公开(公告)号：US08992981B2

公开(公告)日：2015-03-31

申请号：US12679172

申请日：2008-09-11

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： A61K9/14 ,  B01D9/00 ,  A61K9/50 ,  B01J19/10 ,  B01J19/12 ,  B01J19/18

CPC分类号： B01D9/0013 ,  A61K9/146 ,  A61K9/5089 ,  B01D9/0031 ,  B01D9/0081 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  Y10T428/2982

摘要： It is an object of the present invention to provide a method for producing microparticles, which can produce monodispersed microparticles, causes no clogging with a product due to self-dischargeability, requires no great pressure, and is excellent in productivity, wherein a fluid in which at least one kind of microparticle materials is dissolved is introduced between two processing surfaces arranged to be opposite to each other to be able to approach to and separate from each other, at least one of which rotates relative to the other, to be formed into a thin film fluid, and the thin film fluid is cooled or heated (warmed) to allow saturation solubility to change, thereby separating microparticles.

摘要翻译： 本发明的目的是提供一种能够生产单分散微粒的微粒的制造方法，不会由于自放电性而导致产品不堵塞，不需要大的压力，生产率优异，其中， 将至少一种微粒材料溶解在彼此相对布置的两个处理表面之间，以能够彼此接近和分离，其中至少一个相对于另一个旋转，形成为 薄膜流体，并且薄膜流体被冷却或加热（加热）以允许饱和溶解度改变，从而分离微粒。

公开(公告)号：US08889885B2

公开(公告)日：2014-11-18

申请号：US13520239

申请日：2011-02-01

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： B82Y40/00 ,  C07D487/04 ,  B01D9/00 ,  C09B67/10 ,  C09B67/48

CPC分类号： C09B67/0014 ,  B01D9/0013 ,  B01D9/0031 ,  C09B67/0016 ,  C09B67/003

摘要： A method for producing a nanoparticle to separate a diketopyrrolopyrrole pigment includes separating an α-type diketopyrrolopyrrole pigment nanoparticle having high crystallinity by carrying out separation of the diketopyrrolopyrrole pigment and crystal type transformation to the α-type with substantially a single step. The α-type diketopyrrolopyrrole pigment nanoparticle is separated by mixing a diketopyrrolopyrrole pigment solution having the diketopyrrolopyrrole pigment dissolved in a solvent and an alcohol solvent containing an alcohol compound solvent in a thin film fluid formed between at least two processing surfaces 1 and 2 arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. An acidic substance is contained in at least any one of the diketopyrrolopyrrole pigment solution and the alcohol solvent at this moment.

摘要翻译： 用于分离二酮吡咯并吡咯颜料的纳米粒子的制造方法包括通过以基本上一个步骤进行二酮吡咯并吡咯颜料的分离和结晶型转变成α型，分离具有高结晶度的α型二酮吡咯并吡咯颜料纳米粒子。 通过将形成在溶剂中的二酮吡咯并吡咯颜料的二酮吡咯并吡咯颜料溶液和含有醇化合物溶剂的醇溶剂混合在形成在至少两个处理用面1和2之间的薄膜流体中来分离α型二酮吡咯并吡咯颜料纳米颗粒 彼此相对，以便能够彼此接近和分离，其中至少一个相对于另一个旋转。 此时，在二酮吡咯并吡咯颜料溶液和醇溶剂中至少含有一种酸性物质。

公开(公告)号：US20140121336A1

公开(公告)日：2014-05-01

申请号：US14123051

申请日：2012-03-15

申请人： Masaki Maekawa ,  Kaeko Araki ,  Daisuke Honda ,  Masakazu Enomura

发明人： Masaki Maekawa ,  Kaeko Araki ,  Daisuke Honda ,  Masakazu Enomura

IPC分类号： B22F9/16 ,  C07D471/04 ,  C01G23/08

CPC分类号： B22F9/16 ,  B01F3/1221 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/1887 ,  B22F1/0018 ,  B22F1/0022 ,  B22F1/0025 ,  B22F9/24 ,  B22F2998/10 ,  B22F2999/00 ,  C01G23/053 ,  C01G23/08 ,  C01P2004/04 ,  C07D471/04 ,  C22C5/06

摘要： The present invention addresses the problem of providing a new method for increasing the production of fine particles. Using at least two types of fluids to be processed, a raw material fluid containing at least one type of fine particle raw material and a fluid for treating the fine particle raw material, fine particles are obtained by mixing the fluids to be processed in a thin film fluid formed between at least two processing surfaces which are disposed to be faced with each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. At this time, the production of the fine particles is increased by introducing the raw material fluid from the centers of the processing surfaces.

