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公开(公告)号:US20130061799A1
公开(公告)日:2013-03-14
申请号:US13592555
申请日:2012-08-23
申请人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
发明人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
IPC分类号: C30B19/02
CPC分类号: C30B9/12 , C30B9/10 , C30B29/406
摘要: A method of manufacturing a group 13 nitride crystal includes a crystal growth process to form the group 13 nitride crystal by growing the group 13 nitride crystal having a hexagonal crystal structure from a seed crystal which is a gallium nitride crystal having a hexagonal crystal structure in which a length “L” in a c-axis direction is 9.7 mm or more, and a ratio L/d of the length “L” to a crystal diameter “d” in a c-plane is larger than 0.813. The crystal growth process includes a process of forming an outer periphery containing a {10-10} plane and an outer periphery containing a {10-11} plane at side surfaces of the group 13 nitride crystal, and forming an outer periphery containing a {0001} plane at a bottom surface of the group 13 nitride crystal.
摘要翻译: 制造13族氮化物晶体的方法包括通过从具有六方晶系结构的氮化镓晶体的晶种生长具有六方晶系结构的13族氮化物晶体来形成氮化镓族晶体的晶体生长工艺,其中 c轴方向的长度L为9.7mm以上,c面的长度L与晶体直径d的比L / d大于0.813。 晶体生长工艺包括在第13族氮化物晶体的侧面形成包含{10-10}面和包含{10-11}面的外周的外周的工艺,并且形成含有{ 0001}面。
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2.
公开(公告)号:US20130064749A1
公开(公告)日:2013-03-14
申请号:US13609077
申请日:2012-09-10
申请人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
发明人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
IPC分类号: C01B21/06 , C01B21/072 , C01B21/064
CPC分类号: C30B7/105 , C30B9/00 , C30B29/403 , C30B29/406 , C30B29/607
摘要: A group 13 nitride crystal having a hexagonal crystal structure and containing at least a nitrogen atom and at least a metal atom selected from a group consisting of B, Al, Ga, In, and Tl. The group 13 nitride crystal includes a first region disposed on an inner side in a cross section intersecting c-axis, a third region disposed on an outermost side in the cross section and having a crystal property different from that of the first region, and a second region disposed at least partially between the first region and the third region in the cross section, the second region being a transition region of a crystal growth and having a crystal property different from that of the first region and that of the third region.
摘要翻译: 具有六方晶系结构并且至少包含氮原子和至少一个选自B,Al,Ga,In和Tl的金属原子的13族氮化物晶体。 13族氮化物晶体包括设置在与c轴交叉的横截面的内侧的第一区域,设置在截面最外侧的第三区域,并且具有与第一区域不同的晶体特性, 所述第二区域至少部分地设置在所述第一区域和所述第三区域之间,所述第二区域是晶体生长的过渡区域,并且具有与所述第一区域和所述第三区域不同的晶体特性。
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3.
公开(公告)号:US20170204534A1
公开(公告)日:2017-07-20
申请号:US15455339
申请日:2017-03-10
申请人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
发明人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Hiroshi NAMBU , Chiharu KIMURA , Naoya MIYOSHI
CPC分类号: C30B29/406 , C30B9/12 , H01L33/16 , H01L33/32
摘要: A gallium nitride crystal having a hexagonal crystal structure, wherein a full width at half maximum (FWHM) of X-ray rocking curve in a region at a side of one edge in a c-axis direction is smaller than the FWHM in a region at a side of the other edge in the c-axis direction, in at least one of m-plane outer peripheral surfaces of the hexagonal crystal structure.
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4.
公开(公告)号:US20130243680A1
公开(公告)日:2013-09-19
申请号:US13798702
申请日:2013-03-13
申请人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Chiharu KIMURA , Naoya MIYOSHI , Akishige MURAKAMI , Junichi WADA
发明人: Masahiro HAYASHI , Seiji SARAYAMA , Takashi SATOH , Chiharu KIMURA , Naoya MIYOSHI , Akishige MURAKAMI , Junichi WADA
IPC分类号: C01B21/064 , C01B21/06
CPC分类号: C01B21/064 , C01B21/0632 , C30B9/06 , C30B29/403 , C30B29/406
摘要: A group 13 nitride crystal has a hexagonal crystal structure containing a nitrogen atom and at least one type of metal atom selected from the group consisting of B, Al, Ga, In, and Tl. The group 13 nitride crystal has a basal plane dislocation in a plurality of directions. Dislocation density of the basal plane dislocation is higher than dislocation density of a threading dislocation of a c-plane.
摘要翻译: 13族氮化物晶体具有包含氮原子的六方晶系结构和选自B,Al,Ga,In和Tl中的至少一种类型的金属原子。 13族氮化物晶体在多个方向上具有基面位错。 基面位错的位错密度高于c面穿透位错的位错密度。
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公开(公告)号:US20170022629A1
公开(公告)日:2017-01-26
申请号:US15124794
申请日:2014-11-27
申请人: Takashi SATOH , Seiji SARAYAMA , Masahiro HAYASHI , Naoya MIYOSHI , Chiharu KIMURA , Junichi WADA
发明人: Takashi SATOH , Seiji SARAYAMA , Masahiro HAYASHI , Naoya MIYOSHI , Chiharu KIMURA , Junichi WADA
CPC分类号: C30B9/10 , C30B9/12 , C30B29/406 , C30B35/007
摘要: A method for producing a gallium nitride crystal includes growing a gallium nitride crystal 5 by dissolving nitrogen in a mixed melt including gallium and sodium, and collecting the gallium 55 separated from an alloy 51 including the gallium and the sodium by reacting the alloy 51 and a liquid 52 that ionizes the sodium and separating sodium ions and the gallium 55 from the alloy.
摘要翻译: 制造氮化镓晶体的方法包括通过将氮溶解在包含镓和钠的混合熔体中来生长氮化镓晶体5,并且通过使合金51和合金51反应而收集从包含镓和钠的合金51中分离的镓55 使钠离子并从合金中分离钠离子和镓55的液体52。
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公开(公告)号:US20170345694A1
公开(公告)日:2017-11-30
申请号:US15600937
申请日:2017-05-22
申请人: Masahiro HAYASHI , Chiharu KIMURA
发明人: Masahiro HAYASHI , Chiharu KIMURA
IPC分类号: H01L21/673 , H01L21/683 , H01L21/67 , H01L33/16 , C30B29/64 , H01L33/00 , C30B29/38
CPC分类号: H01L21/67309 , C30B29/38 , C30B29/64 , H01L21/67011 , H01L21/67242 , H01L21/67353 , H01L21/6835 , H01L21/6836 , H01L21/68735 , H01L33/0095 , H01L33/16 , H01L2221/68327
摘要: A method for producing a crystal substrate includes preparing, measuring, holding, and machining. The preparing prepares a crystal substrate body including a curved crystal lattice plane. The measuring measures a shape feature of the crystal lattice plane. The holding holds the crystal substrate body in a warped state in accordance with the shape feature measured by the measuring, to more flatten the crystal lattice plane than the crystal lattice plane at the preparing. The machining machines a surface of the crystal substrate body held in the warped state, to flatten the surface.
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