公开(公告)号：US08708550B2

公开(公告)日：2014-04-29

申请号：US12668018

申请日：2008-07-04

Applicant: Masakazu Enomura

Inventor： Masakazu Enomura

IPC: B01F5/12 ,  B01F7/00

CPC classification number: B01J19/0093 ,  B01F7/00758 ,  B01F7/00791 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  C09B67/0022 ,  C09B67/0091 ,  Y10T137/0396 ,  Y10T137/6416 ,  Y10T137/8593 ,  Y10T137/85978

Abstract: A fluid is processed between processing surfaces capable of approaching to and separating from each other, at least one of which rotates relative to the other. A first fluid is introduced between processing surfaces, by using a micropump effect acting with a depression arranged on the processing surfaces from the center of the rotating processing surfaces. A second fluid, independent of this introduced fluid, is introduced from another fluid path that is provided with an opening leading to the processing surfaces, whereby the processing is done by mixing and stirring between the processing members.

Abstract translation: 在能够接近和分离的处理表面之间处理流体，其中至少一个相对于另一个旋转。 通过使用与从旋转处理用面的中心配置在处理用面上的凹部起作用的微型泵效应，在处理用面之间引入第一流体。 独立于该引入的流体的第二流体从另一个流体路径引入，该流体路径设置有通向处理表面的开口，由此通过在处理构件之间混合和搅拌来进行处理。

公开(公告)号：US08636974B2

公开(公告)日：2014-01-28

申请号：US12677606

申请日：2008-09-11

Applicant: Masakazu Enomura

Inventor： Masakazu Enomura

IPC: C01G23/047

CPC classification number: B01F5/221 ,  B01F3/12 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  B82Y30/00 ,  C01G23/053 ,  C01G23/0532 ,  C01G23/0536 ,  C01P2004/64 ,  C08K3/22 ,  C09C1/3676 ,  C09D5/00 ,  C09D7/61 ,  C09D7/67 ,  C09D7/68 ,  C09D17/008

Abstract: It is an object to provide a method for producing titanium dioxide superfine particles, which produces monodispersed titanium dioxide superfine particles depending on its purpose, causes no clogging with a product due to self-dischargeability, requires no great pressure, and is excellent in productivity. In the method for producing titanium dioxide superfine particles in a fluid containing a titanium compound by separation, the fluid is formed into a thin film fluid between two processing surfaces arranged so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, and the titanium dioxide superfine particles are separated in the thin film fluid.

Abstract translation: 本发明的目的是提供一种二氧化钛超细颗粒的制造方法，其根据其目的产生单分散的二氧化钛超微粒子，不会因自放电性而导致产品堵塞，不需要大的压力，生产率优异。 在通过分离含钛化合物的流体中生产二氧化钛超细颗粒的方法中，流体在两个处理表面之间形成为薄膜流体，该处理表面布置成彼此接近和分离，至少一个 其相对于另一个旋转，并且二氧化钛超细颗粒在薄膜流体中分离。

公开(公告)号：US20110015054A1

公开(公告)日：2011-01-20

申请号：US12668012

申请日：2008-07-04

Applicant: Masakazu Enomura

Inventor： Masakazu Enomura

IPC: C04B35/00 ,  C04B35/10 ,  C04B35/48 ,  C04B35/468 ,  C04B35/46 ,  C04B35/515 ,  C04B35/50 ,  C04B35/622

CPC classification number: B01F7/0075 ,  B01F7/00791 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00135 ,  B01J2219/00137 ,  B82Y30/00 ,  C01B13/32 ,  C01B13/36 ,  C01F7/34 ,  C01F7/36 ,  C01G9/02 ,  C01G23/006 ,  C01G23/047 ,  C01G23/053 ,  C01G25/02 ,  C01P2004/04 ,  C01P2004/52 ,  C01P2004/64 ,  Y10S977/84

Abstract: The invention provides a method for producing ceramic nanoparticles, which comprises hydrolyzing a ceramic material in a thin film fluid formed between processing surfaces arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other.