摘要翻译： 本发明解决了提供用于增加细颗粒的生产的新方法的问题。 使用至少两种类型的待处理流体，含有至少一种类型的细粒原料的原料流体和用于处理细粒原料的流体，通过将待处理的流体以薄的 在至少两个处理表面之间形成的薄膜流体，所述至少两个处理表面被设置成彼此面对，以便能够彼此接近和分离，其中至少一个相对于另一个旋转。 此时，通过从处理用面的中心引入原料液，能够提高微粒的制造。

公开(公告)号：US20140037519A1

公开(公告)日：2014-02-06

申请号：US14112887

申请日：2011-04-28

申请人： Jun Kuraki ,  Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

发明人： Jun Kuraki ,  Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

IPC分类号： C22B19/34 ,  C01G9/03

CPC分类号： C22B19/34 ,  B01F3/0807 ,  B01F7/00775 ,  B01F7/00791 ,  B01F15/0203 ,  B01F15/0243 ,  B01F15/0291 ,  B82Y30/00 ,  C01B13/32 ,  C01B13/34 ,  C01G9/02 ,  C01G9/03 ,  C01P2002/01 ,  C01P2002/72 ,  C01P2002/88 ,  C01P2004/04 ,  C01P2004/62 ,  C01P2004/64

摘要： Provided is a method for producing an oxide and/or hydroxide wherein the ratio of oxide and hydroxide has been controlled. The method produces an oxide, a hydroxide, or a mixture thereof, and obtains an oxide and/or a hydroxide wherein the ratio of oxide and hydroxide has been controlled by means of changing a specific condition relating to at least one fluid to be processed introduced between processing surfaces (1, 2) when causing the precipitation of the oxide, hydroxide, or mixture thereof by mixing an basic fluid containing at least one type of basic substance and a fluid containing at least one type of metal or metallic substance as the fluids to be processed between the processing surfaces (1, 2) that are provided facing each other, are able to approach to and separate from each other, and of which at least one rotates relative to the other. The specific condition is at least one condition selected from the group consisting of: the speed of introduction of at least one of the fluids to be processed; and the pH of at least one of the fluids to be processed.

摘要翻译： 提供一种氧化物和/或氢氧化物的制造方法，其中氧化物和氢氧化物的比例已被控制。 该方法产生氧化物，氢氧化物或其混合物，并获得氧化物和/或氢氧化物，其中氧化物和氢氧化物的比例已经通过改变与至少一种待处理流体相关的特定条件来控制 当通过混合含有至少一种碱性物质的碱性流体和含有至少一种类型的金属或金属物质的流体作为流体而使氧化物，氢氧化物或其混合物沉淀时，处理表面（1,2）之间 在彼此面对地设置的处理表面（1,2）之间进行处理，能够彼此接近并分离，并且至少一个相对于另一个旋转。 所述具体条件是选自以下的至少一种条件：至少一种待处理流体的引入速度; 和至少一种要处理的流体的pH。

公开(公告)号：US08623415B2

公开(公告)日：2014-01-07

申请号：US12668021

申请日：2008-07-04

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： A61K9/14 ,  B01J13/00 ,  B01J19/06

CPC分类号： A61K31/196 ,  A61K9/0048 ,  A61K9/14 ,  A61K9/1688 ,  A61K31/00 ,  A61K31/436 ,  A61K31/57 ,  A61K31/58

摘要： A method of separating biologically ingestible microparticles is used to obtain biologically ingestible microparticles in a thin film fluid formed between two processing formed by a fluid to be processed containing at least a first solvent in which an objective substance to be pulverized is dissolved and a second solvent in which the solubility of the microparticles is lower than in the first solvent. The biologically ingestible microparticles are separated by a neutralization reaction in the thin film fluid.

摘要翻译： 使用分离生物摄取性微粒的方法来获得生物学上可摄入的微粒，该薄膜流体是由待处理流体形成的两种处理之间形成的，所述两种处理物至少包含溶解目标物质的第一溶剂和第二溶剂 其中微粒的溶解度低于第一溶剂中的溶解度。 通过薄膜流体中的中和反应分离生物摄取的微粒。

公开(公告)号：US20130220180A1

公开(公告)日：2013-08-29

申请号：US13883692

申请日：2011-05-20

申请人： Masaki Maekawa ,  Kaeko Araki ,  Hideyuki Oka ,  Daisuke Honda ,  Masakazu Enomura

发明人： Masaki Maekawa ,  Kaeko Araki ,  Hideyuki Oka ,  Daisuke Honda ,  Masakazu Enomura

