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    POLYESTER BASED COBALT CONCENTRATES FOR OXYGEN SCAVENGING COMPOSITIONS
    1.
    发明申请
    POLYESTER BASED COBALT CONCENTRATES FOR OXYGEN SCAVENGING COMPOSITIONS 审中-公开
    用于氧气组合物的基于聚酯的钴浓度

    公开(公告)号：US20080045637A1

    公开(公告)日：2008-02-21

    申请号：US11843258

    申请日：2007-08-22

    申请人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    发明人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    IPC分类号： C08K5/053 ,  C08K3/08 ,  C08K3/10

    CPC分类号： C08K5/098 ,  C08L67/02 ,  C08L77/00 ,  Y10T428/1352 ,  Y10T428/1383 ,  C08L2666/14

    摘要： A solid concentrate is provided having a combination of a transition metal present in an amount ranging from 1,000 to 40,000 ppm (weight by metal) and a polyester polymer present in an amount of at least 40 wt. % based on the weight of the concentrate. Concentrates made with highly modified polyester polymers are easy to compound with transition metals forming less brittle polymer upon melt extrusion. Bottle preforms and oxygen scavenging bottles can be made from these concentrates by combining solid polyester particles, solid polyamide particles, and solid these concentrate particles c into an melt processing zone, forming a melt, and forming an article directly from the melt. The b* color and the L* color and the haze levels of the preforms are improved over the preforms made with liquid carriers instead of solid concentrates. The particles are also advantageously simultaneously dried in a drying zone under conditions effective to at least partially remove moisture from the blend to thereby further improve the b* color and L* color.

    摘要翻译： 提供了一种固体浓缩物，其具有以1,000至40,000ppm（金属重量）的量存在的过渡金属和以至少40重量％的量存在的聚酯聚合物的组合。 基于浓缩物的重量％。 用高度改性的聚酯聚合物制成的浓缩物易于与熔融挤出时形成较少脆性聚合物的过渡金属复合。 通过将固体聚酯颗粒，固体聚酰胺颗粒和固体这些浓缩颗粒c结合到熔融加工区域中，形成熔体并从熔体直接形成制品，可以从这些浓缩物制备瓶预成型件和除氧瓶。 相对于用液体载体代替固体浓缩物制成的预成型件，预型件的b *颜色和L *颜色和雾度水平得到改善。 在有效地至少部分地从共混物中除去水分的条件下，还可以在干燥区中同时干燥颗粒，从而进一步改善b *颜色和L *颜色。

    Polyester based cobalt concentrates for oxygen scavenging compositions
    2.
    发明申请
    Polyester based cobalt concentrates for oxygen scavenging compositions 有权
    用于除氧组合物的聚酯基钴精矿

    公开(公告)号：US20060128861A1

    公开(公告)日：2006-06-15

    申请号：US11292441

    申请日：2005-12-02

    申请人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    发明人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    IPC分类号： C08K5/09 ,  C08G63/60

    CPC分类号： C08K5/098 ,  C08L67/02 ,  C08L77/00 ,  Y10T428/1352 ,  Y10T428/1383 ,  C08L2666/14

    摘要： A solid concentrate is provided having a combination of a transition metal present in an amount ranging from 1000 to 40,000 ppm (weight by metal) and a polyester polymer present in an amount of at least 40 wt. % based on the weight of the concentrate. Concentrates made with highly modified polyester polymers are easy to compound with transition metals forming less brittle polymer upon melt extrusion. Bottle preforms and oxygen scavenging bottles can be made from these concentrates by combining solid polyester particles, solid polyamide particles, and solid these concentrate particles c into an melt processing zone, forming a melt, and forming an article directly from the melt. The b* color and the L* color and the haze levels of the preforms are improved over the preforms made with liquid carriers instead of solid concentrates. The particles are also advantageously simultaneously dried in a drying zone under conditions effective to at least partially remove moisture from the blend to thereby further improve the b* color and L* color.

    摘要翻译： 提供了一种固体浓缩物，其具有的存在量为1000至40,000ppm（金属重量）的过渡金属和以至少40重量％的量存在的聚酯聚合物的组合。 基于浓缩物的重量％。 用高度改性的聚酯聚合物制成的浓缩物易于与熔融挤出时形成较少脆性聚合物的过渡金属复合。 通过将固体聚酯颗粒，固体聚酰胺颗粒和固体这些浓缩颗粒c结合到熔融加工区域中，形成熔体并从熔体直接形成制品，可以从这些浓缩物制备瓶预成型件和除氧瓶。 相对于用液体载体代替固体浓缩物制成的预成型件，预型件的b *颜色和L *颜色和雾度水平得到改善。 在有效地至少部分地从共混物中除去水分的条件下，还可以在干燥区中同时干燥颗粒，从而进一步改善b *颜色和L *颜色。