Abstract translation: 本发明提供了一种陶瓷纳米颗粒的制造方法，其包括将布置成彼此相对的处理表面之间形成的薄膜流体中的陶瓷材料水解以使得能够彼此接近和分离的至少一种 其相对于另一个旋转。

公开(公告)号：US20070152360A1

公开(公告)日：2007-07-05

申请号：US10579755

申请日：2004-11-18

Applicant: Tomonori Kawakami ,  Mitsuo Hiramatsu ,  Tokio Takagi

Inventor： Tomonori Kawakami ,  Mitsuo Hiramatsu ,  Tokio Takagi

IPC: A61K9/14 ,  B29B9/00

CPC classification number: B01J19/121 ,  B01J2219/00094 ,  B01J2219/00137 ,  B01J2219/0871 ,  B01J2219/0877 ,  B01J2219/0879

Abstract: A to-be-treated body, which contains raw material particles 5 of a substance and with which a solvent 4 of a to-be-treated liquid 2 is made solid, is used, and a laser light source 10, which supplies a laser light of a predetermined wavelength to a treatment chamber 3 that contains the to-be-treated body, is provided to arrange a production apparatus 1A. The laser light from the laser light source 10 is illuminated onto the to-be-treated body to microparticulate the substance in solvent 4. As the to-be-treated body of solid form, a solidified body 6, with which water 4 is solidified by a cooling device 50 and the solidified state is maintained by a thermally insulating layer 30, may be used. Or, as the to-be-treated body, a gel body, with which the solvent is gelled, may be used. The substance can thereby microparticulated efficiently by photo-pulverization.

Abstract translation: 使用含有物质的原料颗粒5并且待处理液体2的溶剂4与其形成固体的待处理体，以及提供激光的激光源10 设置含有待处理体的处理室3的预定波长的光，以配置制造装置11A。将来自激光光源10的激光照射到被处理体上， 在溶剂中微粒化物质4。 作为固体形式的被处理体，可以使用通过冷却装置50固化水4和固化状态的凝固体6，由绝热层30维持。 或者，作为被处理体，可以使用溶胶凝胶化的凝胶体。 因此可以通过光粉化有效地使物质微粒化。

公开(公告)号：US20040170538A1

公开(公告)日：2004-09-02

申请号：US10473644

申请日：2004-04-15

Inventor： Kouji Kawakami ,  Yujiro Kitaide ,  Nobuhisa Kato

IPC: B06B001/00 ,  B01J019/12 ,  B01J019/10

CPC classification number: B01J19/123 ,  A62D2203/10 ,  B01J19/10 ,  B01J2219/00015 ,  B01J2219/00038 ,  B01J2219/0004 ,  B01J2219/00137 ,  B01J2219/0877 ,  C02F1/325 ,  C02F1/36 ,  C02F1/66 ,  C02F1/722 ,  C02F2101/322 ,  C02F2101/36 ,  C02F2101/363 ,  C02F2101/366 ,  C02F2103/06 ,  C02F2201/3227 ,  C02F2201/3228 ,  C02F2209/02 ,  C02F2209/06

Abstract: The present invention provides a method and a device, by which it is possible to decompose and treat a large amount of organic halogen compounds, etc. which are environmental pollutants, to a low concentration range at which it is dischargeable as waste liquor to sewage in a short time, and it is also possible to decompose organic substances and nitrogen or phosphorus compounds which are hardly decomposable by oxidation. To a sample solution 20 contained in a reaction vessel 10a in which an aqueous solution containing environmental pollutants is stored, for example, ultrasonic waves 50 are irradiated from a transducer 30a disposed at the central bottom portion of the reaction vessel 10a, and at the same time, ultraviolet rays are irradiated from an ultraviolet lamp 40a disposed at the peripheral edge of the reaction vessel 10a. In this instance, the ultraviolet lamp 40a is disposed at a position such that it does not interfere with the path of travel of ultrasonic waves 50.

