摘要:
There is disclosed a method for eliminating an organic dispersion medium from a molded product obtained by plasticizing-molding or casting-molding of metallic and/or ceramic powders wherein the elimination is by extraction by liquid carbon dioxide at a temperature not lower than -30.degree. C. and not higher than -31.1.degree. C. The method prevents nonuniform volumetric decrease of the molded product to be otherwise caused by the extraction of the organic dispersion medium, while also making it possible to completely eliminate the organic dispersion medium without causing residual strain or deformation in the molded product.
摘要:
A tetrafluoroethylene-type fluoroplastic powder is added and mixed with a metal powder and the mixture is shaped. The compact is heated in a nonoxidizing atmosphere and the oxides on the surface of the metal particles are converted and removed as gaseous fluorides. Alternatively, after the oxides are converted to solid or liquid fluorides, the fluorides are reduced by hydrogen and then they are removed as gaseous reaction products. Thereafter, the compact is sintered.
摘要:
A method of sintering compacts of metals, ceramics and the like in powder form. At least the surface portion of the compact is sintered in a plasma atmosphere having a pressure of 10 Torr or less thereby eliminating the open voids and then the compact is subjected to a hot isostatic press process.
摘要:
The invention is concerned with the method of compression molding a metallic or ceramic powders. The method includes the step of maintaining a negative pressure within a first mold of noncompactable powders for intimately contacting on its inner surface a pouch-like member of thin-walled resilient material for producing a second mold, and the step of compactly charging starting powders into the second mold and exhausting air from and sealing the second mold, taking out a pre-molded body of the metallis or ceramic powders together with the second mold and the step of processing the pre-molded body by a cold or hot isostatic press.
摘要:
There is provided a method of blast furnace operation utilizing selective recycling of peripheral gas stream wherein the number of outlet ports for peripheral gas stream and the position of the gas outlet ports relative to the inlet ports for reducing gas are optimalized and the content of nitrogen in the recycling gas and the content of nitrogen in the reducing gas to be injected are controlled within the respective predetermined ranges.
摘要:
A method for eliminating a dispersion medium from a molded product obtained by plasticizing-molding or casting-molding one or more of metallic and ceramic powders, wherein the elimination process is carried out in a supercritical liquid carbon dioxide atmosphere without heating to higher temperatures.
摘要:
A method and an apparatus for continuously manufacturing non-fired pellets, which comprise: continuously supplying green pellets containing a carbonating binder into a vertical type reactor to continuously pass the green pellets sequentially through a predrying zone, a carbonating zone and a drying zone in the vertical type reactor; blowing a predrying gas having a relative humidity of up to 70% and a temperature of from 40.degree. to 250.degree. C. into the predrying zone to predry the green pellets therein until the water content of the green pellets in the predyring zone falls within the range of from 1 to 7 wt. %; blowing a carbonating gas comprising carbon dioxide gas of from 5 to 95 vol. % and saturated steam of from 5 to 95 vol. % and having a temperature of from 30.degree. to 98.degree. C. into the carbonating zone to carbonate the carbonating binder contained in the green pellets therein; and blowing a drying gas at a temperature of from 100.degree. to 300.degree. C. into the drying zone to harden the green pellets therein, thereby continuously manufacturing non-fired pellets.
摘要:
A method of producing a silicon nitride sintered body which comprises using an amorphous Si.sub.3 N.sub.4 powder having a mean particle size of 5 to 50 nm, a nitrogen content of 30 to 39 wt. %, an oxygen content of 1 to 10 wt. %, the sum of the nitrogen content and the oxygen content being 38 to 42 wt. % and an unavoidable impurities content of less than 500 ppm as the raw material to form a molded body, sealing the molded body in a capsule and treating it with HIP in the range of 1000.degree. to 1800.degree. C. and 1000 to 2000 atm until the density becomes 3.1 to 3.4 g/cm.sup.3. In the method of the invention, active surface energy of silicon nitride powder is utilized as the driving force for sintering due to using a super fine powder. The super fine powder improves sintering ability by uniform mixing. The sintering ability is further improved by substituting a suitable amount of the nitrogen in the silicon nitride with oxygen. By the above means, the sintering strength can be secured under not severe sintering conditions. As a result, a sintering aid can be omitted.
摘要:
In the method of invention, the formability is imparted to the slurry of a metal or ceramic powder by employing a porous mold and removing the dispersion medium through the evaporation or thermal decomposition thereof, or by using a silazane oil as the dispersion medium and curing it by heating. Since the phase change usually accompanying volume change does not occur in the dispersion medium, strain and deformation rarely occur in the molded body. As result, the sintered body obtained has high dimensional accuracy.
摘要:
A method for molding powders which comprises introducing a thin-wall resilient mold inside a ventilative mold support, reducing the outside pressure of the ventilative mold support to less than the atmospheric pressure (760 Torr), putting a thin-wall resilient mold exactly close to the inside wall of the ventilative mold support, supplying powder material into the thin-wall resilient mold, exhausting air existing in the voids formed in the powder material, and taking the ventilative mold support apart to apply cold isostatic press treatment to the thin-wall resilient mold. The shape of the thin-wall resilient mold is similar to the shape of the ventilative mold support.