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    Sorbent compositions
    5.
    发明授权
    Sorbent compositions 有权
    吸附剂组合物

    公开(公告)号：US06350422B1

    公开(公告)日：2002-02-26

    申请号：US09575518

    申请日：2000-05-22

    Applicant: Gyanesh P. Khare ,  Donald R. Engelbert

    Inventor： Gyanesh P. Khare ,  Donald R. Engelbert

    IPC: B01D5352

    CPC classification number: B01J20/28019 ,  B01D53/02 ,  B01J20/103 ,  B01J20/28004 ,  B01J20/28011 ,  B01J20/30 ,  Y10S502/517

    Abstract: A process for removing hydrogen sulfide from a fluid stream by contacting a hydrogen sulfide-containing stream with a sorbent composition wherein said sorbent composition is produced by mixing at least one zinc component which is zinc oxide or a compound convertible to zinc oxide, at least one silica component where the silica component comprises silica or a compound convertible to silica, at least one colloidal metal oxide, and optionally at least one pore generator component so as to form a mixture, extruding the mixture, sphering the resulting extrudate to form spherical particles having a size of form about 0.5 to about 15 millimeters drying the resulting spherical particles, calcining the dried particles, steaming the resulting calcined particles, sulfiding the steamed particles by contacting them with sulfides or sulfur at a temperature of about 200° C. to 1400° C. and subjecting the sulfided particles to a temperature sufficient to bum off substantially all of the sulfur on the sulfided particle so as to provide a sorbent composition having improved attrition and crush strength and which is then useful for the desulfurization of hydrogen sulfide-containing fluid stream.

    Abstract translation: 通过使含硫化氢的物流与吸附剂组合物接触来从流体物流中除去硫化氢的方法，其中所述吸附剂组合物是通过混合至少一种锌成分或氧化锌可转化成的化合物，至少一种 二氧化硅组分，其中二氧化硅组分包括二氧化硅或可转化为二氧化硅的化合物，至少一种胶体金属氧化物和任选的至少一个孔产生剂组分，以形成混合物，挤出混合物，将所得挤出物悬浮，形成具有 形成约0.5至约15毫米的尺寸，干燥所得的球形颗粒，煅烧干燥颗粒，蒸发所得煅烧颗粒，通过使蒸汽颗粒与硫化物或硫在大约200℃至1400℃的温度下接触来硫化蒸汽颗粒 并且使硫化颗粒经受足以烧毁基本上所有硫的温度的温度 以提供具有改善的磨耗和压碎强度的吸附剂组合物，然后可用于含硫化氢的流体物流的脱硫。

    Sorbent compositions
    6.
    发明授权
    Sorbent compositions 有权
    吸附剂组合物

    公开(公告)号：US5958830A

    公开(公告)日：1999-09-28

    申请号：US157608

    申请日：1998-09-21

    Applicant: Gyanesh P. Khare ,  Donald R. Engelbert

    Inventor： Gyanesh P. Khare ,  Donald R. Engelbert

    IPC: B01D53/02 ,  B01J20/10 ,  B01J20/28 ,  B01J20/30

    CPC classification number: B01J20/28019 ,  B01D53/02 ,  B01J20/103 ,  B01J20/28004 ,  B01J20/28011 ,  B01J20/30 ,  Y10S502/517

    Abstract: A process to make a sorbent composition said process comprising:(1) contacting(1.1) at least one zinc component, where said zinc component comprises zinc oxide, or a compound convertible to zinc oxide,(1.2) at least one silica component, where said silica component comprises silica, or a compound convertible to silica,(1.3) at least one colloidal oxide component, where said colloidal oxide component comprises a mixture that comprises a metal oxide, and optionally(1.4) at least one pore generator component; to form a first mixture; and thereafter,(2) extruding said first mixture to form an extruded, first mixture; and thereafter,(3) sphering said extruded, first mixture to form a sphered, extruded, first mixture that comprises particles where said particles have a particle size from about 0.5 to about 15 millimeters; and thereafter,(4) drying said sphered, extruded, first mixture to produce a dried, sphered, extruded, first mixture; or simultaneously therewith, or thereafter,(5) calcining said dried, sphered, extruded, first mixture to produce a calcined, dried, sphered, extruded, first mixture; and thereafter,(6) steaming said calcined, dried, sphered, extruded, first mixture, to form a steamed, calcined, dried, sphered, extruded, first mixture; and thereafter,(7) sulfiding said steamed, calcined, dried, sphered, extruded, first mixture, to form said sorbent composition.

    Abstract translation: 一种制备吸附剂组合物的方法，所述方法包括：（1）使（1.1）至少一种锌组分（其中所述锌组分包含氧化锌）或可转化为氧化锌的化合物，（1.2）至少一种二氧化硅组分，其中 所述二氧化硅组分包括二氧化硅或可转化为二氧化硅的化合物，（1.3）至少一种胶体氧化物组分，其中所述胶态氧化物组分包含包含金属氧化物的混合物，和任选地（1.4）至少一种孔发生剂组分; 形成第一混合物; 然后，（2）挤出所述第一混合物以形成挤出的第一混合物; 然后，（3）将所述挤出的第一混合物悬浮以形成包含颗粒的颗粒，其中所述颗粒具有约0.5至约15毫米的粒度; 然后，（4）干燥所述喷出的挤出的第一混合物以产生干燥的，挤出的挤出的第一混合物; 或与此同时或之后，（5）煅烧所述干燥的，挤出的，挤出的第一混合物，以产生煅烧，干燥，喷射，挤出的第一混合物; 然后，（6）将所述煅烧的，干燥的，喷射的，挤出的第一混合物蒸汽，以形成蒸，煅烧，干燥，喷射，挤出的第一混合物; 然后，（7）将所述蒸汽，煅烧，干燥，喷射，挤出的第一混合物硫化以形成所述吸附剂组合物。

    Process for removing sulfur compounds
    7.
    发明授权
    Process for removing sulfur compounds 失效
    去除硫化合物的方法

    公开(公告)号：US5219542A

    公开(公告)日：1993-06-15

    申请号：US727780

    申请日：1991-07-10

    Applicant: Richard E. Lowery ,  Donald R. Engelbert

    Inventor： Richard E. Lowery ,  Donald R. Engelbert

    IPC: B01D53/52 ,  C01B17/04

    CPC classification number: C01B17/04 ,  B01D53/523

    Abstract: A novel composition comprising zinc oxide, zinc phosphate and, optionally, alumina is described which can effectively be used to remove sulfur compounds from a fluid stream by contacting said fluid stream under suitable absorption conditions with the novel composition. A novel method of producing an absorption composition is described where the steps include the formation of a composition comprising zinc oxide, zinc phosphate and, optionally, alumina.

    Abstract translation: 描述了包含氧化锌，磷酸锌和任选的氧化铝的新型组合物，其可以有效地用于通过在合适的吸收条件下使所述流体物流与新组合物接触从流体物流中除去硫化合物。 描述了一种生产吸收组合物的新方法，其中步骤包括形成包含氧化锌，磷酸锌和任选的氧化铝的组合物。

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