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1.发明申请METHOD FOR PRODUCING FUNCTIONALIZED CIS-1,4-POLYDIENES HAVING HIGH CIS-1,4-LINKAGE CONTENT AND HIGH FUNCTIONALITY 有权生产具有高CIS-1,4链接内容和高功能性的官能化CIS-1,4-聚异戊二烯的方法公开(公告)号：US20080182954A1
公开(公告)日：2008-07-31
申请号：US11964848
申请日：2007-12-27
申请人： Steven Luo , Junko Kurazumi , Yoichi Ozawa , Timothy L. Tartamella , Mark Smale
发明人： Steven Luo , Junko Kurazumi , Yoichi Ozawa , Timothy L. Tartamella , Mark Smale
CPC分类号： C08C19/44 , B60C1/00 , B60C1/0016 , B60C1/0025 , C08L15/00 , Y10S525/902 , Y10T152/10495
摘要： This invention relates to a method for producing functionalized cis-1,4-polydienes having a combination of a high cis-1,4-linkage content and a high functionality, the resulting polymers and the vulcanized products containing the polymers. The functionalized cis-1,4-polydienes of the present invention are produced by a method comprising the steps of: (1) preparing a reactive polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst in the presence of less than 20% by weight of organic solvent based on the total weight of monomer, organic solvent, and resulting polymer, where the lanthanide-based catalyst is the combination of or reaction product of (a) a lanthanide compound, (b) an aluminoxane, (c) an organoaluminum compound other than an aluminoxane, and (d) a halogen-containing compound; and (2) contacting the reactive polymer with a functionalizing agent.
摘要翻译： 本发明涉及具有高顺式-1,4-键含量和高官能度组合的官能化顺式-1,4-聚二烯的方法，所得聚合物和含有聚合物的硫化产物。 本发明的官能化顺式-1,4-聚二烯通过包括以下步骤的方法制备：（1）通过将共轭二烯单体与镧系元素基催化剂在少于20％ 基于单体，有机溶剂和所得聚合物的总重量的有机溶剂的重量，其中镧系元素基催化剂是（a）镧系元素化合物，（b）铝氧烷，（c） 除铝氧烷以外的有机铝化合物，和（d）含卤素化合物; 和（2）使反应性聚合物与官能化剂接触。
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2.发明授权Method for producing functionalized cis-1,4-polydienes having high cis-1,4-linkage content and high functionality 有权具有高顺式-1,4-键含量和高官能度的官能化顺式-1,4-聚二烯的方法公开(公告)号：US08017695B2
公开(公告)日：2011-09-13
申请号：US11964848
申请日：2007-12-27
申请人： Steven Luo , Junko Kurazumi , Yoichi Ozawa , Timothy L. Tartamella , Mark Smale , Kevin McCauley
发明人： Steven Luo , Junko Kurazumi , Yoichi Ozawa , Timothy L. Tartamella , Mark Smale , Kevin McCauley
CPC分类号： C08C19/44 , B60C1/00 , B60C1/0016 , B60C1/0025 , C08L15/00 , Y10S525/902 , Y10T152/10495
摘要： This invention relates to a method for producing functionalized cis-1,4-polydienes having a combination of a high cis-1,4-linkage content and a high functionality, the resulting polymers and the vulcanized products containing the polymers. The functionalized cis-1,4-polydienes of the present invention are produced by a method comprising the steps of: (1) preparing a reactive polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst in the presence of less than 20% by weight of organic solvent based on the total weight of monomer, organic solvent, and resulting polymer, where the lanthanide-based catalyst is the combination of or reaction product of (a) a lanthanide compound, (b) an aluminoxane, (c) an organoaluminum compound other than an aluminoxane, and (d) a halogen-containing compound; and (2) contacting the reactive polymer with a functionalizing agent.
