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    Process For Preparing Acylglycinates By Means Of Direct Oxidation
    1.
    发明申请
    Process For Preparing Acylglycinates By Means Of Direct Oxidation 有权
    通过直接氧化制备酰基甘氨酸的方法

    公开(公告)号：US20100286418A1

    公开(公告)日：2010-11-11

    申请号：US12377835

    申请日：2007-08-13

    申请人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Thielecke ,  Klaus-Dieter Vorlop

    发明人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Thielecke ,  Klaus-Dieter Vorlop

    IPC分类号： C07C231/12

    CPC分类号： C07C231/14 ,  C07C233/47 ,  C07C233/49

    摘要： A process is described for preparing acylglycinate salts of the formula (II) in which R1 is a saturated linear or branched alkyl radical having from 1 to 21 carbon atoms or a mono- or polyunsaturated linear or branched alkenyl radical having from 2 to 21 carbon atoms, and B is a cation derived from a base, and/or the corresponding protonated acylglycines, characterized in that one or more fatty acid monoethanolamides of the formula (I) in which R1 is as defined above is oxidized with oxygen in the presence of a transition group metal catalyst in an alkaline medium to give one or more acylglycinate salts of the formula (II), and, in the case of preparation of the protonated acylglycines, the acylglycinate salt(s) of the formula (II) is additionally reacted with an acid.

    摘要翻译： 描述了制备式（II）的酰基甘氨酸盐的方法，其中R 1是具有1至21个碳原子的饱和直链或支链烷基或具有2至21个碳原子的单或多不饱和直链或支链烯基 ，和B是衍生自碱的阳离子和/或相应的质子化酰基甘氨酸，其特征在于，其中R 1如上定义的一种或多种式（I）的一种或多种脂肪酸单乙醇酰胺在氧气存在下被氧化 在碱性介质中的过渡族金属催化剂，得到一种或多种式（II）的酰基甘氨酸盐，并且在制备质子化酰基甘氨酸的情况下，式（II）的酰基甘氨酸盐另外与 酸。

    Method For The Production Of Acyl Glycinates By Means Of Direct Oxidation
    2.
    发明申请
    Method For The Production Of Acyl Glycinates By Means Of Direct Oxidation 有权
    通过直接氧化生产酰基甘氨酸的方法

    公开(公告)号：US20100305358A1

    公开(公告)日：2010-12-02

    申请号：US12812011

    申请日：2009-01-07

    申请人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    发明人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    IPC分类号： C07C51/235

    CPC分类号： C07C231/12 ,  C07C233/47

    摘要： A method is described for producing acyl glycinate salts of formula (II) in which R1 represents a saturated linear or branched alkyl radical comprising 1 to 21 carbon atoms or a monounsaturated or polyunsaturated linear or branched alkenyl radical comprising 2 to 21 carbon atoms, and B represents a cation, and/or the corresponding protonated acyl glycinic acid. Said method is characterized in that one or more fatty acid monoethanol amides of formula (I) in which R1 has the meaning indicated above is/are oxidized with oxygen in the presence of an optionally supported bimetallic catalyst consisting of gold and a metal from group VIII of the periodic table in the alkaline medium in order to obtain one or more acyl glycinate salts of formula (II). In order to produce the protonated acyl glycinic acids, the acyl glycinate salt/s of formula (II) is/are additionally reacted with an acid.

    摘要翻译： 描述了制备式（II）的酰基甘氨酸盐的方法，其中R 1表示包含1至21个碳原子的饱和直链或支链烷基或包含2至21个碳原子的单不饱和或多不饱和直链或支链烯基，B 表示阳离子，和/或相应的质子化酰基甘氨酸。 所述方法的特征在于，其中R1具有上述含义的一种或多种式（I）的一种或多种脂肪酸单乙醇酰胺在由金和金属组成的任选负载的双金属催化剂存在下用氧氧化 的碱性介质中的周期表，以获得一种或多种式（II）的酰基甘氨酸盐。 为了产生质子化的酰基乙二酸，式（II）的酰基甘氨酸盐/另外与酸反应。

