公开(公告)号：US20120324960A1

公开(公告)日：2012-12-27

申请号：US13583605

申请日：2011-03-10

申请人： Ralph Sattmann ,  Jan Vydra ,  Michael Huenermann

发明人： Ralph Sattmann ,  Jan Vydra ,  Michael Huenermann

IPC分类号： C03B37/027 ,  G02B6/036

CPC分类号： C03B37/02754 ,  C03B37/01211 ,  C03B37/01228 ,  C03B37/01242 ,  C03B37/018 ,  C03B37/027 ,  C03B2201/075 ,  C03B2201/12 ,  C03B2201/20 ,  C03B2201/30 ,  C03B2201/31 ,  C03B2203/22 ,  C03B2203/23 ,  C03B2205/30 ,  C03C13/045 ,  C03C2201/12 ,  G02B6/03633 ,  G02B6/0365 ,  Y10T428/2935

摘要： Methods for producing an optical fiber by elongating a silica glass blank or a coaxial group of silica glass components, on the basis of which a fiber is obtained that comprises a core zone, an inner jacket zone enclosing the core zone and a ring zone surrounding the inner jacket zone, are known. In order to provide, proceeding from this, a method, a tubular semi-finished product and a group of coaxial components for the cost-effective production of an optical fiber, which is characterized by a high quality of the boundary between the core and jacket and by low bending sensitivity, according to the invention, the silica glass of the ring zone is provided in the form of a ring zone tube made of silica glass having a mean fluorine content of at least 6000 weight ppm and the tube has an inner tube surface and an outer tube surface, wherein via the wall of the ring zone tube, a radial fluorine concentration profile is adjusted which has an inner fluorine depletion layer with a layer thickness of at least 1 μm and no more than 10 μm, in which the fluorine content decreases toward the inner tube surface and is no more than 3000 weight ppm in a region close to the surface which has a thickness of 1 μm.

摘要翻译： 通过使二氧化硅玻璃坯料或同轴的二氧化硅玻璃成分组延长来制造光纤的方法，在此基础上获得包含芯区的纤维，包围芯区的内护套区和围绕该芯区的环带 内护套区域，已知。 为了提供一种用于成本有效地生产光纤的方法，管状半成品和一组同轴部件，其特征在于芯和夹套之间的边界质量高 并且通过低弯曲灵敏度，根据本发明，环区的石英玻璃以平均氟含量为至少6000重量ppm的石英玻璃制成的环形管的形式提供，并且管具有内管 表面和外管表面，其中通过环带管的壁，调节径向氟浓度分布，其具有层厚度为至少1μm且不大于10μm的内氟耗尽层，其中 氟含量向内管表面减少，并且在接近表面厚度为1μm的区域中不超过3000重量ppm。

公开(公告)号：US09085481B2

公开(公告)日：2015-07-21

申请号：US13583605

申请日：2011-03-10

申请人： Ralph Sattmann ,  Jan Vydra ,  Michael Huenermann

发明人： Ralph Sattmann ,  Jan Vydra ,  Michael Huenermann

IPC分类号： C03B23/047 ,  C03B37/012 ,  C03B37/027 ,  C03C13/04 ,  G02B6/036

CPC分类号： C03B37/02754 ,  C03B37/01211 ,  C03B37/01228 ,  C03B37/01242 ,  C03B37/018 ,  C03B37/027 ,  C03B2201/075 ,  C03B2201/12 ,  C03B2201/20 ,  C03B2201/30 ,  C03B2201/31 ,  C03B2203/22 ,  C03B2203/23 ,  C03B2205/30 ,  C03C13/045 ,  C03C2201/12 ,  G02B6/03633 ,  G02B6/0365 ,  Y10T428/2935

摘要： Methods for producing an optical fiber by elongating a silica glass blank or a coaxial group of silica glass components, on the basis of which a fiber is obtained that comprises a core zone, an inner jacket zone enclosing the core zone and a ring zone surrounding the inner jacket zone, are known. In order to provide, proceeding from this, a method, a tubular semi-finished product and a group of coaxial components for the cost-effective production of an optical fiber, which is characterized by a high quality of the boundary between the core and jacket and by low bending sensitivity, according to the invention, the silica glass of the ring zone is provided in the form of a ring zone tube made of silica glass having a mean fluorine content of at least 6000 weight ppm and the tube has an inner tube surface and an outer tube surface, wherein via the wall of the ring zone tube, a radial fluorine concentration profile is adjusted which has an inner fluorine depletion layer with a layer thickness of at least 1 μm and no more than 10 μm, in which the fluorine content decreases toward the inner tube surface and is no more than 3000 weight ppm in a region close to the surface which has a thickness of 1 μm.