IPC分类号： C09C1/62

CPC分类号： C07F3/06 ,  B01D11/0269 ,  B01F3/0861 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2004/82 ,  C07F1/08 ,  C09B67/0017 ,  C09B67/0019 ,  C09B67/0026 ,  C09B67/0035 ,  C09B67/0092 ,  C09C1/0081 ,  C09C1/04 ,  C09C1/627

摘要： The problem addressed by the present invention is to provide; solid solution pigment nanoparticles having a homogeneous solid solution ratio; a method for producing solid solution pigment nanoparticles having a homogeneous solid solution ratio in each primary particle; and a method for controlling the solid solution ratio of solid solution pigment nanoparticles. The solid solution pigment nanoparticles are prepared by precipitating at least two types of pigment by mixing a pigment precipitation solvent and; at least one type of pigment solution wherein at least two types of pigment are dissolved in a solvent: or at least two types of pigment solution wherein at least one type of pigment is dissolved in a solvent. The solid solution pigment nanoparticles are wherein the solid solution ratio of the at least two types of pigment in the primary particles of the precipitated solid solution pigment nanoparticles with respect to the ratio of the at least two types of pigment in the pigment solution mixed with the pigment precipitation solvent having a precision within 25%.

摘要翻译： 本发明提出的问题在于： 具有均匀固溶比的固溶颜料纳米粒子; 一种在一次粒子中具有均匀固溶比的固溶颜料纳米粒子的制造方法; 以及控制固溶颜料纳米粒子的固溶比的方法。 固溶颜料纳米粒子是通过混合颜料沉淀溶剂和至少两种颜料沉淀来制备的; 至少一种类型的颜料溶液，其中至少两种类型的颜料溶解在溶剂中：或至少两种类型的颜料溶液，其中至少一种类型的颜料溶解在溶剂中。 固溶颜料纳米粒子，其中沉淀的固溶颜料纳米颗粒的初级颗粒中的至少两种类型的颜料的固溶比相对于颜料溶液中的至少两种类型的颜料与 颜料沉淀溶剂的精度在25％以内。

公开(公告)号：US08183299B2

公开(公告)日：2012-05-22

申请号：US12668012

申请日：2008-07-04

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： B01F3/12 ,  C09C1/00

CPC分类号： B01F7/0075 ,  B01F7/00791 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00135 ,  B01J2219/00137 ,  B82Y30/00 ,  C01B13/32 ,  C01B13/36 ,  C01F7/34 ,  C01F7/36 ,  C01G9/02 ,  C01G23/006 ,  C01G23/047 ,  C01G23/053 ,  C01G25/02 ,  C01P2004/04 ,  C01P2004/52 ,  C01P2004/64 ,  Y10S977/84

摘要： The invention provides a method for producing ceramic nanoparticles, which comprises hydrolyzing a ceramic material in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other.

摘要翻译： 本发明提供了一种陶瓷纳米颗粒的制造方法，其包括将布置成彼此相对的处理表面之间形成的薄膜流体中的陶瓷材料水解以使得能够彼此接近和分离的至少一种 其相对于另一个旋转。

公开(公告)号：US20100196788A1

公开(公告)日：2010-08-05

申请号：US12667948

申请日：2008-07-04

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： H01M8/10 ,  H01M4/88 ,  C01B31/02 ,  B01J19/18

CPC分类号： H01M4/9083 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/1887 ,  B01J21/18 ,  B01J23/40 ,  B01J23/80 ,  B01J37/16 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/15 ,  H01M4/8803 ,  H01M4/8842 ,  H01M4/8846 ,  H01M4/8875 ,  H01M4/8882 ,  H01M4/90 ,  H01M4/9016 ,  H01M4/9041 ,  H01M4/92 ,  H01M4/921 ,  H01M4/926 ,  H01M8/1004

摘要： The present invention provides a method for producing metal-supported carbon, which includes supporting metal microparticles on the surface of carbon black, by a liquid-phase reduction method, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, as well as a method for producing crystals comprising fullerene molecules and fullerene nanowhisker/nanofiber nanotubes, which includes uniformly stirring and mixing a solution containing a first solvent having fullerene dissolved therein, and a second solvent in which fullerene is less soluble than in the first solvent, in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other.

