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公开(公告)号：US20180305277A1
公开(公告)日：2018-10-25
申请号：US15491796
申请日：2017-04-19
Applicant: UOP LLC
Inventor： Ashish Suresh Bambal , Anton N. Mlinar , James A. Johnson
IPC: C07C5/27
Abstract: Processes and apparatuses for producing para-xylenes are provided. The processes comprises providing a hydrocarbon stream comprising C7+ hydrocarbons. The hydrocarbon stream is separated to provide a C8 aromatics stream and an ortho-xylene rich stream. The C8 aromatics stream is passed to a para-xylene separation unit for separating para-xylene to provide a para-xylene stream and a raffinate stream. At least a portion of the raffinate stream is passed to a first isomerization unit to provide a first isomerization effluent, wherein the first isomerization effluent is produced in the presence of an ethylbenzene (EB) isomerization catalyst. At least a portion of the ortho-xylene rich stream is contacted with an isomerization catalyst in a second isomerization unit in liquid phase at isomerization conditions in substantial absence of hydrogen to produce a second isomerization effluent.
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2.发明授权Process for converting polycyclic aromatic compounds to monocyclic aromatic compounds 有权将多环芳香族化合物转化成单环芳香族化合物的方法公开(公告)号：US09061953B2
公开(公告)日：2015-06-23
申请号：US14471621
申请日：2014-08-28
Applicant: UOP LLC
Inventor： James A. Johnson , John Q. Chen , Peter K. Coughlin , Stanley J. Frey , Vasant P. Thakkar
IPC: C07C4/26 , C07C4/02 , C07C5/02 , C10G47/00 , C07C4/06 , C07C4/04 , C10G1/04 , C07C7/12 , C01B3/34
CPC classification number: C01B3/34 , C07C5/11 , C07C7/04 , C07C2529/072 , C07C2529/076 , C07C2602/28 , C10G1/002 , C10G69/06 , C10G2400/20 , C10G2400/30 , Y02P30/464 , C07C13/48 , C07C15/24
Abstract: A process for converting polycyclic aromatic compounds to monocyclic aromatic compounds includes pyrolyzing a coal feed to produce a coke stream and a coal tar stream. The coal tar stream is cracked, and the cracked coal tar stream is fractionated to produce an aromatic fraction comprising the polycyclic aromatic compounds. The process further includes hydrocracking the aromatic fraction to partially hydrogenate at least a first portion of the aromatic fraction, and to open at least one ring of a second portion of the aromatic fraction to form the monocyclic aromatic compounds from the polycyclic compounds, and recycling the first portion of the aromatic fraction.
Abstract translation: 将多环芳族化合物转化为单环芳族化合物的方法包括热解煤原料以产生焦炭流和煤焦油流。 煤焦油流裂化，裂解煤焦油流分馏，生成包含多环芳族化合物的芳族馏分。 该方法还包括将芳族馏分加氢裂化以部分氢化至少第一部分芳族馏分，并且打开芳族馏分的第二部分的至少一个环以从多环化合物形成单环芳族化合物，并将 芳族馏分的第一部分。
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公开(公告)号：US20150141724A1
公开(公告)日：2015-05-21
申请号：US14467723
申请日：2014-08-25
Applicant: UOP LLC
Inventor： Stanley J. Frey , Paul T. Barger , Maureen L. Bricker , John Q. Chen , Peter K. Coughlin , James A. Johnson , Joseph A. Kocal , Matthew Lippmann , Vasant P. Thakkar , Kurt M. Vanden Bussche
CPC classification number: C07C4/18 , C07C4/06 , C07C7/12 , C07C2521/12 , C07C2529/06 , C07C2529/18 , C10B53/00 , C10C1/205 , C10G1/002 , C10G1/02 , C10G45/08 , C10G45/10 , C10G45/12 , C10G45/50 , C10G45/52 , C10G45/54 , C10G47/04 , C10G47/16 , C10G47/18 , C10G47/20 , C10G65/12 , C10G2300/1096 , C10G2400/30 , C07C15/06
Abstract: A process for selectively dealkylating aromatic compounds includes providing a coal tar stream comprising aromatic compounds and hydrotreating the coal tar stream to reduce a concentration of one or more of organic sulfur, nitrogen, and oxygen in the coal tar stream, and to hydrogenate at least a portion of the aromatic compounds in the coal tar stream. The process further includes hydrocracking the hydrotreated coal tar stream to further hydrogenate the aromatic compounds and to crack at least one ring of multi-ring aromatic compounds to form single-ring aromatic compounds. The single-ring aromatic compounds present in the hydrocracked stream are then dealkylated to remove alkyl groups containing two or more carbon atoms.
