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    Benzisothiazole- and benzothiophene-azo dyes with a coupling component of the aniline series
    1.
    发明授权
    Benzisothiazole- and benzothiophene-azo dyes with a coupling component of the aniline series 失效
    苯并异噻唑和苯并噻吩 - 偶氮染料与苯胺系列的偶联组分

    公开(公告)号：US5342928A

    公开(公告)日：1994-08-30

    申请号：US054230

    申请日：1993-04-30

    申请人： Thomas Roetsch ,  Helmut Hagen ,  Helmut Reichelt ,  Clemens Grund

    发明人： Thomas Roetsch ,  Helmut Hagen ,  Helmut Reichelt ,  Clemens Grund

    IPC分类号： C09B29/09 ,  B41M5/388 ,  C09B29/00 ,  C09B29/03 ,  C09B29/033 ,  C09B29/045 ,  D06P1/18

    CPC分类号： B41M5/388 ,  C09B29/0059 ,  C09B29/0081 ,  Y10S428/913 ,  Y10S428/914

    摘要： Azo dyes useful for dyeing or printing textile fibers or fabrics and containing novel aminobenzo heterocycles as diazo component have the formula ##STR1## where X is nitrogen or a radical of the formula CR.sup.6, where R.sup.6 is hydrogen, C.sub.1 -C.sub.4 -alkoxycarbonyl or C.sub.1 -C.sub.6 -alkanoyl,R.sup.1 and R.sup.2 are substituted or unsubstituted C.sub.1 -C.sub.10 -alkyl or substituted or unsubstituted C.sub.3 -C.sub.4 -alkenyl or additionally in the case of R.sup.1 hydrogen,R.sup.3 is hydrogen or C.sub.1 -C.sub.4 -alkoxy,R.sup.4 is C.sub.1 -C.sub.6 -alkyl, C.sub.1 -C.sub.4 -alkoxy, substituted or unsubstituted C.sub.1 -C.sub.8 -alkanoylamino, C.sub.1 -C.sub.4 -alkylsulfonylamino, C.sub.3 -C.sub.4 -alkenoylamino or substituted or unsubstituted C.sub.1 -C.sub.4 -alkoxycarbonylamino, andR.sup.5 is hydrogen, nitro, halogen, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -alkylthio or cyano.

    摘要翻译： 可用于染色或印刷纺织纤维或织物并含有新的氨基苯并杂环作为重氮组分的偶氮染料具有式“IMAGE”，其中X是氮或式CR 6的基团，其中R 6是氢，C 1 -C 4 - 烷氧基羰基或C 1 -C 4 - C 1 -C 6烷酰基，R 1和R 2是取代或未取代的C 1 -C 10 - 烷基或取代或未取代的C 3 -C 4 - 链烯基或另外在R 1氢的情况下，R 3是氢或C 1 -C 4烷氧基，R 4是C 1 -C 6 - 烷基，C 1 -C 4 - 烷氧基，取代或未取代的C 1 -C 8 - 烷酰基氨基，C 1 -C 4 - 烷基磺酰基氨基，C 3 -C 4 - 烯酰基氨基或取代或未取代的C 1 -C 4烷氧基羰基氨基，R 5为氢，硝基，卤素，C 1 -C 4 - 烷氧基，C 1 -C 4 - 烷硫基或氰基。

    Azo dyes with a diazo component of the 3-amino thiophene series and a coupling component of the pyridine, pyridone or pyrazole series
    5.
    发明授权
    Azo dyes with a diazo component of the 3-amino thiophene series and a coupling component of the pyridine, pyridone or pyrazole series 失效
    具有3-氨基噻吩系列的重氮组分的偶氮染料和吡啶，吡啶酮或吡唑系的偶联组分

    公开(公告)号：US4994564A

    公开(公告)日：1991-02-19

    申请号：US269646

    申请日：1988-11-10

    申请人： Karl-Heinz Etzbach ,  Helmut Reichelt ,  Guenter Hansen ,  Ernst Schefczik ,  Helmut Hagen ,  Gunther Lamm

    发明人： Karl-Heinz Etzbach ,  Helmut Reichelt ,  Guenter Hansen ,  Ernst Schefczik ,  Helmut Hagen ,  Gunther Lamm