    Method for the production of acyl glycinates by means of direct oxidation
    3.
    发明授权
    Method for the production of acyl glycinates by means of direct oxidation 有权
    通过直接氧化生产酰基甘氨酸盐的方法

    公开(公告)号：US08350080B2

    公开(公告)日：2013-01-08

    申请号：US12812011

    申请日：2009-01-07

    申请人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    发明人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    IPC分类号： C07C231/12

    CPC分类号： C07C231/12 ,  C07C233/47

    摘要： A method is described for producing acyl glycinate salts of formula (II) in which R1 represents a saturated linear or branched alkyl radical comprising 1 to 21 carbon atoms or a monounsaturated or polyunsaturated linear or branched alkenyl radical comprising 2 to 21 carbon atoms, and B represents a cation, and/or the corresponding protonated acyl glycinic acid. Said method is characterized in that one or more fatty acid monoethanol amides of formula (I) in which R1 has the meaning indicated above is/are oxidized with oxygen in the presence of an optionally supported bimetallic catalyst consisting of gold and a metal from group VIII of the periodic table in the alkaline medium in order to obtain one or more acyl glycinate salts of formula (II). In order to produce the protonated acyl glycinic acids, the acyl glycinate salt/s of formula (II) is/are additionally reacted with an acid.

    摘要翻译： 描述了制备式（II）的酰基甘氨酸盐的方法，其中R 1表示包含1至21个碳原子的饱和直链或支链烷基或包含2至21个碳原子的单不饱和或多不饱和直链或支链烯基，B 表示阳离子，和/或相应的质子化酰基甘氨酸。 所述方法的特征在于，其中R1具有上述含义的一种或多种式（I）的一种或多种脂肪酸单乙醇酰胺在由金和金属组成的任选负载的双金属催化剂存在下用氧氧化 的碱性介质中的周期表，以获得一种或多种式（II）的酰基甘氨酸盐。 为了产生质子化的酰基乙二酸，式（II）的酰基甘氨酸盐/另外与酸反应。

    Process for preparing acylglycinates by means of direct oxidation
    4.
    发明授权
    Process for preparing acylglycinates by means of direct oxidation 有权
    通过直接氧化制备酰基甘氨酸盐的方法

    公开(公告)号：US08093414B2

    公开(公告)日：2012-01-10

    申请号：US12377835

    申请日：2007-08-13

    申请人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    发明人： Peter Klug ,  Achim Stankowiak ,  Oliver Franke ,  Franz-Xaver Scherl ,  Ulf Pruesse ,  Nadine Decker ,  Klaus-Dieter Vorlop

    IPC分类号： C07C231/00

    CPC分类号： C07C231/14 ,  C07C233/47 ,  C07C233/49

    摘要： A process is described for preparing acylglycinate salts of the formula (II) in which R1 is a saturated linear or branched alkyl radical having from 1 to 21 carbon atoms or a mono- or polyunsaturated linear or branched alkenyl radical having from 2 to 21 carbon atoms, and B is a cation derived from a base, and/or the corresponding protonated acylglycines, characterized in that one or more fatty acid monoethanolamides of the formula (I) in which R1 is as defined above is oxidized with oxygen in the presence of a transition group metal catalyst in an alkaline medium to give one or more acylglycinate salts of the formula (II), and, in the case of preparation of the protonated acylglycines, the acylglycinate salt(s) of the formula (II) is additionally reacted with an acid.

    摘要翻译： 描述了制备式（II）的酰基甘氨酸盐的方法，其中R 1是具有1至21个碳原子的饱和直链或支链烷基或具有2至21个碳原子的单或多不饱和直链或支链烯基 ，和B是衍生自碱的阳离子和/或相应的质子化酰基甘氨酸，其特征在于，其中R 1如上定义的一种或多种式（I）的一种或多种脂肪酸单乙醇酰胺在氧气存在下被氧化 在碱性介质中的过渡族金属催化剂，得到一种或多种式（II）的酰基甘氨酸盐，并且在制备质子化酰基甘氨酸的情况下，式（II）的酰基甘氨酸盐另外与 酸。

