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公开(公告)号：US07312363B2
公开(公告)日：2007-12-25
申请号：US10502803
申请日：2003-02-06
CPC分类号： C08G65/2696 , B01J27/26 , C08G65/2663
摘要： The present invention relates to a process for reacting epoxides with an initiator compound in the presence of a double metal cyanide compound as a catalyst, said process having a shortened induction period, and the double metal cyanide compound being activated by adding the epoxide to a mixture of double metal cyanide compound and initiator compound at an internal reactor pressure of less than 1 bar, and also to the polyethers themselves obtainable by such a process.
摘要翻译： 本发明涉及一种在双金属氰化物化合物作为催化剂存在下使环氧化物与引发剂化合物反应的方法，所述方法具有缩短的诱导期，并且双金属氰化物通过向混合物中加入环氧化物而被活化 的双金属氰化物化合物和引发剂化合物，其内反应器压力小于1巴，以及可通过这种方法获得的聚醚。
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公开(公告)号：US07470823B2
公开(公告)日：2008-12-30
申请号：US10506601
申请日：2003-03-10
CPC分类号： C10L1/1985 , C08G65/2609 , C08G65/2663 , C10L1/143 , C10L1/2383 , C10L10/04
摘要： The present invention relates to polyethers which are obtainable from 1 -butene oxide and an alcohol using a double metal cyanide compound as a catalyst and have a content of unsaturated components of 6 mol% or more, to a process for preparing such a polyether and also to the use of a polyether according to the invention as a carrier oil or in a carrier oil formulation, in particular in additive packages for gasoline fuels, and furthermore also to carrier oil formulations and also to fuels comprising a polyether according to the invention.
摘要翻译： 本发明涉及可由1-丁烯氧化物得到的聚醚和使用双金属氰化物化合物作为催化剂并且具有6mol％以上的不饱和成分含量的醇与制备这种聚醚的方法 涉及使用根据本发明的聚醚作为载体油或载体油制剂，特别是用于汽油燃料的添加剂包，以及载体油制剂，以及包含根据本发明的聚醚的燃料。
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3.发明授权公开(公告)号：US07348460B2
公开(公告)日：2008-03-25
申请号：US10527529
申请日：2003-04-25
CPC分类号： C11D1/72 , B01F17/0021 , B01F17/0028 , B01J27/26 , C07C41/03 , C08G65/2609 , C08G65/2663 , C07C43/11 , C07C43/13
摘要： The present invention relates to a process for preparing at least one alkoxylate, which comprises bringing at least one alkylene oxide selected from the group consisting of ethylene oxide, propylene oxide, butylene oxide, pentylene oxide and decene oxide into contact with at least one starter compound in the presence of at least one double metal cyanide compound, with the reaction being carried out at a temperature of from 130° C. to 155° C., to the alkoxylates, in particular ethoxylates, themselves and to the use of such ethoxylates as emulsifier, foam regulator or as wetting agents for hard surfaces.
摘要翻译： 本发明涉及一种制备至少一种烷氧基化物的方法，其包括使至少一种选自环氧乙烷，环氧丙烷，环氧丁烷，环氧丁烷和氧化烯的环氧烷与至少一种起始化合物 在至少一种双金属氰化物化合物的存在下，反应在130℃至155℃的温度下进行至烷氧基化物，特别是乙氧基化物本身，以及使用这样的乙氧基化物如 乳化剂，泡沫调节剂或作为硬表面的润湿剂。
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4.发明授权Process for the copolymerization of alkylene oxides and carbon dioxide using suspensions of multi-metal cyanide compounds 有权使用多金属氰化物化合物的悬浮液进行环氧烷和二氧化碳的共聚方法公开(公告)号：US06762278B2
公开(公告)日：2004-07-13
申请号：US10066855
申请日：2002-02-04
IPC分类号： C08G6434
CPC分类号： C08G18/44 , C08G18/7621 , C08G64/34 , C08G65/2603 , C08G65/2663 , C08G2101/0083
摘要： A method of forming a polyethercarbonate polyol using a multimetal cyanide compound is disclosed. The method includes providing a multimetal cyanide compound having a crystalline structure and a content of platelet-shaped particles of at least 30% by weight, based on the weight of the multimetal cyanide compound and further including at least two of the following components: an organic complexing agent, water, a polyether, and a surface-active substance. Then an alcohol initiator is reacted with at least one alkylene oxide and carbon dioxide under a positive pressure in the presence of the multimetal cyanide compound, thereby forming the polyethercarbonate polyol.