    IPC分类号： C09B29/09 ,  C09B29/00 ,  C09B29/42 ,  C09B29/48

    CPC分类号： C09B29/0059 ,  C09B29/3621 ,  C09B29/3634 ,  C09B29/3656

    摘要： Thien-3-ylazo dyes of the formula: ##STR1## where X is cyano, nitro, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are identical or different and each is independently of each other substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.3 -C.sub.4 -alkenyl, substituted or unsubstituted phenyl or together with the nitrogen atom linking them a 5- or 6-membered saturated heterocyclic radical, and R.sup.2 may additionally be hydrogen, Y is hydrogen, cyano, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, C.sub.1 -C.sub.4 -alkylsulfonyl, substituted or unsubstituted phenylsulfonyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are each as defined above, Z is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, substituted or unsubstituted phenyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylthio, substituted or unsubstituted phenylthio, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylsulfonyl or phenylsulfonyl or together with the radical Y a fused benzo ring which may be substituted, and K is the radical of a coupling component of the 2,6-diaminopyridine, 6-hydroxypyrid-2-one or 5-aminopyrazole series, are used for dyeing synthetic fiber materials, in particular synthetic polyesters, in yellow to red shades and are notable for good light fastness, fastness to dry heat setting and pleating and for good affinity.

    摘要翻译： 噻吩-3-基偶氮染料，其结构式如下：其中X为氰基，硝基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R 1和R 2相同或不同， 各自独立地为取代或未取代的C 1 -C 8 - 烷基，C 5 -C 7 - 环烷基，C 3 -C 4 - 烯基，取代或未取代的苯基或与连接它们的氮原子一起形成5-或6-元饱和杂环基， R 2可另外为氢，Y为氢，氰基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，C 1 -C 4 - 烷基磺酰基，取代或未取代的苯基磺酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R1和R2为 Z是氢，取代或未取代的C 1 -C 8 - 烷基，取代或未取代的苯基，取代或未取代的C 1 -C 6 - 烷硫基，取代或未取代的苯硫基，取代或未取代的C 1 -C 6 - 烷基磺酰基 或与苯基磺酰基或与基团Y一起可以被取代的稠合苯并环，K是2,6-二氨基吡啶，6-羟基吡啶-2-酮或5-氨基吡唑系列的偶联组分的基团 用于将合成纤维材料，特别是合成聚酯染色为黄色至红色，并且具有良好的耐光性，耐干燥定型和打褶的牢度以及良好的亲和力。

    Method of producing 2-alkyl-3-(4,5-dihydroisoxazole-3-yl)-halobenzenes
    7.
    发明授权
    Method of producing 2-alkyl-3-(4,5-dihydroisoxazole-3-yl)-halobenzenes 有权
    2-烷基-3-（4,5-二氢异恶唑-3-基） - 卤代苯的制备方法

    公开(公告)号：US06548677B1

    公开(公告)日：2003-04-15

    申请号：US09856037

    申请日：2001-05-17

    申请人： Michael Rack ,  Norbert Götz ,  Helmut Hagen ,  Wolfgang von Deyn ,  Ernst Baumann ,  Rene Lochtman ,  Joachim Gebhardt

    发明人： Michael Rack ,  Norbert Götz ,  Helmut Hagen ,  Wolfgang von Deyn ,  Ernst Baumann ,  Rene Lochtman ,  Joachim Gebhardt

    IPC分类号： C07D26118

    CPC分类号： C07D261/04

    摘要： A novel process for preparing the compounds of the formula I where: n is 0, 1 or 2; R1, R2 are C1-C6-alkyl; R3, R4, R5 are hydrogen or C1-C6-alkyl, or R4 and R5 together form a bond; R6 is Cl, Br, which comprises a synthesis sequence starting from 1,2-dialkylbenzenes of the formula II with subsequent halogenation to give 3,6-dihalo-1,2-dialkylbenzenes, haloalkylation to give benzyl bromides, oxidation to give benzaldehydes, oximation, reaction with alkenes to give isoxazoles, conversion into thioethers and, if appropriate, oxidation to give sulfenyl or sulfonyl derivatives of the formula I.

