。
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公开(公告)号：US5116694A
公开(公告)日：1992-05-26
申请号：US709786
申请日：1991-06-03
CPC分类号： C23C14/0664 , C23C14/0635 , C23C30/005 , Y10T428/24975
摘要： A coated cemented carbide with an improved wear resistance without lowering the toughness as a tool is provided comprising a substrate of a cemented carbide, the surface of which is coated with a multilayer of TiC, TiN and TiCN by the PVD method, the innermost layer in contact with the substrate being a TiN layer with a thickness of 0.1 to 1 .mu.m.
摘要翻译： 提供了具有改善的耐磨性的涂层硬质合金，而不降低作为工具的韧性，包括硬质合金的基材，其表面通过PVD方法涂覆有多层TiC，TiN和TiCN，最内层 与厚度为0.1〜1μm的TiN层的基板接触。
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