Process for producing toluidine compound
    4.
    发明授权
    Process for producing toluidine compound 有权
    甲苯胺化合物的制备方法

    公开(公告)号:US08338612B2

    公开(公告)日:2012-12-25

    申请号:US12671050

    申请日:2008-07-29

    IPC分类号: C07D213/74

    CPC分类号: C07D213/72

    摘要: Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.

    摘要翻译: 由于氟啶胺作为农药的有效成分是优异的,而且是非常有用的,因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。 通过使用工业上有利的反应体系,通过使用包括(1)在碱组分,选自酮,腈的溶剂存在下使ACTF和DCDNBTF反应的步骤,以简单的操作获得所需产物 ,醚和酯和足够量的水以基本上溶解碱组分,(2)用酸中和或酸化反应混合物的步骤和(3)通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为 反应产物和反应溶剂使产物析出晶体。

    PROCESS FOR PRODUCING TOLUIDINE COMPOUND
    5.
    发明申请
    PROCESS FOR PRODUCING TOLUIDINE COMPOUND 有权
    生产托洛芬化合物的方法

    公开(公告)号:US20100197930A1

    公开(公告)日:2010-08-05

    申请号:US12671050

    申请日:2008-07-29

    IPC分类号: C07D213/36

    CPC分类号: C07D213/72

    摘要: Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.

    摘要翻译: 由于氟啶胺作为农药的有效成分是优异的,而且是非常有用的,因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。 通过使用工业上有利的反应体系,通过使用包括(1)在碱组分,选自酮,腈的溶剂存在下使ACTF和DCDNBTF反应的步骤,以简单的操作获得所需产物 ,醚和酯和足够量的水以基本上溶解碱组分,(2)用酸中和或酸化反应混合物的步骤和(3)通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为 反应产物和反应溶剂使产物析出晶体。

    Webbing winding device
    6.
    发明授权
    Webbing winding device 有权
    卷绕装置

    公开(公告)号:US09027865B2

    公开(公告)日:2015-05-12

    申请号:US13525921

    申请日:2012-06-18

    IPC分类号: B65H75/48 B60R22/34

    CPC分类号: B60R22/3413

    摘要: In a webbing winding device, even when a piston moves toward the other side in a movement direction due to a reaction when the piston moves to a maximum movement position, an engagement surface of a hook portion comes into contact with a subject engagement surface of a subject engagement portion, so that the movement of the piston toward the other side in the movement direction is restricted. Accordingly, the piston is prevented from returning to a standby position, and a pawl is prevented from returning to a lock position. For this reason, a state where a rotation of a locking ring in the pull-out direction is maintained. Accordingly, after the piston moves from the standby position to the maximum movement position, the piston is prevented from returning to the standby position, and the force limiter load is prevented from being changed.

    摘要翻译: 在一种织带缠绕装置中,即使当活塞在活塞移动到最大移动位置时由于反应而在活塞方向上朝向另一侧移动时,钩部的接合表面与主体接合表面接触 使得活塞向运动方向的另一侧的运动受到限制。 因此,防止活塞返回到待机位置,并且防止棘爪返回到锁定位置。 因此,保持锁定环在拉出方向上的旋转的状态。 因此,在活塞从待机位置移动到最大移动位置之后,防止活塞返回待机位置,防止力限制器的负载变化。

    Method for producing 3-methyl-2-thiophenecarboxylic acid
    8.
    发明授权
    Method for producing 3-methyl-2-thiophenecarboxylic acid 有权
    3-甲基-2-噻吩羧酸的制备方法

    公开(公告)号:US08350057B2

    公开(公告)日:2013-01-08

    申请号:US13000937

    申请日:2009-06-25

    IPC分类号: C07D333/40

    CPC分类号: C07D333/40

    摘要: A method for producing 3-methyl-2-thiophenecarboxylic acid is provided.A method for producing 3-methyl-2-thiophenecarboxylic acid, which comprises reacting a compound represented by the formula (I): (wherein X is a chlorine atom or a bromine atom) with magnesium in the presence of an alkyl halide to give a Grignard reagent represented by the formula (II): (wherein X is the same as defined above), reacting the Grignard reagent of the formula (II) with carbon dioxide, and acidifying the reaction product.

