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1.发明授权Aliphatic copolyester resin, a preparation method, an aliphatic polyester resin composition, uses thereof, a coating composition, a particle-state composition for agriculture and gardening coated by degradable layer 失效脂肪族共聚酯树脂，制备方法，脂肪族聚酯树脂组合物，其用途，涂料组合物，用于农业的颗粒状组合物和由可降解层涂覆的园艺公开(公告)号：US07220469B2
公开(公告)日：2007-05-22
申请号：US10991658
申请日：2004-11-18
IPC分类号： B41M5/40
CPC分类号： G03G7/008 , B41M5/41 , B41M5/44 , B41M5/5272 , C08G18/284 , C08G18/4277 , C08G18/4286 , C08G18/631 , C08G18/728 , C08G63/00 , C08G63/08 , C08G63/664 , C08G63/78 , C08G63/912 , C08G2230/00 , C08G2310/00 , C08L33/00 , C09D167/04 , C09D175/04 , C09D175/06 , G03G7/0046 , Y10T428/31978 , C08L2666/02 , C08L2666/04
摘要： This invention relates to aliphatic polyesters having a controlled thermal decomposition, hydrolizability, and biodegradability, in which OH terminals and COOH terminals are decreased through a ring-opening polymerization of a lactone and lactide by a mono alcohol or a metal alkoxide, or by decreasing both terminals through combining polymer terminals with diisocyanate. From a composition containing the polyesters, this invention provides a controlled release composition for agriculture. From a resin primarily containing fatty acid cellulose ester derivatives, this invention provides a base film for a marking film without volatilization and plasticizer migration problems; a picture image formable heat-sensitive transfer recording material with excellent strippability, coloring concentration, and brightness; a conductive coating composition with excellent storage stability, adhesion, and conductivity; a single-liquid type coating for a moisture-curable graft copolymer, and a non-toxic and non-irritating coating composition with excellent dryability. The copolymers of this invention also have excellent heat and impact resistance.
摘要翻译： 本发明涉及具有受控热分解，水解和生物降解性的脂肪族聚酯，其中OH末端和COOH末端通过单醇或金属醇盐通过内酯和丙交酯的开环聚合而降低，或通过减少两者 终端通过将聚合物末端与二异氰酸酯结合。 本发明由含有聚酯的组合物提供用于农业的控释组合物。 本发明主要由脂肪酸纤维素酯衍生物构成的树脂，提供了没有挥发和增塑剂迁移的标记膜的基膜， 具有优异的剥离性，着色浓度和亮度的图像形成的热敏转印记录材料; 具有优异的储存稳定性，粘合性和导电性的导电性涂料组合物; 用于湿气固化接枝共聚物的单液体型涂料和具有优异干燥性的无毒无刺激性涂料组合物。 本发明的共聚物也具有优异的耐热和耐冲击性。
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2.发明申请Aliphatic copolyester resin, a preparation method, an aliphatic polyester resin composition, uses thereof, a coating composition, a particle-state composition for agriculture and gardening coated by degradabel layer 失效脂肪族共聚酯树脂，制备方法，脂肪族聚酯树脂组合物，其用途，涂料组合物，用于农业的颗粒状组合物和由降解层涂覆的园艺公开(公告)号：US20050153149A1
公开(公告)日：2005-07-14
申请号：US10991658
申请日：2004-11-18
IPC分类号： B41M5/40 , B41M5/41 , B41M5/44 , B41M5/52 , C08G18/28 , C08G18/42 , C08G18/63 , C08G18/72 , C08G63/00 , C08G63/08 , C08G63/664 , C08G63/78 , C08G63/91 , C08L33/00 , C09D167/04 , C09D175/04 , C09D175/06 , G03G7/00 , B32B23/04
CPC分类号： G03G7/008 , B41M5/41 , B41M5/44 , B41M5/5272 , C08G18/284 , C08G18/4277 , C08G18/4286 , C08G18/631 , C08G18/728 , C08G63/00 , C08G63/08 , C08G63/664 , C08G63/78 , C08G63/912 , C08G2230/00 , C08G2310/00 , C08L33/00 , C09D167/04 , C09D175/04 , C09D175/06 , G03G7/0046 , Y10T428/31978 , C08L2666/02 , C08L2666/04
摘要： This invention relates to aliphatic polyesters having a controlled thermal decomposition, hydrolizability, and biodegradability, in which OH terminals and COOH terminals are decreased through a ring-opening polymerization of a lactone and lactide by a mono alcohol or a metal alkoxide, or by decreasing both terminals through combining polymer terminals with diisocyanate. From a composition containing the polyesters, this invention provides a controlled release composition for agriculture. From a resin primarily containing fatty acid cellulose ester derivatives, this invention provides a base film for a marking film without volatilization and plasticizer migration problems; a picture image formable heat-sensitive transfer recording material with excellent strippability, coloring concentration, and brightness; a conductive coating composition with excellent storage stability, adhesion, and conductivity; a single-liquid type coating for a moisture-curable graft copolymer, and a non-toxic and non-irritating coating composition with excellent dryability. The copolymers of this invention also have excellent heat and impact resistance.