    POLYESTER BASED COBALT CONCENTRATES FOR OXYGEN SCAVENGING COMPOSITIONS
    3.
    发明申请
    POLYESTER BASED COBALT CONCENTRATES FOR OXYGEN SCAVENGING COMPOSITIONS 审中-公开
    用于氧气组合物的基于聚酯的钴浓度

    公开(公告)号：US20080021142A1

    公开(公告)日：2008-01-24

    申请号：US11843275

    申请日：2007-08-22

    申请人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    发明人： Mark Stewart ,  Emerson Sharpe ,  Benjamin Gamble ,  Steven Stafford ,  Robert Estep ,  James Williams ,  Thomas Clark

    IPC分类号： C08K5/098 ,  C08K3/10 ,  C08K3/22 ,  C08K3/28 ,  C08K3/30 ,  C08K3/32 ,  C08K3/34 ,  C08K3/38

    CPC分类号： C08K5/098 ,  C08L67/02 ,  C08L77/00 ,  Y10T428/1352 ,  Y10T428/1383 ,  C08L2666/14

    摘要： A solid concentrate is provided having a combination of a transition metal present in an amount ranging from 1000 to 40,000 ppm (weight by metal) and a polyester polymer present in an amount of at least 40 wt. % based on the weight of the concentrate. Concentrates made with highly modified polyester polymers are easy to compound with transition metals forming less brittle polymer upon melt extrusion. Bottle preforms and oxygen scavenging bottles can be made from these concentrates by combining solid polyester particles, solid polyamide particles, and solid these concentrate particles c into an melt processing zone, forming a melt, and forming an article directly from the melt. The b* color and the L* color and the haze levels of the preforms are improved over the preforms made with liquid carriers instead of solid concentrates. The particles are also advantageously simultaneously dried in a drying zone under conditions effective to at least partially remove moisture from the blend to thereby further improve the b* color and L* color.

    摘要翻译： 提供了一种固体浓缩物，其具有的存在量为1000至40,000ppm（金属重量）的过渡金属和以至少40重量％的量存在的聚酯聚合物的组合。 基于浓缩物的重量％。 用高度改性的聚酯聚合物制成的浓缩物易于与熔融挤出时形成较少脆性聚合物的过渡金属复合。 通过将固体聚酯颗粒，固体聚酰胺颗粒和固体这些浓缩颗粒c结合到熔融加工区域中，形成熔体并从熔体直接形成制品，可以从这些浓缩物制备瓶预成型件和除氧瓶。 相对于用液体载体代替固体浓缩物制成的预成型件，预型件的b *颜色和L *颜色和雾度水平得到改善。 在有效地至少部分地从共混物中除去水分的条件下，还可以在干燥区中同时干燥颗粒，从而进一步改善b *颜色和L *颜色。

    Aluminum/alkaline or alkali/titanium containing polyesters having improved reheat, color and clarity
    6.
    发明申请
    Aluminum/alkaline or alkali/titanium containing polyesters having improved reheat, color and clarity 有权
    具有改善的再热，颜色和透明度的铝/碱性或碱/含钛聚酯

    公开(公告)号：US20070066735A1

    公开(公告)日：2007-03-22

    申请号：US11229238

    申请日：2005-09-16

    申请人： Donna Quillen ,  Rodney Armentrout ,  Mary Jernigan ,  Steven Stafford ,  Zhiyong Xia

    发明人： Donna Quillen ,  Rodney Armentrout ,  Mary Jernigan ,  Steven Stafford ,  Zhiyong Xia

    IPC分类号： B32B27/08 ,  C08K3/38 ,  C08K3/22

    CPC分类号： C08G63/83 ,  B29C47/0004 ,  B29C47/0016 ,  B29C47/0021 ,  C08G63/183 ,  C08G63/84 ,  Y10T428/1352 ,  Y10T428/1355 ,  Y10T428/139 ,  Y10T428/1397

    摘要： A polyester composition containing: a) aluminum atoms; and b) alkaline earth atoms or alkali metal atoms or alkali compound residues such as lithium atoms; and c) particles comprising titanium, zirconium, vanadium, niobium, hafnium, tantalum, chromium, tungsten, molybdenum, iron, or nickel atoms or combinations thereof, where the particles improve the reheat rate of the polyester composition. The polyester polymer compositions may also contain phosphorus catalyst deactivators/stabilizers. The polyester compositions and the articles made from the compositions such as bottle preforms and stretch blow molded bottles have improved reheat rate while maintaining low haze, high L*, a b* below 3, and have low levels of acetaldehyde. In the process for making the polyester polymer, the polymer melt is polycondensed in the presence of a) and b), with the particles c) added in a melt phase process or added to the polymer in an injection molding machine or extruder. The polyester polymer composition can be made to high IV from the melt phase while avoiding solid state polymerization.