    Phosphoric acid esters containing phosphorus atoms bridged by diol units
    7.
    发明授权
    Phosphoric acid esters containing phosphorus atoms bridged by diol units 失效
    含有由二醇单元桥连的磷原子的磷酸酯

    公开(公告)号：US08686033B2

    公开(公告)日：2014-04-01

    申请号：US12671422

    申请日：2008-07-29

    申请人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    发明人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    IPC分类号： A61K33/42 ,  C07F9/02

    CPC分类号： C08G65/327 ,  A61K8/86 ,  A61K8/90 ,  A61K2800/48 ,  A61K2800/52 ,  A61Q5/02 ,  A61Q19/00 ,  C08G65/3312 ,  C08G65/3353 ,  C08L71/02

    摘要： Phosphoric esters comprise A) one or more structural units derived from substances of component a), the substances of component a) being selected from orthophosphoric acid and one or more of its derivatives, B) one or more structural units derived from substances of component b), the substances of component b) being selected from one or more compounds of formula (I) R2—O—(CH2CH2O)u(C3H6O)v(DO)w—H  (I) and C) one or more structural units derived from substances of component c), the substances of component c) being selected from one or more diols of formula (II) HO—(CH2CH2O)a(C3H6O)b(DO)c—H  (II) where the sum total a+b+c is ≧1, and the phosphoric ester contains 2 or more phosphorus atoms per molecule which are bridged via a structural unit derived from the compounds of formula (II). The phosphoric esters of the invention are very useful in the manufacture of cosmetic, pharmaceutical and dermatological compositions.

    摘要翻译： 磷酸酯包括A）一种或多种衍生自组分a）的物质的结构单元，组分a）的物质选自正磷酸及其一种或多种衍生物，B）一种或多种衍生自组分b的物质的结构单元 ），组分b）的物质选自一种或多种式（I）R 2 -O-（CH 2 CH 2 O）u（C 3 H 6 O）v（DO）w-H（I））的化合物和C）一种或多种衍生的结构单元 从组分c）的物质中，组分c）的物质选自一种或多种式（II）的二醇HO-（CH 2 CH 2 O）a（C 3 H 6 O）b（DO）c-H（II），其中总和a + b + c为≥1，磷酸酯每分子含有2个以上的磷原子，该磷原子通过衍生自式（II）化合物的结构单元桥连。 本发明的磷酸酯在制造化妆品，药​​物和皮肤病学组合物中非常有用。

    Phosphoric Acid Esters Containing Phosphorus Atoms Bridged By Diol Units
    8.
    发明申请
    Phosphoric Acid Esters Containing Phosphorus Atoms Bridged By Diol Units 失效
    含有由二醇单元桥接的磷原子的磷酸酯

    公开(公告)号：US20110003010A1

    公开(公告)日：2011-01-06

    申请号：US12671422

    申请日：2008-07-29

    申请人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    发明人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    IPC分类号： A61K31/765 ,  C07F9/11 ,  A61K8/86 ,  A61K8/55 ,  A61K31/6615 ,  A61K31/661 ,  A61P31/00 ,  A61K33/40 ,  A61Q5/00 ,  A61Q19/00 ,  A61Q15/00 ,  A61Q1/00 ,  C11D3/36 ,  A61Q19/10

    CPC分类号： C08G65/327 ,  A61K8/86 ,  A61K8/90 ,  A61K2800/48 ,  A61K2800/52 ,  A61Q5/02 ,  A61Q19/00 ,  C08G65/3312 ,  C08G65/3353 ,  C08L71/02

    摘要： Phosphoric esters comprise A) one or more structural units derived from substances of component a), the substances of component a) being selected from orthophosphoric acid and one or more of its derivatives, B) one or more structural units derived from substances of component b), the substances of component b) being selected from one or more compounds of formula (I) R2—O—(CH2CH2O)u(C3H6O)v(DO)w—H  (I) and C) one or more structural units derived from substances of component c), the substances of component c) being selected from one or more diols of formula (II) HO—(CH2CH2O)a(C3H6O)b(DO)c—H  (II) where the sum total a+b+c is ≧1 and the phosphoric ester contains 2 or more phosphorus atoms per molecule which are bridged via a structural unit derived from the compounds of formula (II).The phosphoric esters of the invention are very useful in the manufacture of cosmetic, pharmaceutical and dermatological compositions.