摘要翻译： 本发明涉及具有受控热分解，水解和生物降解性的脂肪族聚酯，其中OH末端和COOH末端通过单醇或金属醇盐通过内酯和丙交酯的开环聚合而降低，或通过减少两者 终端通过将聚合物末端与二异氰酸酯结合。 本发明由含有聚酯的组合物提供用于农业的控释组合物。 本发明主要由脂肪酸纤维素酯衍生物构成的树脂，提供了没有挥发和增塑剂迁移的标记膜的基膜， 具有优异的剥离性，着色浓度和亮度的图像形成的热敏转印记录材料; 具有优异的储存稳定性，粘合性和导电性的导电性涂料组合物; 用于湿气固化接枝共聚物的单液体型涂料和具有优异干燥性的无毒无刺激性涂料组合物。 本发明的共聚物也具有优异的耐热和耐冲击性。
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3.发明申请Aliphatic copolyester resin, a preparation method, an aliphatic polyester resin composition, uses thereof, a coating composition, a particle-state composition for agriculture and gardening coated by degradable layer 失效脂肪族共聚酯树脂，制备方法，脂肪族聚酯树脂组合物，其用途，涂料组合物，用于农业的颗粒状组合物和由可降解层涂覆的园艺公开(公告)号：US20050090401A1
公开(公告)日：2005-04-28
申请号：US10992524
申请日：2004-11-18
IPC分类号： B41M5/40 , B41M5/41 , B41M5/44 , B41M5/52 , C08G18/28 , C08G18/42 , C08G18/63 , C08G18/72 , C08G63/00 , C08G63/08 , C08G63/664 , C08G63/78 , C08G63/91 , C08L33/00 , C09D167/04 , C09D175/04 , C09D175/06 , G03G7/00 , C08G63/02 , A01N25/10
CPC分类号： G03G7/008 , B41M5/41 , B41M5/44 , B41M5/5272 , C08G18/284 , C08G18/4277 , C08G18/4286 , C08G18/631 , C08G18/728 , C08G63/00 , C08G63/08 , C08G63/664 , C08G63/78 , C08G63/912 , C08G2230/00 , C08G2310/00 , C08L33/00 , C09D167/04 , C09D175/04 , C09D175/06 , G03G7/0046 , Y10T428/31978 , C08L2666/02 , C08L2666/04
摘要： In the present invention, there are obtained aliphatic polyesters having a controlled thermal decomposing property, hydrolizability, and biodegradability, in which OH terminals and COOH terminals are decreased to 50% and 30%, respectively, through a ring-opening polymerization of a lactone and lactide by a mono alcohol having a high boiling point or a metal alkoxide, or by further decreasing both terminals through combining produced polymer terminals with a diisocyanate and, from a composition containing the polyesters, there is obtained a particle-state composition for agriculture and gardening in which a duration period of a fertilizing effect can be controlled, and which is not remained in soil by decomposition. From a resin primarily containing fatty acid cellulose ester derivatives, there are obtained a base film for a marking film which does not include a problem such as volatilization and migration of a plasticizer and a picture image formable heat-sensitive transfer recording material which is excellent in strippability, coloring concentration, and brightness, a conductive coating composition which is excellent in storage stability, adhesion, and conductivity, a single-liquid type coating and a moisture-curable graft copolymer, and a coating composition which have a non toxicity and nonirritating property and which are excellent in dryability. A copolymer in which average chain length in lactone and lactide units are controlled is excellent in heat resistance and impact resistance.