    摘要翻译： 一种制备式I化合物的新方法，其中n为0,1或2; R 1，R 2为C 1 -C 6 - 烷基; R 3，R 4，R 5为氢或C 1 -C 6烷基，或者R 4和R 5一起形成 R 6是Cl，Br，其包含从式II的1,2-二烷基苯开始的合成序列，随后卤化以得到3,6-二卤代-1,2-二烷基苯，卤代烷基化得到苄基溴，氧化得到 苯甲醛，肟化，与烯烃的反应得到异恶唑，转化成硫醚，如果合适，氧化得到式I的磺酰基或磺酰基衍生物。

    Herbicides containing substituted 2-aminothiophenes
    8.
    发明授权
    Herbicides containing substituted 2-aminothiophenes 失效

    公开(公告)号：US5422335A

    公开(公告)日：1995-06-06

    申请号：US70389

    申请日：1993-06-07

    申请人： Helmut Hagen ,  Gerhard Nilz ,  Helmut Walter ,  Andreas Landes

    发明人： Helmut Hagen ,  Gerhard Nilz ,  Helmut Walter ,  Andreas Landes

    IPC分类号： A01N25/32 ,  A01N35/06 ,  A01N39/02 ,  A01N43/10 ,  C07D333/38 ,  C07D333/68 ,  C07D333/70 ,  C07D409/04 ,  C07D409/12 ,  C07D417/12 ,  A01N43/12 ,  A01N47/24 ,  C07D333/54

    CPC分类号： C07D409/04 ,  A01N25/32 ,  C07D333/38 ,  C07D333/68 ,  C07D409/12 ,  C07D417/12

    摘要： A herbicidal composition containing one or more substituted 2-aminothiophenes of the formula I ##STR1## where R.sup.1 and R.sup.2 together from a C.sub.4 -alkylene chain to which a benzene ring may be fused,R.sup.3 is --CN or CX--R.sup.6, where R.sup.6 is hydroxyl, C.sub.1 -C.sub.4 -alkoxy or amino,R.sup.4 is hydrogen or a phenyl group which may carry one or two nitro radicals,--PO(OR.sup.8).sub.2, --CX--R.sup.9, --SO.sub.2 R.sup.10, --CX--N(H) --CO--R.sup.8 or --CX--N(R.sup.7)--SO.sub.2 --R.sup.11,whereR.sup.8 is hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl groupR.sup.9 is C.sub.1 -C.sub.20 -alkyl, partially or completely halogenated C.sub.1 -C.sub.6 -alkyl, C.sub.2 -C.sub.6 -alkenyl, C.sub.6 -cycloalkyl, or amino, C.sub.1 -C.sub.4 -alkylamino, C.sub.3 -C.sub.8 -cycloalkylamino, phenyl or phenylamino, where the aromatic moiety may carry at least one of nitro and halogen;R.sup.10 is C.sub.1 -C.sub.4 -alkyl or phenyl, which may carry one C.sub.1 -C.sub.4 -alkyl radical;R.sup.11 is pyrrolidin-1-yl, piperidin-1-yl, morpholin-4-yl or piperazin-1-yl, where the heterocyclic structures may carry one C.sub.1 -C.sub.4 -group;R.sup.5 is hydrogen;orR.sup.4 and R.sup.5 together form a group .dbd.CR.sup.12 R.sup.13 or --CO--W--CO--, where R.sup.12 is hydrogen, amino, C.sub.1 -C.sub.4 -alkylamino or C.sub.3 -C.sub.8 -cycloalkylamino;R.sup.13 is amino, C.sub.3 -C.sub.8 -cycloalkylamino, phenyl or pyridyl, where the two last mentioned substituents may carry at least one halogen or nitro radicals;W is an ethylene or ethenylene bridge, or a 6-membered 1,2-C-bonded aromatic bridge where these bridge members may carry, on each substitutable carbon atom, at least one halogena 5-membered or 6-membered 1,2-C-bonded cycloalkylene or cycloalkenylene bridge,and the basic salts of the compounds I in which R.sup.3 is hydroxycarbonyl or hydroxythiocarbonyl, and the acidic salts of the compounds I which contain a basic nitrogen atom, as antagonistic compoundsand one or more herbicidal active ingredients from the group consisting ofthe cyclohexenone derivatives of the formula III ##STR2##