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公开(公告)号：US20150141700A1
公开(公告)日：2015-05-21
申请号：US14466660
申请日：2014-08-22
Applicant: UOP LLC
Inventor： James A. Johnson , Paul T. Barger , Maureen L. Bricker , John Q. Chen , Peter K. Coughlin , Stanley J. Frey , Joseph A. Kocal , Matthew Lippmann , Vasant P. Thakkar
CPC classification number: C07C2/66 , C07C2/864 , C07C5/2729 , C07C6/126 , C07C7/10 , C10C1/205 , C10G21/00 , C10G29/205 , C10G45/00 , C10G69/06 , C10G2300/1044 , C10G2400/30 , C07C15/08 , C07C15/073 , C07C15/085 , C07C15/02
Abstract: A process for producing alkylated aromatic compounds includes pyrolyzing a coal feed to produce a coke stream and a coal tar stream. The coal tar stream is hydrotreated and the resulting hydrotreated coal tar stream is cracked. A portion of the cracked coal tar stream is separated to obtain a fraction having an initial boiling point in the range of about 60° C. to about 180° C., and an aromatics-rich hydrocarbon stream is extracted by contacting the fraction with one or more solvents. The aromatics-rich hydrocarbon stream is contacted with an alkylating agent to produce an alkylated aromatic stream, or the aromatics-rich hydrocarbon stream is reacted with an aliphatic compound or methanol in the presence of a catalyst to produce a methylated aromatic stream. The alkylated aromatic stream, the methylated aromatic stream, or both are separated into at least a benzene stream, a toluene stream, and a xylenes stream.
Abstract translation: 制备烷基化芳族化合物的方法包括热解煤进料以产生焦炭流和煤焦油流。 将煤焦油流加氢处理，得到的加氢处理煤焦油流裂化。 将一部分裂化煤焦油流分离，得到初馏点在约60℃至约180℃范围内的馏分，并通过使该馏分与一个馏分接触而提取富含芳烃的烃流 或更多的溶剂。 富含芳烃的烃流与烷基化剂接触以产生烷基化芳族物流，或者在催化剂存在下使富含芳烃的烃物流与脂肪族化合物或甲醇反应，生成甲基化芳族物流。 将烷基化芳族物流，甲基化芳族物流或二者分离成至少一个苯物流，甲苯物流和二甲苯物流。
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公开(公告)号：US20150136655A1
公开(公告)日：2015-05-21
申请号：US14470274
申请日：2014-08-27
Applicant: UOP LLC
Inventor： John Q. Chen , Peter K. Coughlin , Stanley J. Frey , James A. Johnson , Vasant P. Thakkar
Abstract: A process for producing hydrogen-rich coal tar includes introducing a coal feed into a pyrolysis zone, and contacting the coal feed with a hydrogen donor stream and a multifunctional catalyst in the pyrolysis zone. The multifunctional catalyst includes a hydrogenation function for increasing a hydrogen content of said coal tar stream. The process further includes pyrolyzing the coal feed with the hydrogen donor stream and the multifunctional catalyst to produce a coke stream and a coal tar stream comprising hydrocarbon vapor.