摘要翻译： 在本发明中，通过内酯的开环聚合，得到具有受控的热分解性，水解性和生物降解性的脂肪族聚酯，其中OH末端和COOH末端分别降低至50％和30％ 通过具有高沸点的单醇或金属醇盐的丙交酯，或者通过将产生的聚合物末端与二异氰酸酯组合而进一步减少两个末端，并且从含有聚酯的组合物获得农业和园艺的颗粒状组合物 可以控制施肥持续时间，并且不会被分解留在土壤中。 从主要含有脂肪酸纤维素酯衍生物的树脂，得到不含有增塑剂的挥发，迁移，图像形成性热敏转印记录材料等的问题的标记膜用基膜， 剥离性，着色浓度和亮度，保存稳定性，粘合性和导电性优异的导电性涂料组合物，单液型涂布和湿润性接枝共聚物，以及具有非毒性和无刺激性的涂料组合物 并且其干燥性优异。 控制内酯和丙交酯单元的平均链长的共聚物的耐热性和耐冲击性优异。
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4.发明授权ALIPHATIC COPOLYMER, PRODUCTION PROCESS, ALIPHATIC POLYESTER RESIN COMPOSITION, VARIOUS USES, COATING COMPOSITION, AND AGRICULTURAL OR HORTICULTURAL PARTICULATE COMPOSITION COMPRISING DEGRADABLE COATING FILM 失效二次共聚物，生产方法，聚氨酯树脂组合物，各种用途，涂料组合物和包含可降解涂料膜的农业或农业颗粒组合物公开(公告)号：US06509440B1
公开(公告)日：2003-01-21
申请号：US09600242
申请日：2000-09-14
IPC分类号： C08L6700
CPC分类号： C08G63/78 , C08G18/4277 , C08G18/4286 , C08G18/631 , C08G18/728 , C08G63/00 , C08G63/08 , C08G63/912 , C08G2230/00 , C09D167/04 , C09D175/04 , Y10T428/164 , C08L2666/02
摘要： In the present invention, there are obtained aliphatic polyesters having a controlled thermal decomposing property, hydrolizability, and biodegradability, in which OH terminals and COOH terminals are decreased to 50% and 30%, respectively, through a ring-opening polymerization of a lactone and lactide by a mono alcohol having a high boiling point or a metal alkoxide, or by further decreasing both terminals through combining produced polymer terminals with a diisocyanate and, from a composition containing the polyesters, there is obtained a particle-state composition for agriculture and gardening in which a duration period of a fertilizing effect can be controlled, and which is not remained in soil by decomposition. From a resin primarily containing fatty acid cellulose ester derivatives, there are obtained a base film for a marking film which does not include a problem such as volatilization and migration of a plasticizer and a picture image formable heat-sensitive transfer recording material which is excellent in strippability, coloring concentration, and brightness, a conductive coating composition which is excellent in storage stability, adhesion, and conductivity, a single-liquid type coating and a moisture-curable graft copolymer, and a coating composition which have a non toxicity and nonirritating property and which are excellent in dryability. A copolymer in which average chain length in lactone and lactide units are controlled is excellent in heat resistance and impact resistance.