摘要翻译： 通过使二氧化硅玻璃坯料或同轴的二氧化硅玻璃成分体组织进行拉伸来制造光纤的方法，基于该光纤获得包含芯部区域的纤维，包围芯部区域的内部护套区域和围绕该区域的环形区域 内护套区域，已知。 为了提供一种用于成本有效地生产光纤的方法，管状半成品和一组同轴部件，其特征在于芯和夹套之间的边界质量高 并且通过低弯曲灵敏度，根据本发明，环区的石英玻璃以平均氟含量为至少6000重量ppm的石英玻璃制成的环形管的形式提供，并且管具有内管 表面和外管表面，其中通过环带管的壁，调节径向氟浓度分布，其具有层厚度为至少1μm且不大于10μm的内氟耗尽层，其中 氟含量向内管表面减少，并且在接近表面厚度为1μm的区域中不超过3000重量ppm。

公开(公告)号：US20060207293A1

公开(公告)日：2006-09-21

申请号：US10565099

申请日：2004-07-18

申请人： Rene Sowa ,  Ralph Sattmann ,  Jan Vydra

发明人： Rene Sowa ,  Ralph Sattmann ,  Jan Vydra

IPC分类号： C03B37/07 ,  C03B37/028

CPC分类号： C03B37/01211 ,  C03B37/01245 ,  C03B37/01251 ,  C03B37/0126 ,  C03B37/02736 ,  C03B37/02754 ,  C03B2205/14

摘要： The production of an optical component from quartz glass by elongation of a coaxial arrangement of a core rod and a hollow cylinder is known. The arrangement is thus introduced into a heating zone, such that the lower end begins to partly soften and the component drawn from the softened part. According to the invention, a pseudo-continuous method for the formation of the restriction in the inner passage of the hollow cylinder on which the core rod is supported, is disclosed, whereby an upper hollow cylinder is fused end on with a lower hollow cylinder to form an axial composite cylinder, a core rod is introduced into the lower hollow cylinder and the axial cylinder composite partly softened and elongated to form the optical component. A drawing bulb extending to the upper hollow cylinder forms, within which the inner passage at least partly collapses with formation of the restriction and the upper cylinder is then separated off from the drawn optical component at a separating plane and then elongated together with a core rod to form an optical component.

摘要翻译： 已知通过芯棒和中空圆柱体的同轴布置的延长从石英玻璃生产光学部件。 因此，该布置被引入加热区，使得下端开始部分软化，并且从软化部分拉出的部件。 根据本发明，公开了一种用于在其上支撑有芯棒的中空圆柱体的内部通道中形成限制的伪连续方法，其中上空心圆筒以下空心圆筒熔化， 形成轴向复合圆筒，将芯棒引入下空心圆筒中，轴向圆筒复合材料部分软化和拉长以形成光学部件。 延伸到上部中空圆筒的拉丝灯泡形成，其中内部通道至少部分地与形成限制部分地折叠，并且上部圆柱体在分离平面处从拉出的光学部件分离出来，然后与芯棒一起拉长 以形成光学部件。

公开(公告)号：US20060174659A1

公开(公告)日：2006-08-10

申请号：US10565134

申请日：2004-07-18

申请人： Oliver Ganz ,  Rene Sowa ,  Peter Bauer ,  Norbert Cibis ,  Ralph Sattmann ,  Jan Vydra ,  Clemens Schmitt

发明人： Oliver Ganz ,  Rene Sowa ,  Peter Bauer ,  Norbert Cibis ,  Ralph Sattmann ,  Jan Vydra ,  Clemens Schmitt

IPC分类号： C03B37/027

CPC分类号： C03B37/01211 ,  C03B37/01245 ,  C03B37/01251 ,  C03B37/0126 ,  C03B37/02736 ,  C03B37/02754 ,  C03B2205/14

摘要： The production of an optical component from quartz glass, by elongation of a coaxial arrangement of a core rod and a hollow cylinder of a given length, is known. The arrangement is thus introduced into a heating zone with a vertical orientation, such that the lower end begins to partly soften and the component is drawn downwards from the softened part. The hollow cylinder has an inner passage, provided with a restriction in the region of the lower end thereof, on which the core rod is supported. Several methods are disclosed for formation of the restriction in which the inner passage (55) is mechanically machined to a final dimension and, in one version of the method, the restriction in the inner passage (55) is generated by means of softening the lower end face of the hollow cylinder, swaged against a tool and thus folded inwards with formation of a peripheral bead ring.

