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公开(公告)号：US20070100168A1
公开(公告)日：2007-05-03
申请号：US10581802
申请日：2004-12-14
申请人： Rainer Papp , Rocco Paciello , Christoph Benisch
发明人： Rainer Papp , Rocco Paciello , Christoph Benisch
IPC分类号： C07C45/49
CPC分类号： C07C209/26 , C07C29/141 , C07C47/347 , C07C2603/68 , C07C211/19 , C07C31/278
摘要： Process for preparing tricyclodecanedialdehyde by hydroformylation of dicyclopentadiene by means of a CO/H2 mixture at elevated temperature and under superatmospheric pressure in the presence of a rhodium catalyst which has not been modified by means of a ligand and is homogeneously dissolved in the hydroformylation medium, wherein the hydroformylation is carried out at a pressure of from 200 to 350 bar in at least two reaction zones, with a reaction temperature of from 80 to 120° C. being set in a first reaction zone and a reaction temperature of from 120 to 150° C. being set in a reaction zone following this reaction zone, with the proviso that the reaction temperature in the subsequent reaction zone is at least 5° C. higher than in the preceding reaction zone.
摘要翻译： 在高温和超大气压下，在没有通过配体修饰的铑催化剂存在下，通过二环戊二烯加氢甲酰化二环戊二烯制备三环癸二醛的方法， 均匀地溶解在加氢甲酰基化介质中，其中加氢甲酰化在至少两个反应区中在200-350巴的压力下进行，反应温度为80-120℃设定在第一反应区和 在该反应区之后的反应区中设置120至150℃的反应温度，条件是后续反应区中的反应温度比前述反应区高至少5℃。
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公开(公告)号：US07321068B2
公开(公告)日：2008-01-22
申请号：US10581802
申请日：2004-12-14
申请人： Rainer Papp , Rocco Paciello , Christoph Benisch
发明人： Rainer Papp , Rocco Paciello , Christoph Benisch
IPC分类号： C07C45/50 , C07C35/21 , C07C209/00
CPC分类号： C07C209/26 , C07C29/141 , C07C47/347 , C07C2603/68 , C07C211/19 , C07C31/278
摘要： Process for preparing tricyclodecanedialdehyde by hydroformylation of dicyclopentadiene by means of a CO/H2 mixture at elevated temperature and under superatmospheric pressure in the presence of a rhodium catalyst which has not been modified by means of a ligand and is homogeneously dissolved in the hydroformylation medium, wherein the hydroformylation is carried out at a pressure of from 200 to 350 bar in at least two reaction zones, with a reaction temperature of from 80 to 120° C. being set in a first reaction zone and a reaction temperature of from 120 to 150° C. being set in a reaction zone following this reaction zone, with the proviso that the reaction temperature in the subsequent reaction zone is at least 5° C. higher than in the preceding reaction zone.
摘要翻译： 在高温和超大气压下，在没有通过配体修饰的铑催化剂存在下，通过二环戊二烯加氢甲酰化二环戊二烯制备三环癸二醛的方法， 均匀地溶解在加氢甲酰基化介质中，其中加氢甲酰化在至少两个反应区中在200-350巴的压力下进行，反应温度为80-120℃设定在第一反应区和 在该反应区之后的反应区中设置120至150℃的反应温度，条件是后续反应区中的反应温度比前述反应区高至少5℃。
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公开(公告)号：US20100048959A1
公开(公告)日：2010-02-25
申请号：US12516855
申请日：2007-11-29
申请人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
发明人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
IPC分类号： C07C45/41 , C07C29/151
CPC分类号： C07C45/50 , C07C5/2506 , C07C29/141 , C07C45/74 , C07C47/02 , C07C11/08 , C07C31/125 , C07C47/21
摘要： The present invention relates to a process for preparing hydroformylation products of olefins having at least four carbon atoms, in which a high proportion of both the linear Ci-olefins having a terminal double bond comprised in the olefin-comprising feed used and of the linear Ci-olefins having an internal double bond is converted into hydroformylation products. Furthermore, the invention relates to a process for preparing 2-propylheptanol which comprises such a hydroformylation process.