摘要翻译： 在本发明中，通过内酯的开环聚合，得到具有受控的热分解性，水解性和生物降解性的脂肪族聚酯，其中OH末端和COOH末端分别降低至50％和30％ 通过具有高沸点的单醇或金属醇盐的丙交酯，或者通过将产生的聚合物末端与二异氰酸酯组合而进一步减少两个末端，并且从含有聚酯的组合物获得农业和园艺的颗粒状组合物 可以控制施肥持续时间，并且不会被分解留在土壤中。 从主要含有脂肪酸纤维素酯衍生物的树脂，得到不含有增塑剂的挥发，迁移，图像形成性热敏转印记录材料等的问题的标记膜用基膜， 剥离性，着色浓度和亮度，保存稳定性，粘合性和导电性优异的导电性涂料组合物，单液型涂布和湿润性接枝共聚物，以及具有非毒性和无刺激性的涂料组合物 并且其干燥性优异。 控制内酯和丙交酯单元的平均链长的共聚物的耐热性和耐冲击性优异。
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5.发明授权ALIPHATIC COPOLYESTER RESIN, A PREPARATION METHOD, AN ALIPHATIC POLYESTER RESIN COMPOSITION, USES THEREOF, A COATING COMPOSITION, A PARTICLE-STATE COMPOSITION FOR AGRICULTURE AND GARDENING COATED BY DEGRADABLE LAYER 失效聚酰胺树脂，制备方法，聚氨酯树脂组合物，其用途，涂料组合物，由可降解层包覆的农业和园艺的颗粒状组合物公开(公告)号：US06864351B2
公开(公告)日：2005-03-08
申请号：US10261422
申请日：2002-09-30
申请人： Masanori Sakane , Masaaki Ito
发明人： Masanori Sakane , Masaaki Ito
IPC分类号： B41M5/40 , B41M5/41 , B41M5/44 , B41M5/52 , C08G18/28 , C08G18/72 , C08G63/00 , C08G63/08 , C08G63/664 , C08L33/00 , C09D175/06 , G03G7/00
CPC分类号： G03G7/008 , B41M5/41 , B41M5/44 , B41M5/5272 , C08G18/284 , C08G18/728 , C08G63/00 , C08G63/08 , C08G63/664 , C08G2230/00 , C08G2310/00 , C08L33/00 , C09D175/06 , G03G7/0046 , C08L2666/04
摘要： In the present invention, there are obtained aliphatic polyesters having a controlled thermal decomposing property, hydrolizability, and biodegradability, in which OH terminals and COOH terminals are decreased to 50% and 30%, respectively, through a ring-opening polymerization of a lactone and lactide by a mono alcohol having a high boiling point or a metal alkoxide, or by further decreasing both terminals through combining produced polymer terminals with a diisocyanate and, from a composition containing the polyesters, there is obtained a particle-state composition for agriculture and gardening in which a duration period of a fertilizing effect can be controlled, and which is not remained in soil by decomposition. From a resin primarily containing fatty acid cellulose ester derivatives, there are obtained a base film for a marking film which does not include a problem such as volatilization and migration of a plasticizer and a picture image formable heat-sensitive transfer recording material which is excellent in strippability, coloring concentration, and brightness, a conductive coating composition which is excellent in storage stability, adhesion, and conductivity, a single-liquid type coating and a moisture-curable graft copolymer, and a coating composition which have a non toxicity and nonirritating property and which are excellent in dryability. A copolymer in which average chain length in lactone and lactide units are controlled is excellent in heat resistance and impact resistance.
摘要翻译： 在本发明中，通过内酯的开环聚合，得到具有受控的热分解性，水解性和生物降解性的脂肪族聚酯，其中OH末端和COOH末端分别降低至50％和30％ 通过具有高沸点的单醇或金属醇盐的丙交酯，或者通过将产生的聚合物末端与二异氰酸酯组合而进一步减少两个末端，并且从含有聚酯的组合物获得农业和园艺的颗粒状组合物 可以控制施肥持续时间，并且不会被分解留在土壤中。 从主要含有脂肪酸纤维素酯衍生物的树脂，得到不含有增塑剂的挥发，迁移，图像形成性热敏转印记录材料等的问题的标记膜用基膜， 剥离性，着色浓度和亮度，保存稳定性，粘合性和导电性优异的导电性涂料组合物，单液型涂布和湿润性接枝共聚物，以及具有非毒性和无刺激性的涂料组合物 并且其干燥性优异。 控制内酯和丙交酯单元的平均链长的共聚物的耐热性和耐冲击性优异。
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公开(公告)号：US20090198020A1
公开(公告)日：2009-08-06
申请号：US12224957
申请日：2007-02-21
申请人： Masanori Sakane
发明人： Masanori Sakane
IPC分类号： C08G63/91
CPC分类号： C08L67/00 , C08G63/91 , C08G2261/126 , C08K5/29 , C08L63/00 , C08L79/00 , C08L2666/14 , C08L2666/22 , C08L2666/18
摘要： A polyester-series resin composition comprises (A) a polyester block copolymer, (B) a polyepoxy compound and (C) a polycarbodiimide compound. The copolymer (A) is obtainable by a reaction of (a1) a crystalline aromatic polyester and (a2) a lactone, and if necessary (a3) at least one compound selected from the group consisting of a polycarboxylic acid or an ester-formable derivative thereof and a polyol or an ester-formable derivative thereof in the presence of an acidic phosphate ester and a tin compound. Such a resin composition is particularly excellent in recycling efficiency (or thermal cycling resistance) and is useful for blow molding.
