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    Method and device for producing dispersions
    4.
    发明授权
    Method and device for producing dispersions 有权
    生产分散体的方法和装置

    公开(公告)号：US07538142B2

    公开(公告)日：2009-05-26

    申请号：US10584464

    申请日：2004-12-01

    申请人： Wolfgang Lortz ,  Christoph Batz-Sohn

    发明人： Wolfgang Lortz ,  Christoph Batz-Sohn

    IPC分类号： B01F5/02 ,  B01F3/10 ,  B01F5/10

    CPC分类号： B01F13/1041 ,  B01F3/12 ,  B01F5/0256 ,  B01F5/102 ,  B01F2013/1083 ,  B01F2015/061 ,  B01F2215/0431 ,  B01F2215/0468 ,  B02C19/065

    摘要： A method and device for producing a finely divided dispersion of solids having a mean particle size of 10 nm to 10 µm, in which at least two flows of a predispersion are sprayed by means of pumps, preferably high-pressure pumps, through one nozzle each into a grinding chamber enclosed by a reactor housing onto a collision point, wherein the grinding chamber is flooded with the predispersion and the finally divided dispersion is removed from the grinding chamber by the overpressure of the predispersion continuing to flow into the grinding chamber.

    摘要翻译： 一种用于生产平均粒径为10nm至10μm的细分散固体分散体的方法和装置，其中通过泵，优选高压泵将至少两个预分散液流喷射至每个 进入由反应器壳体围绕在碰撞点上的研磨室中，其中研磨室充满预分散体，并且最终分散的分散体通过预分散体的超压继续流入研磨室而从研磨室移除。

    Titanium dioxide coated with silicon dioxide
    5.
    发明申请
    Titanium dioxide coated with silicon dioxide 有权
    二氧化钛涂覆二氧化硅

    公开(公告)号：US20060057385A1

    公开(公告)日：2006-03-16

    申请号：US10539061

    申请日：2003-12-02

    申请人： Kai Schumacher ,  Christoph Batz-Sohn ,  Steffen Hasenzahl

    发明人： Kai Schumacher ,  Christoph Batz-Sohn ,  Steffen Hasenzahl

    IPC分类号： C09C1/36 ,  B32B5/16

    CPC分类号： C09C1/3661 ,  C01G23/07 ,  C01P2004/03 ,  C01P2004/84 ,  C01P2006/12 ,  C01P2006/90 ,  Y10T428/2993

    摘要： Powder consisting of particles with a core of titanium dioxide and a coating of silicon dioxide, which powder has a content of silicon dioxide of between 0.5 and 40 wt. %, a BET surface of between 5 and 300 m2/g, and which consists of primary particles that have a coating of silicon dioxide and a core of titanium dioxide. The powder is produced according to a process in which a vaporisable silicon compound and a vaporisable titanium compound are mixed corresponding to the subsequently desired ratio of SiO2 and TiO2 in the product, are vaporised at temperatures of 200° C. or less, and conveyed by means of an inert gas stream together with hydrogen and air or with oxygen-enriched air to the central pipe (core) of a known burner, the reaction mixture is ignited at the mouth of the burner and introduced together with secondary air, is combusted in a cooled flame pipe, following which the titanium dioxide powder coated with silicon dioxide is separated from the gaseous reaction products and if necessary is freed in moist air from adhering hydrogen chloride, the ratio of primary air to secondary air being greater than 0.3, the ratio of core hydrogen to secondary air being greater than 1, and the ratio of titanium dioxide precursor to secondary air being greater than 0.5. Sunscreen agent containing the powder in an amount of between 0.01 and 25 wt. %.