    摘要翻译： 一种聚酯组合物，其含有：a）铝原子; 和b）碱土金属原子或碱金属原子或碱金属化合物残基如锂原子; 和c）包含钛，锆，钒，铌，铪，钽，铬，钨，钼，铁或镍原子或其组合的颗粒，其中颗粒改善了聚酯组合物的再热速率。 聚酯聚合物组合物还可以含有磷催化剂失活剂/稳定剂。 聚酯组合物和由诸如瓶子预成型件和拉伸吹塑成型瓶的组合物制成的制品具有改善的再加热速率，同时保持低雾度，高L *，低于3的b *，并且具有低水平的乙醛。 在制备聚酯聚合物的方法中，聚合物熔体在a）和b）存在下缩聚，颗粒c）在熔融相中加入或在注射成型机或挤出机中加入到聚合物中。 聚酯聚合物组合物可以从熔融相制成高IV，同时避免固态聚合。

    Accelerated acetaldehyde testing of polymers
    8.
    发明申请
    Accelerated acetaldehyde testing of polymers 审中-公开
    聚合物加速乙醛检测

    公开(公告)号：US20060287471A1

    公开(公告)日：2006-12-21

    申请号：US11154146

    申请日：2005-06-16

    申请人： Benjamin Schreiber ,  Eric Olsen ,  Steven Stafford ,  Jack Hensley ,  Donald Ellison

    发明人： Benjamin Schreiber ,  Eric Olsen ,  Steven Stafford ,  Jack Hensley ,  Donald Ellison

    IPC分类号： C08G63/02

    CPC分类号： C08G63/88 ,  G01N33/442

    摘要： An acetaldehyde screening method is developed by feeding solid polymer sample particles having a free acetaldehyde (“AA”) content of 2 ppm or less, melting at least a portion of the sample particles to obtain a polymer sample having a heat history, and thereafter measuring the amount of acetaldehyde present in the polymer sample having the heat history. There is also provided a screening method in which the quantity of free or residual AA in or on a polymer sample is measured to obtain a first value AAf, the sample is melted, and thereafter the amount of AA generated upon remelting the polymer is measured to obtain a second value AAg.

    摘要翻译： 通过将具有2ppm或更低的游离乙醛（“AA”）含量的固体聚合物样品颗粒进料到熔融至少一部分样品颗粒以获得具有热历史的聚合物样品，然后测量 存在于具有热历史的聚合物样品中的乙醛的量。 还提供了一种筛选方法，其中测量聚合物样品中或其上的游离或残留AA的量以获得第一值AAf，样品熔化，然后将聚合物重熔后产生的AA的量测量为 获得第二个值AAg。

    Polyester polymer and copolymer compositions containing titanium nitride particles
    9.
    发明申请
    Polyester polymer and copolymer compositions containing titanium nitride particles 有权
    含有氮化钛颗粒的聚酯聚合物和共聚物组合物

    公开(公告)号：US20060106146A1

    公开(公告)日：2006-05-18

    申请号：US11228672

    申请日：2005-09-16

    申请人： Zhiyong Xia ,  Steven Stafford ,  Susan Sims ,  Frederick Colhoun

    发明人： Zhiyong Xia ,  Steven Stafford ,  Susan Sims ,  Frederick Colhoun

    IPC分类号： C08K3/22

    CPC分类号： C08K3/28 ,  Y10T428/1321 ,  Y10T428/1359 ,  C08L67/00

    摘要： Polyester compositions are disclosed that include polyester polymers or copolymers having incorporated therein titanium nitride particles that provide one or more of the following advantages: improving the reheat properties of the compositions, improving the color of the compositions through reduced yellowness, and improving the UV-blocking properties of the compositions. Processes for making such compositions are also disclosed. The titanium nitride particles may be incorporated in the polyester by melt compounding, or may be added at any stage of the polymerization, such as during the melt-phase of the polymerization. A range of particle sizes may be used, as well as a range of particle size distributions. The polyester compositions are suitable for use in packaging made from processes in which a reheat step is desirable, or decreased yellowness is desired, or increased resistance to the effects of ultraviolet light is desired, or any combination of the foregoing.

    摘要翻译： 公开了聚酯组合物，其包括具有纳入其中的氮化钛颗粒的聚酯聚合物或共聚物，其提供一个或多个以下优点：改善组合物的再热性能，通过减少黄度改善组合物的颜色，并改善UV-阻断 组合物的性质。 还公开了制备这种组合物的方法。 可以通过熔融配混将氮化钛颗粒引入聚酯中，或者可以在聚合的任何阶段例如在聚合的熔融相期间加入。 可以使用一定范围的粒度，以及一定范围的粒度分布。 聚酯组合物适用于由期望再热步骤或期望减少黄色的方法制成的包装或期望提高对紫外光效果的耐受性，或上述任何组合。