METHOD FOR PURIFYING A CHLORINE SUPPLY
    1.
    发明申请
    METHOD FOR PURIFYING A CHLORINE SUPPLY 有权
    净化氯素供应的方法

    公开(公告)号:US20110144381A1

    公开(公告)日:2011-06-16

    申请号:US12945031

    申请日:2010-11-12

    摘要: This invention provides a method for purifying a chlorine supply that includes a chlorine component, a bromine component, and nitrogen trichloride. The method includes the steps of introducing the chlorine supply into a vaporizer, heating the chlorine supply in the vaporizer to form a vapor, and introducing the vapor into a distillation system to provide purified chlorine gas, a distillate that includes liquid chlorine and the bromine component, and a bottoms component including the nitrogen trichloride. The method also includes the steps of condensing the vapor in a reflux condenser, heating the condensate in a reboiler, removing the purified chlorine gas from the distillation system, and removing the distillate from the distillation system.

    摘要翻译: 本发明提供了一种用于纯化氯供应的方法,其包括氯组分,溴组分和三氯化氮。 该方法包括以下步骤:将氯供应引入蒸发器中,加热蒸发器中的氯供应以形成蒸气,并将蒸气引入蒸馏系统中以提供纯化的氯气,包括液氯的馏出物和溴成分 ,和含有三氯化氮的底部成分。 该方法还包括以下步骤:将蒸气冷凝在回流冷凝器中,加热再沸器中的冷凝物,从蒸馏系统中除去纯化的氯气,以及从蒸馏系统中除去馏出物。

    Method for purifying a chlorine supply
    2.
    发明授权
    Method for purifying a chlorine supply 有权
    净化氯气供应的方法

    公开(公告)号:US08512447B2

    公开(公告)日:2013-08-20

    申请号:US12945031

    申请日:2010-11-12

    IPC分类号: B01D53/02 C01B21/00

    摘要: This invention provides a method for purifying a chlorine supply that includes a chlorine component, a bromine component, and nitrogen trichloride. The method includes the steps of introducing the chlorine supply into a vaporizer, heating the chlorine supply in the vaporizer to form a vapor, and introducing the vapor into a distillation system to provide purified chlorine gas, a distillate that includes liquid chlorine and the bromine component, and a bottoms component including the nitrogen trichloride. The method also includes the steps of condensing the vapor in a reflux condenser, heating the condensate in a reboiler, removing the purified chlorine gas from the distillation system, and removing the distillate from the distillation system.

    摘要翻译: 本发明提供了一种用于纯化氯供应的方法,其包括氯组分,溴组分和三氯化氮。 该方法包括以下步骤:将氯供应引入蒸发器中,加热蒸发器中的氯供应以形成蒸气,并将蒸气引入蒸馏系统中以提供纯化的氯气,包括液氯的馏出物和溴成分 ,和含有三氯化氮的底部成分。 该方法还包括以下步骤:将蒸气冷凝在回流冷凝器中,加热再沸器中的冷凝物,从蒸馏系统中除去纯化的氯气,以及从蒸馏系统中除去馏出物。

    Novel surfactants based on poly(alkylene carbonate)s
    7.
    发明授权
    Novel surfactants based on poly(alkylene carbonate)s 失效
    基于聚(碳酸亚烷基酯)的新型表面活性剂

    公开(公告)号:US4866143A

    公开(公告)日:1989-09-12

    申请号:US184585

    申请日:1988-04-21

    摘要: A polyether polycarbonate block copolymer nonionic surface-active agent and method for making the same. The polyether polycarbonate surface active agent is comprised of a hydrophilic portion comprised of a polymer selected from the group consisting of a polyoxyalkylene polyether, a saccharide, a saccharide polyoxyalkylenate, a polycarbonate having a carbon dioxide content of from about 1 to 15 molar percent and mixtures thereof and a hydrophobic portion comprising alkylene and carbonate units arranged in alternating or random order to form a poly(alkylene carbonate) having a total carbon dioxide content of from about 25 to 50 molar percent and a total molecular weight of from about 300 to 10,000. The hydrophobic portion is bonded to the hydrophilic portion at each side of a reactive hydrogen. The surface active agent is prepared by polymerizing the hydrophilic portion with the hydrophobic portion in a weight ratio of about 10:90 to 90:10.