    摘要翻译： 磷酸酯包括A）一种或多种衍生自组分a）的物质的结构单元，组分a）的物质选自正磷酸及其一种或多种衍生物，B）一种或多种衍生自组分b的物质的结构单元 ），组分b）的物质选自一种或多种式（I）R 2 -O-（CH 2 CH 2 O）u（C 3 H 6 O）v（DO）w-H（I））的化合物和C）一种或多种衍生的结构单元 从组分c）的物质中，组分c）的物质选自一种或多种式（II）的二醇HO-（CH 2 CH 2 O）a（C 3 H 6 O）b（DO）c-H（II），其中总和a + b + c为≥1，磷酸酯每分子含有2个或更多个磷原子，该磷原子通过衍生自式（II）化合物的结构单元桥连。 本发明的磷酸酯在制造化妆品，药​​物和皮肤病学组合物中非常有用。

    Aqueous Compositions Containing Alkoxylated Phosphoric Acid Triesters
    9.
    发明申请
    Aqueous Compositions Containing Alkoxylated Phosphoric Acid Triesters 审中-公开
    含有烷氧基化磷酸三酯的水性组合物

    公开(公告)号：US20100260696A1

    公开(公告)日：2010-10-14

    申请号：US12671441

    申请日：2008-07-29

    申请人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    发明人： Peter Klug ,  Franz-Xaver Scherl ,  Waltraud Simsch ,  Adelgunde Oberhauser

    IPC分类号： A61K8/55 ,  A61K47/24 ,  A61Q15/00 ,  A61P17/00 ,  A61P43/00

    CPC分类号： C08L71/02 ,  A61K8/86 ,  A61Q1/14 ,  A61Q5/02 ,  A61Q15/00 ,  A61Q17/04 ,  A61Q19/00 ,  A61Q19/02 ,  A61Q19/04 ,  A61Q19/08 ,  A61Q19/10 ,  B01F17/0064 ,  C08G65/327 ,  C08G65/3312 ,  C08G65/3353

    摘要： The invention relates to compositions containing A) at least one phosphoric acid ester of formula (I) wherein R1, R2 and R3 can be the same or different and stand for a linear or branched, saturated alkyl group comprising between 6 and 30 carbon atoms, a linear or branched, monounsaturated or polyunsaturated alkenyl group comprising between 6 and 30 carbon atoms, or an aryl group that can be substituted with between 1 and 3 branched alkyl groups each independently containing between 3 and 18 carbon atoms, the individual groups (OA1)x, (A2O)y and (A3O)z each independently consisting of units selected from CH2CH2O, C3H6O and C4H8O, the units CH2CH2O, C3H6O and C4H8O being arranged inside the individual groups (OA1)X, (A2O)y and (A3O), in blocks or in a statistically distributed manner, and x, y and z each independently standing for a number between 30 and 150, and B); water in a proportion of >50.0 wt. % in relation to the finished composition. The compositions according to the invention are preferably cosmetic, pharmaceutical or dermatological compositions.

    摘要翻译： 本发明涉及包含A）至少一种式（I）的磷酸酯的组合物，其中R 1，R 2和R 3可以相同或不同，代表包含6至30个碳原子的直链或支链饱和烷基， 包含6至30个碳原子的直链或支链单不饱和或多不饱和链烯基，或可被1至3个各自独立地含有3至18个碳原子的支链烷基取代的芳基，各基团（OA1） x，（A 2 O）y和（A3O）z各自独立地由选自CH 2 CH 2 O，C 3 H 6 O和C 4 H 8 O的单元组成，单元CH 2 CH 2 O，C 3 H 6 O和C 4 H 8 O设置在各组（OA1）X，（A2O）y和（A3O） 以块或统计分布的方式，x，y和z各自独立地代表30到150之间的数字，B）; 水比例> 50.0wt。 相对于成品组成的百分比。 根据本发明的组合物优选为化妆品，药​​物或皮肤病学组合物。