    摘要翻译： 由具有二氧化钛核心和二氧化硅涂层的颗粒组成的粉末，该粉末的二氧化硅含量为0.5〜40重量％。 ％，BET表面积在5和300m 2 / g之间，并且其由具有二氧化硅涂层和二氧化钛核心的一次粒子组成。 该粉末根据其中可蒸发的硅化合物和可蒸发的钛化合物混合的方法制备，相应产物中随后所需的SiO 2和TiO 2的比例 ，在200℃或更低的温度下蒸发，并通过惰性气体流与氢气和空气或富氧空气一起输送到已知燃烧器的中心管（核心）上，将反应混合物点燃 在燃烧器的口处并与二次空气一起引入，在冷却的火焰管中燃烧，随后将二氧化硅涂覆的二氧化钛粉末与气态反应产物分离，如果需要，在潮湿的空气中从附着的氯化氢 ，一次空气与二次空气的比例大于0.3，核心氢气与二次空气的比例大于1，二氧化钛前体与二次空气的比例大于0.5。 含有粉末的防晒剂的量为0.01至25wt。 ％。

    Methods for producing a dispersion containing silicon dioxide particles and cationization agent
    8.
    发明授权
    Methods for producing a dispersion containing silicon dioxide particles and cationization agent 有权
    生产含有二氧化硅颗粒和阳离子化剂的分散体的方法

    公开(公告)号：US08980960B2

    公开(公告)日：2015-03-17

    申请号：US13642862

    申请日：2011-05-23

    申请人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    发明人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    IPC分类号： C01B33/141 ,  C09C1/28 ,  D21H19/40 ,  B41M5/52 ,  B41M5/42

    CPC分类号： B41M5/5218 ,  B41M5/426 ,  C01B33/141 ,  D21H19/40

    摘要： Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of cationizing agent per square meter of the BET surface area of the silicon dioxide particles, wherein the cationizing agent is obtainable by reacting at least one haloalkyl-functional alkoxysilane, hydrolysis products, condensation products and/or mixtures thereof with at least one aminoalcohol and water; and optionally removing the resulting hydrolysis alcohol from the reaction mixture. Also the process for preparing the dispersion, wherein the cationizing agent comprises one or more quaternary, aminoalcohol-functional, organosilicon compounds of formula III and/or condensation products thereof, wherein Ru and Rv are independently C2-4 alkyl group, m is 2-5 and n is 2-5.

    摘要翻译： 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂可通过使至少一种卤代烷基官能的烷氧基硅烷，水解产物，缩合产物和/或其与至少一种氨基醇的混合物和 水; 并任选地从反应混合物中除去所得的水解醇。 还有制备分散体的方法，其中阳离子化剂包含一种或多种式III的季氨基醇官能的有机硅化合物和/或其缩合产物，其中Ru和Rv独立地是C 2-4烷基，m是2- 5，n为2-5。

    METHODS FOR PRODUCING A DISPERSION CONTAINING SILICON DIOXIDE PARTICLES AND CATIONIZATION AGENT
    9.
    发明申请
    METHODS FOR PRODUCING A DISPERSION CONTAINING SILICON DIOXIDE PARTICLES AND CATIONIZATION AGENT 有权
    生产含二氧化硅颗粒和起泡剂的分散体的方法

    公开(公告)号：US20130040078A1

    公开(公告)日：2013-02-14

    申请号：US13642862

    申请日：2011-05-23

    申请人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    发明人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    IPC分类号： C09D5/00 ,  B41M5/50 ,  C09D129/04

    CPC分类号： B41M5/5218 ,  B41M5/426 ,  C01B33/141 ,  D21H19/40

    摘要： Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent is obtainable by reacting at least one haloalkyl-functional alkoxysilane, its hydrolysis products or condensation products and/or a mixture thereof with at least one aminoalcohol and a defined amount of water and optionally removing the resulting hydrolysis alcohol at least partly from the reaction mixture.Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of a cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent comprises one or more quaternary, aminoalcohol-functional, organosilicon compounds of the general formula III and/or condensation products thereof, wherein Ru and Rv are each independently of each other an alkyl group having 2 to 4 carbon atoms, m is 2 to 5 and n is 2 to 5.

    摘要翻译： 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂可通过使至少一种卤代烷基官能的烷氧基硅烷，其水解产物或缩合产物和/或其混合物与至少一种 氨基醇和限定量的水，并任选地从反应混合物中部分地除去所得的水解醇。 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂包含一种或多种通式III的季铵，氨基醇官能的有机硅化合物和/或其缩合产物，其中Ru和 Rv各自独立地为具有2至4个碳原子的烷基，m为2至5，n为2至5。