摘要翻译： 聚酯系树脂组合物包含（A）聚酯嵌段共聚物，（B）聚环氧化合物和（C）聚碳化二亚胺化合物。 共聚物（A）可以通过（a1）结晶性芳香族聚酯和（a2）内酯的反应获得，并且根据需要（a3）至少一种选自多元羧酸或酯形成衍生物的化合物 和多元醇或其可形成酯的衍生物在酸性磷酸酯和锡化合物的存在下反应。 这种树脂组合物在回收效率（或耐热循环性）方面特别优异，并且可用于吹塑。
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公开(公告)号：US06914101B2
公开(公告)日：2005-07-05
申请号：US10451963
申请日：2002-04-01
申请人： Masanori Sakane
发明人： Masanori Sakane
IPC分类号： C08L67/00 , C08G59/42 , C08G63/20 , C08G63/60 , C08G63/91 , C08K5/05 , C08K5/053 , C08K5/1515 , C08K5/524 , C08K5/526 , C08K5/5333 , C08F20/00
摘要： The present invention relates to a polyester block copolymer composition which is obtained by reacting 0.5 to 5.0 parts by weight of an epoxy compound (C) having two or more functionalities with 100 parts by weight of a polyester block copolymer (P) having an acid value of 0 to 5 mgKOH/g obtained by reacting a crystalline aromatic polyester (A) having a hydroxyl group at a molecular terminal with a lactone (B) and optionally with a polyfunctional compound (D) having three or more groups selected among carboxyl, hydroxyl, and/or ester groups thereof. The composition has such excellent moldability that it is applicable to molding techniques including blow molding without arousing any trouble. It is satisfactory in heat resistance, water resistance, impact resistance, or flame retardancy, and has rubber-like elasticity.
摘要翻译： 本发明涉及一种聚酯嵌段共聚物组合物，其通过使0.5-5.0重量份具有两个或更多个官能团的环氧化合物（C）与100重量份具有酸值的聚酯嵌段共聚物（P） 通过使分子末端具有羟基的结晶性芳香族聚酯（A）与内酯（B）和任选具有三个以上选自羧基，羟基的多官能化合物（D）反应而得到的0〜5mgKOH / g ，和/或其酯基。 该组合物具有优异的成型性，适用于包括吹塑成型在内的成型技术，而不会引起任何麻烦。 耐热性，耐水性，耐冲击性或阻燃性令人满意，具有橡胶状弹性。
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公开(公告)号：US20130131216A1
公开(公告)日：2013-05-23
申请号：US13812583
申请日：2011-07-20
申请人： Masanori Sakane
发明人： Masanori Sakane
IPC分类号： C09D163/00
CPC分类号： C09D163/00 , C08G59/24 , C08G59/68 , C08K5/51 , C08L63/00 , C08L67/00 , H01L23/293 , H01L2924/0002 , H01L2924/00
摘要： Disclosed is a liquid thermosetting epoxy resin composition including a base resin, a curing agent (D), and curing accelerator (E) or including a base resin and a curing catalyst (D′), each base resin including an alicyclic epoxy compound (A) having at least one alicyclic skeleton and two or more epoxy groups per molecule; a polyester polyol and/or a polycarbonate polyol (B), each polyol having two or more terminal hydroxyl groups; and a phosphorous ester (C). The liquid thermosetting epoxy resin composition exhibits excellent viscosity stability and can give a cured article which is homogeneous even when having a large thickness, does not crack under heat cycle conditions, and is highly thermally stable and satisfactorily optically transparent.