    摘要翻译: 提供了3-甲基-2-噻吩羧酸的制备方法。 一种3-甲基-2-噻吩羧酸的制备方法,其包括在烷基卤存在下使式(I)表示的化合物(其中X为氯原子或溴原子)与镁反应,得到 由式(II)表示的格利雅试剂(其中X与上述定义相同),使式(II)的格氏试剂与二氧化碳反应,并使反应产物酸化。

    METHOD FOR PRODUCING 3-METHYL-2-THIOPHENECARBOXYLIC ACID
    9.
    发明申请
    METHOD FOR PRODUCING 3-METHYL-2-THIOPHENECARBOXYLIC ACID 有权
    3-甲基-2-噻吩羧酸的制备方法

    公开(公告)号:US20110112311A1

    公开(公告)日:2011-05-12

    申请号:US13000937

    申请日:2009-06-25

    IPC分类号: C07D333/40

    CPC分类号: C07D333/40

    摘要: A method for producing 3-methyl-2-thiophenecarboxylic acid is provided.A method for producing 3-methyl-2-thiophenecarboxylic acid, which comprises reacting a compound represented by the formula (I): (wherein X is a chlorine atom or a bromine atom) with magnesium in the presence of an alkyl halide to give a Grignard reagent represented by the formula (II): (wherein X is the same as defined above), reacting the Grignard reagent of the formula (II) with carbon dioxide, and acidifying the reaction product.

    摘要翻译: 提供了3-甲基-2-噻吩羧酸的制备方法。 一种3-甲基-2-噻吩羧酸的制备方法,其包括在烷基卤存在下使式(I)表示的化合物(其中X为氯原子或溴原子)与镁反应,得到 由式(II)表示的格利雅试剂(其中X与上述定义相同),使式(II)的格氏试剂与二氧化碳反应,并使反应产物酸化。

    Webbing take-up device
    10.
    发明授权
    Webbing take-up device 有权
    织带收卷装置

    公开(公告)号:US08376258B2

    公开(公告)日:2013-02-19

    申请号:US12904955

    申请日:2010-10-14

    IPC分类号: B65H75/48

    CPC分类号: B60R22/46 B60R2022/468

    摘要: A webbing take-up device enabling a reduction in size of an overload release mechanism and easy adjustment of an operation torque of the overload release mechanism is provided. In the overload release mechanism of this webbing take-up device, rotary force of a large diameter gear is transmitted to a small diameter gear via plural annular friction springs. The friction springs are disposed between an inner periphery face of a main body portion of the large diameter gear and a tubular portion of the small diameter gear, side by side along an axial direction of the two gears. Consequently, a radial direction enlargement of the large diameter gear and small diameter gear due to space for disposing the friction springs may be restrained. Moreover, the operation torque of the overload release mechanism may be adjusted stepwise by changing the number of the friction springs to be used, in accordance with requirements.

    摘要翻译: 提供一种能够减小过载释放机构的尺寸并且容易调节过载释放机构的操作扭矩的织带卷取装置。 在这种织带卷取装置的过载释放机构中,大直径齿轮的旋转力通过多个环形摩擦弹簧传递到小直径齿轮。 摩擦弹簧沿着两个齿轮的轴向并排设置在大直径齿轮的主体部分的内周面和小直径齿轮的管状部分之间。 因此,可以抑制由于设置摩擦弹簧的空间而引起的大直径齿轮和小直径齿轮的径向扩大。 此外,可以根据要求通过改变要使用的摩擦弹簧的数量来逐步地调节过载释放机构的操作扭矩。