    2-amino-4-trichloropyridine derivatives
    9.
    发明授权
    2-amino-4-trichloropyridine derivatives 失效
    2-氨基-4-三氯吡啶衍生物

    公开(公告)号：US5216171A

    公开(公告)日：1993-06-01

    申请号：US681254

    申请日：1991-04-08

    申请人： Helmut Hagen ,  Hans Ziegler ,  Juergen Pfister ,  Gerhard Nilz ,  Gisela Lorenz ,  Juergen Dressel

    发明人： Helmut Hagen ,  Hans Ziegler ,  Juergen Pfister ,  Gerhard Nilz ,  Gisela Lorenz ,  Juergen Dressel

    IPC分类号： C05G3/08 ,  C07D213/74 ,  C07D213/75 ,  C07D213/76 ,  C07D401/04 ,  C07F9/58

    CPC分类号： C07D213/74 ,  C07D213/75 ,  C07D213/76 ,  C07D401/04 ,  C07F9/588 ,  Y02P60/218 ,  Y10S106/90

    摘要： 2-Amino-4-trichloromethylpyridines of the general formula I ##STR1## where R.sup.1 is hydrogen or C.sub.1 -C.sub.8 -alkyl,R.sup.2 is C.sub.1 -C.sub.8 -alkyl, C.sub.5 -C.sub.8 -cycloalkyl, C.sub.2 -C.sub.4 -alkenyl or phenyl, benzyl or phenylsulfonyl,--CX--R.sup.3, --SO.sub.2 R.sup.3 or --PX(OR.sup.4).sub.2 orR.sup.1 and R.sup.2 together form .dbd.CR.sup.5 R.sup.6 or --CO--Z--CO--,X is oxygen or sulfur,R.sup.3 is C.sub.1 -C.sub.20 -alkyl, C.sub.2 -C.sub.6 -alkenyl, amino, C.sub.1 -C.sub.6 -alkylamino, di-C.sub.1 -C.sub.6 -alkylamino, morpholino, piperidino, pyrazolidino or C.sub.1 -C.sub.8 -alkylcarbonylamino, substituted or unsubstituted phenylamino or benzylamino,R.sup.4 is C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -haloalkyl or substituted or unsubstituted phenyl,R.sup.5 is hydrogen, C.sub.1 -C.sub.4 -alkyl, or substituted or unsubstituted phenyl,R.sup.6 is substituted or unsubstituted phenyl,Z is substituted or unsubstituted ethylene which may be part of a substituted or unsubstituted cycloalkyl or cycloalkylene radical, substituted or unsubstituted ethenylene which may be part of a substituted or unsubstituted aromatic or heteroaromatic ring, and Z is not part of an unsubstituted phenyl radical, agriculturally useful salts thereof, processes for their preparation and the use thereof as nitrification inhibitors.

    摘要翻译： 通式I的2-氨基-4-三氯甲基吡啶其中R1是氢或C1-C8-烷基，R2是C1-C8-烷基，C5-C8-环烷基，C2-C4-烯基或苯基，苄基 或苯基磺酰基，-CX-R3，-SO2R3或-PX（OR4）2或R1和R2一起形成= CR5R6或-CO-Z-CO-，X是氧或硫，R3是C1-C20-烷基，C2- C 1 -C 6 - 烯基，氨基，C 1 -C 6 - 烷基氨基，二-C 1 -C 6烷基氨基，吗啉代，哌啶子基，吡唑烷基或C 1 -C 8烷基羰基氨基，取代或未取代的苯基氨基或苄基氨基，R 4是C 1 -C 8烷基， 卤代烷基或取代或未取代的苯基，R 5是氢，C 1 -C 4烷基或取代或未取代的苯基，R 6是取代或未取代的苯基，Z是可以是取代或未取代的环烷基或环亚烷基的一部分的取代或未取代的乙烯 取代或未取代的亚乙烯基，其可以是取代或未取代的芳族或杂芳族环的一部分，Z不是未取代的苯基的一部分，农业 其文化上有用的盐，其制备方法及其作为硝化抑制剂的用途。