摘要翻译： 公开了包含基础树脂，固化剂（D）和固化促进剂（E）或包括基础树脂和固化催化剂（D'）的液体热固性环氧树脂组合物，每种基础树脂包括脂环族环氧化合物（A ）每分子具有至少一个脂环骨架和两个或更多个环氧基团; 聚酯多元醇和/或聚碳酸酯多元醇（B），每个多元醇具有两个或多个末端羟基; 和磷酯（C）。 液态热固性环氧树脂组合物表现出优异的粘度稳定性，并且即使在厚度较大的情况下也能均匀的固化物，在热循环条件下不会发生裂纹，而且热稳定性高，光学透明性好。
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公开(公告)号：US20130241086A1
公开(公告)日：2013-09-19
申请号：US13883297
申请日：2011-11-09
申请人： Masanori Sakane
发明人： Masanori Sakane
CPC分类号： C08K3/36 , C08G59/24 , C08K5/52 , C08L63/00 , H01L23/29 , H01L23/293 , H01L2924/0002 , H01L2924/00
摘要： Disclosed is a liquid curable epoxy resin composition which includes a cycloaliphatic epoxy compound (A) having at least one alicyclic skeleton and two or more epoxy groups per molecule; a silica (B); and a phosphite ester (C). The liquid curable epoxy resin composition preferably includes, for example, 5 to 80 parts by weight of the cycloaliphatic epoxy compound (A) having at least one alicyclic skeleton and two or more epoxy groups per molecule; 20 to 95 parts by weight of the silica (B); and 0.001 to 5.0 parts by weight of the phosphite ester (C), per 100 parts by weight of the total amount of the components (A) and (B).
摘要翻译： 公开了一种液体固化型环氧树脂组合物，其包含每分子具有至少一个脂环骨架和两个或更多个环氧基团的脂环族环氧化合物（A） 二氧化硅（B）; 和亚磷酸酯（C）。 液固环氧树脂组合物优选包含例如每分子具有至少一个脂环骨架和两个或更多个环氧基团的脂环族环氧化合物（A）5至80重量份; 20〜95重量份二氧化硅（B）; 和0.001〜5.0重量份的亚磷酸酯（C），相对于成分（A）和（B）的总量100重量份。
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公开(公告)号：US20090163674A1
公开(公告)日：2009-06-25
申请号：US12086290
申请日：2006-11-21
申请人： Masanori Sakane , Akihiro Yabui
发明人： Masanori Sakane , Akihiro Yabui
IPC分类号： C08G63/91
CPC分类号： C08L67/00 , C08L63/00 , C08L79/00 , C08L2205/03 , C08L2666/20 , C08L2666/02 , C08L2666/18 , C08L2666/22
摘要： A polyester-series resin composition comprises (A) a polyester block copolymer and (C) a polycarbodiimide compound, and if necessary (B) a polyepoxy compound. The copolymer (A) is obtainable by reaction of (a1) a crystalline aromatic polyester and (a2) a lactone, and if necessary (a3) at least one compound selected from the group consisting of a polycarboxylic acid or an ester-formable derivative thereof and a polyol or an ester-formable derivative thereof in the presence of a phosphorous ester. Such a resin composition is particularly excellent in recycling efficiency and is useful for blow molding. The resin composition has a high hydrolysis resistance and an excellent heat resistance (particularly thermal cycling resistance).
摘要翻译： 聚酯系树脂组合物包含（A）聚酯嵌段共聚物和（C）聚碳二亚胺化合物，如果需要（B）聚环氧化合物。 共聚物（A）可以通过（a1）结晶性芳香族聚酯和（a2）内酯的反应获得，并且根据需要（a3）至少一种选自多羧酸或其可形成酯的衍生物的化合物 和多元醇或其可形成酯的衍生物在磷酸酯存在下进行。 这种树脂组合物的再循环效率特别优异，可用于吹塑。 树脂组合物具有高耐水解性和优异的耐热性（特别是耐热循环性）。
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