摘要翻译： 公开了使用多金属氰化合物形成聚醚碳酸酯多元醇的方法。 该方法包括提供具有基于多金属氰化合物的重量至少30重量％的晶体结构和片状颗粒的含量的多金属氰化合物，并且还包括以下组分中的至少两种：有机 络合剂，水，聚醚和表面活性物质。 然后在多金属氰化合物的存在下，在正压下使醇引发剂与至少一种烯化氧和二氧化碳反应，从而形成聚醚碳酸酯多元醇。
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5.发明授权公开(公告)号：US07196030B2
公开(公告)日：2007-03-27
申请号：US10528414
申请日：2003-04-25
IPC分类号： C08F4/02
CPC分类号： C11D1/72 , B01J27/26 , B01J37/03 , C07C41/03 , C08G65/2609 , C08G65/2663 , C07C43/11
摘要： The present invention relates to a process for the preparation of at least one alkoxylate comprising the bringing into contact of an alkylene oxide mixture at least comprising ethylene oxide with at least one starter compound in the presence of at least one double-metal cyanide compound, where, during the induction phase, the sum of inert gas partial pressure and ethylene oxide partial pressure is 1.5 bar to 6.0 bar, to the alkoxylates obtainable by such a process, and to the use of such alkoxylates as emulsifier, foam regulator or as wetting agent for hard surfaces.
摘要翻译： 本发明涉及一种制备至少一种烷氧基化物的方法，其包括在至少一种双金属氰化物化合物的存在下使至少包含环氧乙烷的环氧烷烃与至少一种起始化合物接触，其中 在诱导阶段，惰性气体分压和环氧乙烷分压的总和为1.5巴至6.0巴，可通过这种方法获得的烷氧基化物，以及使用这种烷氧基化物作为乳化剂，泡沫调节剂或作为润湿剂 用于硬表面。
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公开(公告)号：US06764978B2
公开(公告)日：2004-07-20
申请号：US10229979
申请日：2002-08-28
申请人： Georg Heinrich Grosch , Edward Bohres , Raimund Ruppel , Kathrin Harre , Eva Baum , Michael Stösser , Jeffery T. Miller , Richard B. Prager
发明人： Georg Heinrich Grosch , Edward Bohres , Raimund Ruppel , Kathrin Harre , Eva Baum , Michael Stösser , Jeffery T. Miller , Richard B. Prager
IPC分类号： B01J2726
CPC分类号： B01J35/002 , B01J27/26 , C08G65/2663
摘要： The invention relates to DMC catalysts which comprise at least 10% by weight, based on the weight of the DMC catalysts, of a crystalline multimetal cyanide compound whose X-ray diffractogram shows sharp reflections at least at the d values of 11.4 ű0.5 Å 8.9 ű0.5 Å 6.3 ű0.5 Å 5.8 ű0.5 Å 5.5 ű0.5 Å 4.5 ű0.5 Å 4.4 ű0.5 Å 3.9 ű0.4 Å 3.7 ű0.4 Å 3.4 ű0.4 Å.
摘要翻译： 本发明涉及DMC催化剂，其基于DMC催化剂的重量计至少10重量％的结晶多金属氰化物化合物，其X射线衍射图至少在d值为±0.4±0.5时显示出尖锐的反射 Å8.9ű0.5Å6.3ű0.5Å5.8ű0.5Å5.5ű0.5Å4.5ű0.5Å4.4ű0.5Å3.9ű0.4Å3.7ű0.4Å3。 4ű0.4Å。
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公开(公告)号：US07342140B2
公开(公告)日：2008-03-11
申请号：US10526937
申请日：2003-09-11
申请人： Edward Bohres , Hartmut Hibst , Michael Stoesser , Raimund Ruppel , Eva Baum
发明人： Edward Bohres , Hartmut Hibst , Michael Stoesser , Raimund Ruppel , Eva Baum
IPC分类号： C07C43/00
CPC分类号： C08G65/2645 , C08G65/266
摘要： The present invention relates to a process for preparing a polyetherol which comprises reacting at least one alkylene oxide with at least one starter compound in the presence of a catalyst of the formula I: M1p[M2qOn(OH)2(3-n)]x, (I) and to the polyetherols prepared by such a process and to their use for the synthesis of polyurethanes, as fuel additive or as surfactant.