Abstract translation: 本发明提供一种方法和装置，通过该方法和装置，可以将大量作为环境污染物的有机卤素化合物等分解和处理至低浓度范围，作为废液排放到污水中 短时间，也可以分解通过氧化难以分解的有机物质和氮或磷化合物。 存储在其中储存有环境污染物的水溶液的反应容器10a中的样品溶液20例如从设置在反应容器10a的中央底部的换能器30a照射超声波50， 时间，从设置在反应容器10a的周缘的紫外灯40a照射紫外线。 在这种情况下，紫外线灯40a设置在不干扰超声波50的行进路径的位置。

公开(公告)号：US20240149238A1

公开(公告)日：2024-05-09

申请号：US18500612

申请日：2023-11-02

Applicant: Waters Technologies Corporation

Inventor： Lindsay Morrison

IPC: B01J19/00 ,  G01N30/02

CPC classification number: B01J19/0013 ,  G01N30/02 ,  B01J2219/00031 ,  B01J2219/00054 ,  B01J2219/00135 ,  B01J2219/00137 ,  G01N2030/027

Abstract: The present disclosure discusses a device and method for improving the reaction rate of enzymatic modification of biopolymers. A thermophoretic device is used to increase the rate of enzymatic reactions with biopolymers by creating a temperature gradient using a heating element and a cooling element. The use of a temperature gradient within a cavity in the thermophoretic device concentrates the reacts along an interior surface of the device, increasing the reaction rate.

公开(公告)号：US07938344B2

公开(公告)日：2011-05-10

申请号：US10579755

申请日：2004-11-18

Applicant: Tomonori Kawakami ,  Mitsuo Hiramatsu ,  Tokio Takagi

Inventor： Tomonori Kawakami ,  Mitsuo Hiramatsu ,  Tokio Takagi

IPC: B02C19/18

CPC classification number: B01J19/121 ,  B01J2219/00094 ,  B01J2219/00137 ,  B01J2219/0871 ,  B01J2219/0877 ,  B01J2219/0879

Abstract: A to-be-treated body, which contains raw material particles 5 of a substance and with which a solvent 4 of a to-be-treated liquid 2 is made solid, is used, and a laser light source 10, which supplies a laser light of a predetermined wavelength to a treatment chamber 3 that contains the to-be-treated body, is provided to arrange a production apparatus 1A. The laser light from the laser light source 10 is illuminated onto the to-be-treated body to microparticulate the substance in solvent 4. As the to-be-treated body of solid form, a solidified body 6, with which water 4 is solidified by a cooling device 50 and the solidified state is maintained by a thermally insulating layer 30, may be used. Or, as the to-be-treated body, a gel body, with which the solvent is gelled, may be used. The substance can thereby microparticulated efficiently by photo-pulverization.

Abstract translation: 使用含有物质的原料颗粒5并且待处理液体2的溶剂4与其形成固体的待处理体，以及提供激光的激光源10 提供预定波长的光到包含被处理体的处理室3，以布置生产设备1A。 来自激光光源10的激光被照射到被处理体上以使溶剂4中的物质微粒化。作为待固化体的待处理体，凝固体6与水4固化 通过冷却装置50，并且可以使用由隔热层30保持固化状态。 或者，作为被处理体，可以使用溶胶凝胶化的凝胶体。 因此可以通过光粉化有效地使物质微粒化。

公开(公告)号：US20100326321A1

公开(公告)日：2010-12-30

申请号：US12668015

申请日：2008-07-04

Applicant: Masakazu Enomura

Inventor： Masakazu Enomura

IPC: C09D11/02

CPC classification number: C09B67/0017 ,  B01F7/00758 ,  B01F7/00791 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  B01J2219/00141 ,  B82Y30/00 ,  C09B67/0005 ,  C09B67/0022 ,  C09B67/0091 ,  C09D11/322

Abstract: A forced ultrathin film rotary reaction method is used to maintain a minute space of 1 mm or less between two processing surfaces capable of approaching to and separating from each other and being rotating relative to each other, and the minute space is maintained between the two processing surfaces to serve as a flow path of a fluid to be processed thereby forming a forced thin film of the processed fluid and separating the pigment material in the forced thin film.