摘要翻译： 本发明涉及一种制备具有至少四个碳原子的烯烃的加氢甲酰化产物的方法，其中在所用含烯烃的原料中包含的具有末端双键的直链C 1 -C 20烯烃和线性C 1 具有内部双键的烯烃转化为加氢甲酰化产物。 此外，本发明涉及一种制备2-丙基庚醇的方法，其包括这种加氢甲酰化方法。
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4.发明申请公开(公告)号：US20060224000A1
公开(公告)日：2006-10-05
申请号：US10576282
申请日：2004-10-22
CPC分类号： B01J31/186 , B01J2231/321 , B01J2531/0238 , B01J2531/822 , C07C45/50 , C07C47/02
摘要： The present invention relates to a process for the hydroformylation of ethylenically unsaturated compounds by reaction with carbon monoxide and hydrogen in the presence of a catalytically active fluid which comprises a dissolved metal complex of a metal of transition group VIII of the Periodic Table of the Elements with at least one phosphoramidite compound as ligand, wherein the fluid is brought into contact with a base.
摘要翻译： 本发明涉及通过在催化活性流体存在下与一氧化碳和氢气反应来进行烯键式不饱和化合物的加氢甲酰基化的方法，该催化活性流体包含元素周期表的第八族过渡金属的金属络合物与 至少一种亚磷酰胺化合物作为配体，其中流体与碱接触。
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5.发明授权公开(公告)号：US07012162B2
公开(公告)日：2006-03-14
申请号：US10311584
申请日：2001-06-25
申请人： Thomas Mackewitz , Wolfgang Ahlers , Edgar Zeller , Michael Röper , Rocco Paciello , Rainer Papp , Konrad Knoll , Hartwig Voss
发明人： Thomas Mackewitz , Wolfgang Ahlers , Edgar Zeller , Michael Röper , Rocco Paciello , Rainer Papp , Konrad Knoll , Hartwig Voss
CPC分类号： B01J31/2466 , B01J31/20 , B01J31/2423 , B01J31/2433 , B01J2231/321 , B01J2531/80 , B01J2531/822 , C07C45/50 , C07F9/65683 , C07F15/0026 , C07F15/0053 , C07F15/0066 , C07F15/008 , C07F15/045 , C07F15/065 , C07C47/21 , C07C47/02
摘要： The invention relates to phosphacyclohexanes of general formulae I and II, wherein the following designations, among others, apply: R can represent hydrogen, C1-100-alkyl, C7-20-aralkyl, C7-20-alkaryl, and C6-12-aryl: R1 to R10 can independently represent hydrogen, C1-20-alkyl, C7-20-aralkyl, C7-20-alkaryl, and C6-12-aryl: W, W′ can independently represent single bonds or bridges comprising 1 to 20 carbon atoms, which can form part of a cyclic or aromatic group and can be interrupted by heteroatoms. Said phosphacyclohexanes are used as ligands in transition metal complexes of transition metals belonging to groups VIII to X of the periodic table.
摘要翻译： 本发明涉及通式I和II的磷杂环己烷，其中应用以下名称：R可以表示氢，C 1-100 - 烷基，C 7-20〜 C 1 -C 6烷基，C 7-20芳烷基和C 6-12 - 芳基：R 1至R 10， / SUP>可以独立地表示氢，C 1-20 - 烷基，C 7-20-20芳烷基，C 7-20 - 烷芳基， 和C 6-12 - 芳基：W，W'可以独立地表示单键或包含1至20个碳原子的桥，其可以形成环状或芳族基团的一部分并且可以被杂原子中断。 所述磷杂环己烷用作属于周期表第VIII至X族过渡金属的过渡金属络合物中的配体。
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公开(公告)号：US09266808B2
公开(公告)日：2016-02-23
申请号：US12516855
申请日：2007-11-29
申请人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
发明人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
IPC分类号： C07C29/141 , C07C45/50 , C07C5/25 , C07C45/74
CPC分类号： C07C45/50 , C07C5/2506 , C07C29/141 , C07C45/74 , C07C47/02 , C07C11/08 , C07C31/125 , C07C47/21
摘要： The present invention relates to a process for preparing hydroformylation products of olefins having at least four carbon atoms, in which a high proportion of both the linear Ci-olefins having a terminal double bond comprised in the olefin-comprising feed used and of the linear Ci-olefins having an internal double bond is converted into hydroformylation products. Furthermore, the invention relates to a process for preparing 2-propylheptanol which comprises such a hydroformylation process.