摘要翻译： 本发明提供一种金属负载碳的制造方法，其包括在碳黑表面上通过液相还原法在形成在彼此相对的处理表面之间形成的薄膜流体中支撑金属微粒， 能够彼此接近并分离，其中至少一个相对于另一个旋转，以及包含富勒烯分子和富勒烯纳米晶须/纳米纤维纳米管的晶体的制造方法，其包括均匀地搅拌和混合溶液 含有溶解有富勒烯的第一溶剂和富勒烯比第一溶剂中溶解性低的第二溶剂，在形成在彼此相对的处理表面之间形成的薄膜流体中，以便能够接近和 彼此分离，其中至少一个相对于另一个旋转。

公开(公告)号：US09580447B2

公开(公告)日：2017-02-28

申请号：US13989082

申请日：2011-11-22

申请人： Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

发明人： Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

IPC分类号： C07D487/22 ,  C07F3/06 ,  B01D11/02 ,  B01F3/08 ,  C09B67/14 ,  C09B67/22 ,  C09C1/00 ,  C09C1/62 ,  C09C1/04 ,  C07F1/08 ,  B82Y30/00 ,  C09B67/42 ,  C09B67/16 ,  C09B67/50

CPC分类号： C07F3/06 ,  B01D11/0269 ,  B01F3/0861 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2004/82 ,  C07F1/08 ,  C09B67/0017 ,  C09B67/0019 ,  C09B67/0026 ,  C09B67/0035 ,  C09B67/0092 ,  C09C1/0081 ,  C09C1/04 ,  C09C1/627

摘要： The problem addressed by the present invention is to provide a high heat-resistant phthalocyanine. The phthalocyanine is separated by mixing a phthalocyanine separation solvent and a phthalocyanine solution wherein a phthalocyanine starting material is dissolved in a solvent. The phthalocyanine is wherein having high heat resistance, the decomposition temperature of the separated phthalocyanine being at least 10° C. higher than the decomposition temperature of the phthalocyanine starting material. Also, the phthalocyanine solution may be the result of dissolving at least two types of phthalocyanine starting material in the solvent, the separated phthalocyanine being wherein containing a solid solvent of the at least two types of phthalocyanine starting material and by the decomposition temperature of the separated phthalocyanine being at least 10° C. higher than the decomposition temperature of a mixture of at least two types of phthalocyanine separated by mixing the phthalocyanine separation solvent and each of at least two types of phthalocyanine solution resulting from dissolving each of the at least two types of phthalocyanine starting material in a solvent.

摘要翻译： 本发明解决的问题是提供高耐热酞菁。 通过混合酞菁分离溶剂和酞菁溶液将酞菁原料溶解在溶剂中来分离酞菁。 酞菁具有高耐热性，分离的酞菁的分解温度比酞菁起始原料的分解温度高10℃以上。 此外，酞菁溶液可能是将至少两种类型的酞菁原料溶解在溶剂中的结果，其中分离的酞菁含有至少两种类型的酞菁起始原料的固体溶剂和分离的 酞菁比通过混合酞菁分离溶剂和由至少两种类型的酞菁溶液中分离出的至少两种类型的酞菁溶液中的至少两种类型的酞菁溶液的分解温度高至少两种类型的酞菁的分解温度高至少10℃ 的酞菁原料在溶剂中。

公开(公告)号：US09242922B2

公开(公告)日：2016-01-26

申请号：US14009015

申请日：2012-03-27

申请人： Masakazu Enomura

发明人： Masakazu Enomura

IPC分类号： C07C51/42 ,  C01G23/02 ,  C04B35/468 ,  C07C51/41 ,  C01G23/00

CPC分类号： C07C51/412 ,  C01G23/006 ,  C01P2002/72 ,  C01P2004/04 ,  C04B35/4682 ,  C04B2235/449

摘要： A method for producing a high-quality barium titanyl salt includes using, as the fluids to be treated, at least two kinds of fluids, namely, a barium titanium mixed solution that is obtained by dissolving both a barium compound and a titanium compound in a solvent, a compound solution that is obtained by dissolving, in a solvent, a compound capable of deposing the barium and titanium contained in the barium-titanium mixed solution into a barium titanyl salt, and if necessary, one or more other fluids; and mixing these fluids together in a thin film fluid formed at least between two treating surfaces and to form a barium titanyl salt. The treating surfaces are so arranged as to face each other in an approachable/separable state with one of the treating surfaces and being capable of turning relatively to the other.

摘要翻译： 制造高质量的钛酸钡盐的方法包括使用至少两种流体，即将钡化合物和钛化合物两者同时溶解在钡钛混合溶液中的至少两种流体作为待处理流体 溶剂，通过将能够将钡 - 钛混合溶液中所含的钡和钛所含的化合物溶解在溶剂中而获得的化合物溶液形成钡钛酸盐，如果需要，将一种或多种其它流体溶解; 并将这些流体在至少形成在两个处理表面之间的薄膜流体中混合在一起并形成钡钛酸盐。 处理表面被布置为以可接近/可分离的状态与其中一个处理表面相对地相对并且能够相对于另一个转动。