Abstract translation: 使用强制超薄膜旋转反应方法，能够在能够接近并分离并相对于彼此旋转的两个处理用面之间保持1mm以下的微小空间，并且在两处理之间保持微小空间 表面用作待处理流体的流动路径，从而形成被处理流体的强制薄膜并分离强制薄膜中的颜料。

公开(公告)号：US20100215958A1

公开(公告)日：2010-08-26

申请号：US12679172

申请日：2008-09-11

Applicant: Masakazu Enomura

Inventor： Masakazu Enomura

IPC: A61K9/14 ,  B29B9/00

CPC classification number: B01D9/0013 ,  A61K9/146 ,  A61K9/5089 ,  B01D9/0031 ,  B01D9/0081 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  Y10T428/2982

Abstract: It is an object of the present invention to provide a method for producing microparticles, which can produce monodispersed microparticles, causes no clogging with a product due to self-dischargeability, requires no great pressure, and is excellent in productivity, wherein a fluid in which at least one kind of microparticle materials is dissolved is introduced between two processing surfaces arranged to be opposite to each other to be able to approach to and separate from each other, at least one of which rotates relative to the other, to be formed into a thin film fluid, and the thin film fluid is cooled or heated (warmed) to allow saturation solubility to change, thereby separating microparticles.

Abstract translation: 本发明的目的是提供一种能够生产单分散微粒的微粒的制造方法，不会由于自放电性而导致产品不堵塞，不需要大的压力，生产率优异，其中， 将至少一种微粒材料溶解在彼此相对布置的两个处理表面之间，以能够彼此接近和分离，其中至少一个相对于另一个旋转，形成为 薄膜流体，并且薄膜流体被冷却或加热（加热）以允许饱和溶解度改变，从而分离微粒。

公开(公告)号：US20080265070A1

公开(公告)日：2008-10-30

申请号：US12213977

申请日：2008-06-26

Applicant: Tomonori Kawakami ,  Bo Li ,  Mitsuo Hiramatsu

Inventor： Tomonori Kawakami ,  Bo Li ,  Mitsuo Hiramatsu

IPC: B02C19/00

CPC classification number: C09C3/00 ,  B01J19/0013 ,  B01J19/121 ,  B01J2219/00063 ,  B01J2219/00094 ,  B01J2219/00126 ,  B01J2219/00137 ,  B01J2219/0871 ,  B01J2219/0877 ,  B01J2219/0879 ,  C01P2004/64

Abstract: With this invention, in a nanoparticle production method, wherein nanoparticles are produced by irradiating a laser light irradiation portion 2a of a to-be-treated liquid 8 with a laser light, in which suspended particles are suspended, to pulverize the suspended particles in laser light irradiation portion 2a, laser light irradiation portion 2a of to-be-treated liquid 8 is cooled. In this case, by the cooling of to-be-treated liquid 8, the respective suspended particles are cooled in their entireties. When the portion 2a of this to-be-treated liquid 8 is irradiated with the laser light, the laser light is absorbed at the surfaces of the suspended particles at portion 2a. Since to-be-treated liquid 8 is cooled during this process, significant temperature differences arise between the interiors and surfaces of the suspended particles and between the surfaces of the suspended particles and the to-be-treated liquid at laser light irradiation portion 2a, and highly efficient nanoparticulation is realized.

Abstract translation: 通过本发明，在纳米粒子制造方法中，其中通过用悬浮颗粒悬浮的激光照射待处理液体8的激光照射部分2a来制造纳米颗粒，以将悬浮颗粒粉碎 激光照射部分2a，被处理液体8的激光照射部分2a被冷却。 在这种情况下，通过冷却待处理液体8，各个悬浮颗粒全部被冷却。 当被处理液8的部分2a被激光照射时，激光在部分2a处被悬浮颗粒的表面吸收。 由于待处理液体8在该过程中被冷却，因此在悬浮颗粒的内部和表面之间以及在激光照射部分2a处的悬浮颗粒和待处理液体的表面之间产生显着的温度差 ，实现了高效的纳米微粒化。