摘要翻译： 本发明涉及一种制备具有至少四个碳原子的烯烃的加氢甲酰化产物的方法，其中在所用含烯烃的原料中包含的具有末端双键的直链C 1 -C 20烯烃和线性C 1 具有内部双键的烯烃转化为加氢甲酰化产物。 此外，本发明涉及一种制备2-丙基庚醇的方法，其包括这种加氢甲酰化方法。
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7.发明授权公开(公告)号：US08110709B2
公开(公告)日：2012-02-07
申请号：US10576282
申请日：2004-10-22
CPC分类号： B01J31/186 , B01J2231/321 , B01J2531/0238 , B01J2531/822 , C07C45/50 , C07C47/02
摘要： The present invention relates to a process for the hydroformylation of ethylenically unsaturated compounds by reaction with carbon monoxide and hydrogen in the presence of a catalytically active fluid which comprises a dissolved metal complex of a metal of transition group VIII of the Periodic Table of the Elements with at least one phosphoramidite compound as ligand, wherein the fluid is brought into contact with a base.
摘要翻译： 本发明涉及通过在催化活性流体存在下与一氧化碳和氢气反应来进行烯键式不饱和化合物的加氢甲酰基化的方法，该催化活性流体包含元素周期表的第八族过渡金属的金属络合物与 至少一种亚磷酰胺化合物作为配体，其中流体与碱接触。
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8.发明授权公开(公告)号：US08232439B2
公开(公告)日：2012-07-31
申请号：US12602187
申请日：2008-05-30
申请人： Arno Lange , Klaus Seip , Ulf Dietrich , Rainer Papp
发明人： Arno Lange , Klaus Seip , Ulf Dietrich , Rainer Papp
CPC分类号： C04B20/1033 , C04B24/2611 , C04B24/36 , C04B2103/0057 , C04B2103/0075 , C04B2111/00189 , C04B24/2641 , C04B7/02
摘要： The present invention relates to the use of isoalkane mixtures for reducing or minimizing the dust emission during the handling of pulverulent construction chemistry products, a process for the preparation of the pulverulent construction chemistry products, and hydraulically setting materials comprising the isoalkane mixtures according to the invention.
摘要翻译： 本发明涉及使用异烷烃混合物来减少或最小化处理粉状建筑化学产品期间的粉尘排放，制备粉状结构化学产品的方法和包含根据本发明的异烷烃混合物的水硬定型材料 。
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9.发明授权公开(公告)号：US08124658B2
公开(公告)日：2012-02-28
申请号：US13165349
申请日：2011-06-21
申请人： Christian Bittner , Oetter Günter , Ulrich Steinbrenner , Marcus Guzmann , Andrea Haunert , Rainer Papp , Jens Rudolph
发明人： Christian Bittner , Oetter Günter , Ulrich Steinbrenner , Marcus Guzmann , Andrea Haunert , Rainer Papp , Jens Rudolph
CPC分类号： B01F17/0021 , B01F17/0042 , B01F17/0057 , C09K8/584
摘要： Surfactants of the general formula R1—X where R1 is an aliphatic C17H35-alkyl radical and X is a hydrophilic group, and the mean degree of branching of the R1 radical is from 2.8 to 3.7. Mixtures which comprise such surfactants and the use of such surfactants and of mixtures thereof for tertiary mineral oil extraction.
摘要翻译： 通式R1-X的表面活性剂，其中R1是脂族C17H35-烷基，X是亲水基团，R1基团的平均支化度为2.8-3.7。 包含这种表面活性剂的混合物以及这些表面活性剂及其混合物用于三次矿物油提取的用途。
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公开(公告)号：US06943274B2
公开(公告)日：2005-09-13
申请号：US10505705
申请日：2003-02-28
申请人： Werner Peschel , Till Adrian , Harald Rust , Arnd Böttcher , Thomas Hill , Ulrich Müller , Rainer Papp
发明人： Werner Peschel , Till Adrian , Harald Rust , Arnd Böttcher , Thomas Hill , Ulrich Müller , Rainer Papp
CPC分类号： C07C29/04 , C07C2601/14 , C07C35/08
摘要： A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.
摘要翻译： 一种通过以下步骤由苯制备环己醇的方法：a）在催化剂存在下，通过氢化苯来制备环己烯，和b）通过在催化剂存在下使环己烯水合制备环己醇，包括：进行步骤a）和b） 具有下端的底部区域，上端的顶部区域和顶部区域和底部区域之间的反应区域的反应设备，其包含根据步骤a）和b）的催化剂，蒸发一部分 苯在反应区中使用反应热，在顶部区域冷凝并将其返回到反应区，并在底部区域中抽出含有环己醇的反应混合物。
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