摘要翻译： 已知通过芯棒的同轴布置和给定长度的中空圆柱体从石英玻璃生产光学部件。 因此，该布置被引入具有垂直取向的加热区域，使得下端开始部分软化，并且部件从软化部分向下拉。 中空圆筒具有内部通道，在其下端的区域中设置有限制，其上支撑有芯棒。 公开了几种用于形成限制的方法，其中内部通道（55）被机械加工到最终尺寸，并且在该方法的一种形式中，内部通道（55）中的限制是通过软化下部 中空圆筒的端面，相对于工具进行锻压，从而向内折叠，形成周边的胎圈环。

公开(公告)号：US07854146B2

公开(公告)日：2010-12-21

申请号：US10565099

申请日：2004-07-18

申请人： Rene Sowa ,  Ralph Sattmann ,  Jan Vydra

发明人： Rene Sowa ,  Ralph Sattmann ,  Jan Vydra

IPC分类号： C03B37/025

CPC分类号： C03B37/01211 ,  C03B37/01245 ,  C03B37/01251 ,  C03B37/0126 ,  C03B37/02736 ,  C03B37/02754 ,  C03B2205/14

摘要： The production of an optical component from quartz glass by elongation of a coaxial arrangement of a core rod and a hollow cylinder is known. The arrangement is thus introduced into a heating zone, such that the lower end begins to partly soften and the component drawn from the softened part. According to the invention, a pseudo-continuous method for the formation of the restriction in the inner passage of the hollow cylinder on which the core rod is supported, is disclosed, whereby an upper hollow cylinder is fused end on with a lower hollow cylinder to form an axial composite cylinder, a core rod is introduced into the lower hollow cylinder and the axial cylinder composite partly softened and elongated to form the optical component. A drawing bulb extending to the upper hollow cylinder forms, within which the inner passage at least partly collapses with formation of the restriction and the upper cylinder is then separated off from the drawn optical component at a separating plane and then elongated together with a core rod to form an optical component.

摘要翻译： 已知通过芯棒和中空圆柱体的同轴布置的延长从石英玻璃生产光学部件。 因此，该布置被引入加热区，使得下端开始部分软化，并且从软化部分拉出的部件。 根据本发明，公开了一种用于在其上支撑有芯棒的中空圆柱体的内部通道中形成限制的伪连续方法，其中上空心圆筒以下空心圆筒熔化， 形成轴向复合圆筒，将芯棒引入下空心圆筒中，轴向圆筒复合材料部分软化和拉长以形成光学部件。 延伸到上部中空圆筒的拉丝灯泡形成，其中内部通道至少部分地与形成限制部分地折叠，并且上部圆柱体在分离平面处从拉出的光学部件分离出来，然后与芯棒 以形成光学部件。

公开(公告)号：US20100260949A1

公开(公告)日：2010-10-14

申请号：US12820001

申请日：2010-06-21

申请人： Oliver Ganz ,  Ralph Sattmann ,  Jan Vydra

发明人： Oliver Ganz ,  Ralph Sattmann ,  Jan Vydra

IPC分类号： B32B1/08 ,  C03C15/00

CPC分类号： C03C3/06 ,  C03B19/1453 ,  C03B19/1469 ,  C03B37/0124 ,  C03B37/01892 ,  C03B2201/04 ,  C03B2201/075 ,  Y10T428/13

摘要： Known synthetic quartz glass tubes for the production of a preform have an inner bore with a surface layer produced without using tools in the molten state and an inner zone. The aim of the invention is to provide a tube which does not release any OH groups to the surroundings. For this purpose, the surface layer (30) has a thickness of 10 μm and an average OH content of not more than 5 ppm by weight and an average surface roughness Ra of not more than 0.1 μm. The inner zone (34) that starts on the surface layer (30) and terminates 10 μm before the outer wall has an average OH content of not more than 0.2 ppm by weight. A simple and inexpensive method for producing a quartz tube of the above type is to continuously draw a tube strand from a softened quartz glass mass in a vertical drawing process. A scavenging gas is circulated through the inner bore of the tube, said gas having a water content of less than 100 ppb per weight. The front end of the tube strand (19) is closed by a flow obstacle (26) that is permeable the scavenging gas and that reduces the amount of scavenging gas (23) flowing through.