    摘要翻译: 聚醚聚碳酸酯嵌段共聚物非离子表面活性剂及其制造方法。 聚醚聚碳酸酯表面活性剂由亲水部分组成,该亲水部分由选自聚氧化烯聚醚,糖类,糖类聚氧化亚烯酸酯,二氧化碳含量为约1至15摩尔%的聚碳酸酯和聚合物 和疏水部分,其包含交替或无规排列的亚烷基和碳酸酯单元以形成总二氧化碳含量为约25至50摩尔%且总分子量为约300至10,000的聚(碳酸亚烷基酯)。 疏水部分结合到反应性氢的每一侧的亲水部分。 表面活性剂的制备方法是将亲水部分与疏水部分以约10:90至90:10的重量比聚合。

    Recovery of products from toluenediisocyanate residues
    8.
    发明授权
    Recovery of products from toluenediisocyanate residues 失效
    从甲苯二异氰酸酯残留物中回收产物

    公开(公告)号:US5902459A

    公开(公告)日:1999-05-11

    申请号:US661176

    申请日:1996-06-10

    CPC分类号: C07D233/30 C07C209/62

    摘要: There is now provided a method of recycling toluenediisocyanate residue resulting from the production of toluenediisocyanate by the reaction of toluenediamine by phosgenation in the presence of a solvent. In accordance with the teachings of the present invention, the toluenediisocyanate residue is treated at reflux with an alkanolamine to obtain an intermediary product which is distilled thereby giving rise to various products including but not limited to at least one component selected from toluenediamine, oxazolidone and hydroxyethylimidiazolidone. Preferably the alkanolamine employed is a monoethanolamine.

    摘要翻译: 现在提供一种在溶剂存在下通过甲苯二胺通过光气化反应而产生甲苯二异氰酸酯产生的甲苯二异氰酸酯残基的方法。 根据本发明的教导,甲苯二异氰酸酯残基用链烷醇胺回流处理以获得中间产物,其被蒸馏,从而产生各种产物,包括但不限于选自甲苯二胺,恶唑烷酮和羟乙基亚氨基二唑烷酮中的至少一种 。 优选使用的链烷醇胺是单乙醇胺。

    Novel surfactants based on poly(alkylene carbonate)s
    10.
    发明授权
    Novel surfactants based on poly(alkylene carbonate)s 失效
    基于聚(碳酸亚烷基酯)的新型表面活性剂

    公开(公告)号:US4948845A

    公开(公告)日:1990-08-14

    申请号:US340812

    申请日:1989-04-17

    IPC分类号: B01F17/00 C08G64/18 C11D3/37

    摘要: A polyether polycarbonate block copolymer nonionic surface-active agent and method for making the same. The polyether polycarbonate surface active agent is comprised of a hydrophilic portion comprised of a polymer selected from the group consisting of a polyoxyalkylene polyether, a saccharide, a saccharide polyoxyalkylenate, a polycarbonate having a carbon dioxide content of from about 1 to 15 molar percent and mixtures thereof and a hydrophobic portion comprising alkylene and carbonate units arranged in alternating or random order to form a poly(alkylene carbonate) having a total carbon dioxide content of from about 25 to 50 molar percent and a total molecular weight of from about 300 to 10,000. The hydrophobic portion is bonded to the hydrophilic portion at each side of a reactive hydrogen. The surface active agent is prepared by polymerizing the hydrophilic portion with the hydrophobic portion in a weight ratio of about 10:90 to 90:10.

    摘要翻译: 聚醚聚碳酸酯嵌段共聚物非离子表面活性剂及其制造方法。 聚醚聚碳酸酯表面活性剂由亲水部分组成,该亲水部分由选自聚氧化烯聚醚,糖类,糖类聚氧化亚烯酸酯,二氧化碳含量为约1至15摩尔%的聚碳酸酯和聚合物 和疏水部分,其包含交替或无规排列的亚烷基和碳酸酯单元以形成总二氧化碳含量为约25至50摩尔%且总分子量为约300至10,000的聚(碳酸亚烷基酯)。 疏水部分结合到反应性氢的每一侧的亲水部分。 表面活性剂的制备方法是将亲水部分与疏水部分以约10:90至90:10的重量比聚合。