摘要翻译： 本发明涉及具有高顺式-1,4-键含量和高官能度组合的官能化顺式-1,4-聚二烯的方法，所得聚合物和含有聚合物的硫化产物。 本发明的官能化顺式-1,4-聚二烯通过包括以下步骤的方法制备：（1）通过将共轭二烯单体与镧系元素基催化剂在少于20％ 基于单体，有机溶剂和所得聚合物的总重量的有机溶剂的重量，其中镧系元素基催化剂是（a）镧系元素化合物，（b）铝氧烷，（c） 除铝氧烷以外的有机铝化合物，和（d）含卤素化合物; 和（2）使反应性聚合物与官能化剂接触。
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公开(公告)号：US20080275199A1
公开(公告)日：2008-11-06
申请号：US12113375
申请日：2008-05-01
IPC分类号： C08F4/44
CPC分类号： C08F36/08 , Y10S526/919 , C08F4/52 , C08F4/545
摘要： There is disclosed a process for producing a conjugated diene-containing polymer wherein a stream comprising conjugated diene monomer and a specified catalyst, that includes a lanthanide compound and an aluminoxane, is passed through an orifice into the reaction zone of a polymerization vessel, maintained under specific pressure conditions to form a cement having a viscosity that allows the cement to be conveyed through a devolatilization zone, where desired.
摘要翻译： 公开了一种制备含共轭二烯的聚合物的方法，其中将包含共轭二烯单体和特定催化剂的物流（包括镧系元素化合物和铝氧烷）通过孔进入聚合容器的反应区，保持在 特定压力条件，以形成具有允许粘合剂在需要时通过脱挥发分区域输送的粘度的水泥。
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公开(公告)号：US07572867B2
公开(公告)日：2009-08-11
申请号：US12113375
申请日：2008-05-01
CPC分类号： C08F36/08 , Y10S526/919 , C08F4/52 , C08F4/545
摘要： There is disclosed a process for producing a conjugated diene-containing polymer wherein a stream comprising conjugated diene monomer and a specified catalyst, that includes a lanthanide compound and an aluminoxane, is passed through an orifice into the reaction zone of a polymerization vessel, maintained under specific pressure conditions to form a cement having a viscosity that allows the cement to be conveyed through a devolatilization zone, where desired.
摘要翻译： 公开了一种制备含共轭二烯的聚合物的方法，其中将包含共轭二烯单体和特定催化剂的物流（包括镧系元素化合物和铝氧烷）通过孔进入聚合容器的反应区，保持在 特定压力条件，以形成具有允许粘合剂在需要时通过脱挥发分区域输送的粘度的水泥。
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公开(公告)号：US07687589B2
公开(公告)日：2010-03-30
申请号：US11893121
申请日：2007-08-14
摘要： A method for the continuous production of polydienes, the method comprising the steps of (a) charging a mixture of one or more monomer, catalyst system, and less than 50% weight percent organic solvent based on the total weight of the monomer, catalyst and solvent, into first vessel, (b) polymerizing the monomer to a conversion of up to 20% by weight of the monomer to form a mixture of reactive polymer and monomer, (c) removing the mixture of reactive polymer and monomer from the vessel, and (d) terminating the reactive polymer prior to a total monomer conversion of 25% by weight.
摘要翻译： 一种连续生产聚二烯的方法，所述方法包括以下步骤：（a）将单体，催化剂体系和小于50％重量百分比的有机溶剂的混合物以单体，催化剂和 溶剂进入第一容器，（b）将单体聚合至高达单体重量的20％的转化率以形成反应性聚合物和单体的混合物，（c）从容器中除去反应性聚合物和单体的混合物， 和（d）在总单体转化率为25重量％之前终止反应性聚合物。
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公开(公告)号：US07351776B2
公开(公告)日：2008-04-01
申请号：US11062673
申请日：2005-02-22
摘要： A method for the continuous production of polydienes, the method comprising the steps of (a) charging a mixture of one or more monomer, catalyst system, and less than 50% weight percent organic solvent based on the total weight of the monomer, catalyst and solvent, into first vessel, (b) polymerizing the monomer to a conversion of up to 20% by weight of the monomer to form a mixture of reactive polymer and monomer, (c) removing the mixture of reactive polymer and monomer from the vessel, and (d) terminating the reactive polymer prior to a total monomer conversion of 25% by weight.