摘要翻译： 本发明涉及一种制备聚己二醇的方法，该方法包括在式I的催化剂存在下使至少一种环氧烷与至少一种起始化合物反应：<？in-line-formula description =“In-Line Formulas “end =”lead“？> M （I）<？in-line-formula description =“In-line Formulas”end =“tail（”）“（OH）2（3-n） “以及通过这种方法制备的聚醚酯，以及它们用于合成聚氨酯，作为燃料添加剂或作为表面活性剂的用途。
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公开(公告)号：US20050159627A1
公开(公告)日：2005-07-21
申请号：US10502803
申请日：2003-02-06
申请人： Michael Stosser , Edward Bohres , Georg Grosch , Wilfried Sager
发明人： Michael Stosser , Edward Bohres , Georg Grosch , Wilfried Sager
CPC分类号： C08G65/2696 , B01J27/26 , C08G65/2663
摘要： The present invention relates to a process for reacting epoxides with an initiator compound in the presence of a double metal cyanide compound as a catalyst, said process having a shortened induction period, and the double metal cyanide compound being activated by adding the epoxide to a mixture of double metal cyanide compound and initiator compound at an internal reactor pressure of less than 1 bar, and also to the polyethers themselves obtainable by such a process.
摘要翻译： 本发明涉及一种在双金属氰化物化合物作为催化剂存在下使环氧化物与引发剂化合物反应的方法，所述方法具有缩短的诱导期，并且双金属氰化物通过向混合物中加入环氧化物而被活化 的双金属氰化物化合物和引发剂化合物，其内反应器压力小于1巴，以及可通过这种方法获得的聚醚。
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公开(公告)号：US20050159628A1
公开(公告)日：2005-07-21
申请号：US10506601
申请日：2003-03-10
申请人： Michael Stosser , Edward Bohres , Georg Grosch , Wilfried Sager , Marc Walter
发明人： Michael Stosser , Edward Bohres , Georg Grosch , Wilfried Sager , Marc Walter
IPC分类号： C10L1/192 , C08G65/26 , C08G65/28 , C08L71/08 , C10L1/14 , C10L1/18 , C10L1/198 , C10L1/22 , C10L10/04 , C07C41/03
CPC分类号： C10L1/1985 , C08G65/2609 , C08G65/2663 , C10L1/143 , C10L1/2383 , C10L10/04
摘要： The present invention relates to polyethers which are obtainable from 1-butene oxide and an alcohol using a double metal cyanide compound as a catalyst and have a content of unsaturated components of 6 mol % or more, to a process for preparing such a polyether and also to the use of a polyether according to the invention as a carrier oil or in a carrier oil formulation, in particular in additive packages for gasoline fuels, and furthermore also to carrier oil formulations and also to fuels comprising a polyether according to the invention.
摘要翻译： 本发明涉及可从1-丁烯氧化物获得的聚醚和使用双金属氰化物化合物作为催化剂并具有6mol％以上的不饱和组分含量的醇与制备这种聚醚的方法 涉及使用根据本发明的聚醚作为载体油或载体油制剂，特别是用于汽油燃料的添加剂包，以及载体油制剂，以及包含根据本发明的聚醚的燃料。
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10.发明授权Process for the alkoxylation of organic compounds in the presence of novel framework materials 失效有机化合物在新型骨架材料存在下的烷氧基化方法公开(公告)号：US07279517B2
公开(公告)日：2007-10-09
申请号：US10492192
申请日：2002-10-18
申请人： Ulrich Mueller , Michael Stoesser , Raimund Ruppel , Eva Baum , Edward Bohres , Marcus Sigl , Lisa Lobree , Omar M. Yaghi , Mohamed Eddaoudi
发明人： Ulrich Mueller , Michael Stoesser , Raimund Ruppel , Eva Baum , Edward Bohres , Marcus Sigl , Lisa Lobree , Omar M. Yaghi , Mohamed Eddaoudi
CPC分类号： C08G65/266 , C08G18/48
摘要： The present invention relates to a process for the alkoxylation of organic compounds comprising the reaction of at least one organic compound with at least one alkoxylating agent in the presence of a catalyst system, wherein a polyether alcohol is obtained. The catalyst system comprises a metallo organic framework mate-rial comprising pores and at least one metal ion and at least one at least bidentate organic compound, which is coordinately bounded to said metal ion. Furthermore it relates to polyurethanes or polyurethane foams, which are obtainable by using a prepared polyether alcohol as a starting material.
摘要翻译： 本发明涉及有机化合物的烷氧基化方法，包括在催化剂体系存在下使至少一种有机化合物与至少一种烷氧基化剂反应，其中获得聚醚醇。 催化剂体系包括金属有机骨架材料，其包含孔和至少一种金属离子以及与所述金属离子配位结合的至少一种至少二齿有机化合物。 此外，它涉及可通过使用制备的聚醚醇作为原料获得的聚氨酯或聚氨酯泡沫。
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