摘要翻译： 用于生产预成型件的已知的合成石英玻璃管具有内孔，其具有在不使用处于熔融状态的工具和内部区域的情况下制备的表面层。 本发明的目的是提供一种不会向周围释放任何OH基团的管。 为此，表面层（30）的厚度为10μm，平均OH含量为5重量ppm以下，平均表面粗糙度Ra为0.1μm以下。 在表层（30）上开始并在外壁之前终止10μm的内部区域（34）具有不大于0.2重量ppm的平均OH含量。 用于生产上述类型的石英管的简单和便宜的方法是在垂直拉伸过程中连续地从软化的石英玻璃块抽取管束。 清除气体通过管的内孔循环，所述气体的含水量小于100ppb /重量。 管股（19）的前端由能够吸收清除气体的流动障碍物（26）封闭，并减少流过的清除气体（23）的量。

公开(公告)号：US07681416B2

公开(公告)日：2010-03-23

申请号：US10565134

申请日：2004-07-18

申请人： Oliver Ganz ,  Rene Sowa ,  Peter Bauer ,  Norbert Cibis ,  Ralph Sattmann ,  Jan Vydra ,  Clemens Schmitt

发明人： Oliver Ganz ,  Rene Sowa ,  Peter Bauer ,  Norbert Cibis ,  Ralph Sattmann ,  Jan Vydra ,  Clemens Schmitt

IPC分类号： C03B37/012 ,  C03B37/02

CPC分类号： C03B37/01211 ,  C03B37/01245 ,  C03B37/01251 ,  C03B37/0126 ,  C03B37/02736 ,  C03B37/02754 ,  C03B2205/14

摘要： The production of an optical component from quartz glass, by elongation of a coaxial arrangement of a core rod and a hollow cylinder of a given length, is known. The arrangement is thus introduced into a heating zone with a vertical orientation, such that the lower end begins to partly soften and the component is drawn downwards from the softened part. The hollow cylinder has an inner passage, provided with a restriction in the region of the lower end thereof, on which the core rod is supported. Several methods are disclosed for formation of the restriction in which the inner passage (55) is mechanically machined to a final dimension and, in one version of the method, the restriction in the inner passage (55) is generated by means of softening the lower end face of the hollow cylinder, swaged against a tool and thus folded inwards with formation of a peripheral bead ring.

摘要翻译： 已知通过芯棒的同轴布置和给定长度的中空圆柱体从石英玻璃生产光学部件。 因此，该布置被引入具有垂直取向的加热区域，使得下端开始部分软化，并且部件从软化部分向下拉。 中空圆筒具有内部通道，在其下端的区域中设置有限制，其上支撑有芯棒。 公开了几种用于形成限制的方法，其中内部通道（55）被机械加工到最终尺寸，并且在该方法的一种形式中，内部通道（55）中的限制是通过软化下部 中空圆筒的端面，相对于工具进行锻压，从而向内折叠，形成周边的胎圈环。

公开(公告)号：US20060191294A1

公开(公告)日：2006-08-31

申请号：US10550049

申请日：2004-03-19

申请人： Oliver Ganz ,  Ralph Sattmann ,  Jan Vydra

发明人： Oliver Ganz ,  Ralph Sattmann ,  Jan Vydra

IPC分类号： C03B37/025 ,  C03B37/02

CPC分类号： C03C3/06 ,  C03B19/1453 ,  C03B19/1469 ,  C03B37/0124 ,  C03B37/01892 ,  C03B2201/04 ,  C03B2201/075 ,  Y10T428/13

摘要： Known synthetic quartz glass tubes for the production of a preform have an inner bore with a surface layer produced without using tools in the molten state and an inner zone. The aim of the invention is to provide a tube which does not release any OH groups to the surroundings. For this purpose, the surface layer (30) has a thickness of 10 μm and an average OH content of not more than 5 ppm by weight and an average surface roughness Ra of not more than 0.1 μm. The inner zone (34) that starts on the surface layer (30) and terminates 10 μm before the outer wall has an average OH content of not more than 0.2 ppm by weight. A simple and inexpensive method for producing a quartz tube of the above type is to continuously draw a tube strand from a softened quartz glass mass in a vertical drawing process. A scavenging gas is circulated through the inner bore of the tube, said gas having a water content of less than 100 ppb per weight. The front end of the tube strand (19) is closed by a flow obstacle (26) that is permeable the scavenging gas and that reduces the amount of scavenging gas (23) flowing through.