摘要翻译： 一种连续生产聚二烯的方法，所述方法包括以下步骤：（a）将单体，催化剂体系和小于50％重量百分比的有机溶剂的混合物以单体，催化剂和 溶剂进入第一容器，（b）将单体聚合至高达单体重量的20％的转化率以形成反应性聚合物和单体的混合物，（c）从容器中除去反应性聚合物和单体的混合物， 和（d）在总单体转化率为25重量％之前终止反应性聚合物。
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7.发明授权Rubber compositions including a polymeric component having a multi-modal molecular weight distribution 有权包括具有多分子量分布的聚合物组分的橡胶组合物公开(公告)号：US09303154B2
公开(公告)日：2016-04-05
申请号：US13142510
申请日：2009-12-28
申请人： Zhong-Ren Chen , Kevin McCauley , Mark Smale , Michael W. Hayes , Steven Luo
发明人： Zhong-Ren Chen , Kevin McCauley , Mark Smale , Michael W. Hayes , Steven Luo
IPC分类号： C08L9/00 , C08F136/00 , C08L9/06
CPC分类号： C08L9/00 , C08L9/06 , C08L2205/02 , C08L2666/08
摘要： A vulcanizable composition of matter comprising a rubber component, a filler, a curative for the rubber, where the rubber component includes a multi-modal polymer including at least two distinct peak molecular weights within a range defined by a lower limit of 80 kg/mole and an upper limit of 500 kg/mole.
摘要翻译： 一种可硫化的物质组合物，包括橡胶组分，填料，橡胶固化剂，其中橡胶组分包括在下限80kg / mol范围内包含至少两个不同峰分子量的多模态聚合物 上限为500公斤/摩尔。
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8.发明申请RUBBER COMPOSITIONS INCLUDING A POLYMERIC COMPONENT HAVING A MULTI-MODAL MOLECULAR WEIGHT DISTRIBUTION 有权橡胶组合物，包括具有多模式分子量分布的聚合物组分公开(公告)号：US20120108736A1
公开(公告)日：2012-05-03
申请号：US13142510
申请日：2009-12-28
申请人： Zhong-Ren Chen , Kevin McCauley , Mark Smale , Michael W. Hayes , Steven Luo
发明人： Zhong-Ren Chen , Kevin McCauley , Mark Smale , Michael W. Hayes , Steven Luo
IPC分类号： C08L9/00 , C08F136/06 , C08L9/06
CPC分类号： C08L9/00 , C08L9/06 , C08L2205/02 , C08L2666/08
摘要： A vulcanizable composition of matter comprising a rubber component, a filler, a curative for the rubber, where the rubber component includes a multi-modal polymer including at least two distinct peak molecular weights within a range defined by a lower limit of 80 kg/mole and an upper limit of 500 kg/mole.
摘要翻译： 一种可硫化的物质组合物，包括橡胶组分，填料，橡胶固化剂，其中橡胶组分包括在下限80kg / mol范围内包含至少两个不同峰分子量的多模态聚合物 上限为500公斤/摩尔。
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公开(公告)号：US20080076890A1
公开(公告)日：2008-03-27
申请号：US11893121
申请日：2007-08-14
申请人： Timothy Tartamella , William Cole , Mark Smale
发明人： Timothy Tartamella , William Cole , Mark Smale
IPC分类号： C08F4/44
摘要： A method for the continuous production of polydienes, the method comprising the steps of (a) charging a mixture of one or more monomer, catalyst system, and less than 50% weight percent organic solvent based on the total weight of the monomer, catalyst and solvent, into first vessel, (b) polymerizing the monomer to a conversion of up to 20% by weight of the monomer to form a mixture of reactive polymer and monomer, (c) removing the mixture of reactive polymer and monomer from the vessel, and (d) terminating the reactive polymer prior to a total monomer conversion of 25% by weight.
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