摘要翻译： 用于生产预成型件的已知的合成石英玻璃管具有内孔，其具有在不使用处于熔融状态的工具和内部区域的情况下制备的表面层。 本发明的目的是提供一种不会向周围释放任何OH基团的管。 为此，表面层（30）的厚度为10μm，平均OH含量为5重量ppm以下，平均表面粗糙度R a a为0.1μm以下。 在表层（30）之前开始并在外壁具有不大于0.2重量ppm的平均OH含量之前终止10um的内部区域（34）。 用于生产上述类型的石英管的简单和便宜的方法是在垂直拉伸过程中连续地从软化的石英玻璃块抽取管束。 清除气体通过管的内孔循环，所述气体的含水量小于100ppb /重量。 管股（19）的前端由能够吸收清除气体的流动障碍物（26）封闭，并减少流过的清除气体（23）的量。

公开(公告)号：US07748258B2

公开(公告)日：2010-07-06

申请号：US11863966

申请日：2007-09-28

申请人： Ralph Sattmann

发明人： Ralph Sattmann

IPC分类号： G01N1/00 ,  G01K1/12

CPC分类号： G01N1/125 ,  G01J5/0037 ,  G01J5/004 ,  G01J5/0255 ,  G01J5/0285 ,  G01J5/041 ,  G01J5/045 ,  G01J5/048 ,  G01J5/08 ,  G01N21/0332 ,  G01N21/718 ,  G01N21/8507 ,  G01N33/206 ,  G01N2201/024

摘要： An immersion sensor for analysis of liquids or melts includes an immersion carrier, a detector and a radiation-guiding unit, and a sample chamber arranged in the immersion carrier. The sample chamber has an inlet opening for liquid or melt, and the sensing components for measurement of the liquid or melt act inside the sample chamber.

摘要翻译： 用于分析液体或熔体的浸没传感器包括浸没载体，检测器和辐射引导单元以及布置在浸没载体中的样品室。 样品室具有用于液体或熔体的入口，用于测量液体或熔体的感测部件在样品室内作用。

公开(公告)号：US20080028797A1

公开(公告)日：2008-02-07

申请号：US11629227

申请日：2005-06-08

申请人： Ralph Sattmann

发明人： Ralph Sattmann

IPC分类号： C03B37/022

CPC分类号： C03B37/02736 ,  C03B37/0126 ,  C03B2205/30 ,  Y02P40/57

摘要： In a conventional method for the production of an optical component made from quartz glass, a coaxial arrangement with a core rod, surrounded by a quartz glass envelope tube comprising an evacuable inner drilling, is introduced in the vertical direction into a heating zone, softened therein by sections and, with formation of a drawing bulb, elongated to give the quartz glass component. According to the invention, a simple and cheap method based on the above, permitting the production of high-grade optical components by elongation of a coaxial arrangement of core rod and an enveloping tube with great economy, may be achieved, whereby a core rod is used, comprising at least two separate core rods arranged one above the other in the inner drilling and the weight of an upper core rod section is taken by a mounting or support region of the enveloping tube, provided above the drawing bulb.

摘要翻译： 在制造由石英玻璃制成的光学部件的常规方法中，将包括可抽真空的内钻的石英玻璃封套管包围的芯棒的同轴布置在垂直方向上引入加热区，在其中软化 通过切片形成一个拉丝灯泡，拉长以得到石英玻璃部件。 根据本发明，可以实现基于上述的简单且便宜的方法，允许通过延长具有经济性的芯棒和包络管的同轴布置来生产高级光学部件，由此芯棒 使用的，包括在内部钻孔中一个在另一个上彼此排列的至少两个分离的芯棒，并且上芯棒部分的重量由设置在牵伸灯泡上方的包封管的安装或支撑区域取走。