Abstract translation: 一种生产富氢煤焦油的方法包括将煤进料引入热解区，并使煤进料与热解区中的供氢物流和多官能催化剂接触。 多功能催化剂包括用于增加所述煤焦油流的氢含量的氢化功能。 该方法还包括用供氢物流和多功能催化剂热解煤进料以产生焦炭流和包含烃蒸气的煤焦油流。
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Patent Agency Ranking
公开(公告)号：US20150136580A1
公开(公告)日：2015-05-21
申请号：US14468746
申请日：2014-08-26
Applicant: UOP LLC
Inventor： Peter K. Coughlin , John Q. Chen , Stanley J. Frey , James A. Johnson , Vasant P. Thakkar
CPC classification number: C10C1/08 , C10B57/08 , C10B57/12 , C10C1/205 , C10J3/00 , C10J2300/093 , C10J2300/0959 , C10J2300/0976 , C10J2300/1659 , C10K3/04
Abstract: A process for pyrolyzing coal using a recycled hydrogen donor includes introducing a coal feed to a pyrolysis zone and heating the coal feed to a temperature of about 300° C. in the absence of hydrogen. A hydrogen donor solvent is introduced to the pyrolysis zone after the coal feed is heated to about 300° C., and the temperature of the coal feed and the hydrogen donor solvent is increased to about 475° C., while increasing a pressure in the pyrolysis zone to at or above a vapor pressure of the hydrogen donor solvent. At least an aromatic hydrocarbon rich fraction is separated from the coal tar stream and hydrogenated. The hydrogenated aromatic hydrocarbon rich fraction is recycled to the pyrolysis zone as the hydrogen donor solvent.
Abstract translation: 使用再循环氢供体来对煤进行热解的方法包括将煤进料引入热解区并在不存在氢的情况下将煤进料加热到约300℃的温度。 在将煤进料加热至约300℃之后，将氢供体溶剂引入热解区，并将供煤和供氢溶剂的温度升高至约475℃，同时增加 热解区至等于或高于氢供体溶剂的蒸气压。 至少一种富含芳烃的级分与煤焦油流分离并氢化。 氢化富芳烃馏分作为氢供体溶剂再循环到热解区。
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公开(公告)号：US09162952B2
公开(公告)日：2015-10-20
申请号：US14472152
申请日：2014-08-28
Applicant: UOP LLC
Inventor： Deng-Yang Jan , Robert L. Bedard , John Q. Chen , Peter K. Coughlin , Jayant K. Gorawara , James A. Johnson , Gregory F. Maher , Dean E. Rende , Vasant P. Thakkar
CPC classification number: C07C37/82 , C07C7/005 , C07C7/10 , C07C7/12 , C07C7/13 , C07C37/007 , C10C1/18 , C10C1/20 , C10G1/045 , C10G19/00 , C10G2300/1051 , C07C39/02 , C07C39/07 , C07C15/24
Abstract: A process for purifying at least one product from coal tar is described. The process involves separating a coal tar fraction having a boiling point in the range of about 180° C. to about 230° C. into an acidic portion and a non-acidic portion by contacting the fraction with a caustic compound. The acidic portion is separated into a cresol portion and a xylenol portion, and the non-acidic portion is separated into a naphthalene portion and a naphthalene co-boiler portion. The acidic portion and the non-acidic portions are separated by contacting with an adsorbent comprising small, discrete crystallites, the adsorbent having less than 10 wt % amorphous binder component. The various portions can be separated in a similar manner.
Abstract translation: 描述了从煤焦油中纯化至少一种产物的方法。 该方法包括通过使馏分与苛性化合物接触，将沸点在约180℃至约230℃的煤焦油馏分分离成酸性部分和非酸性部分。 将酸性部分分离成甲酚部分和二甲苯酚部分，将非酸性部分分离成萘部分和萘共沸点部分。 通过与包含小的离散晶体的吸附剂接触来分离酸性部分和非酸性部分，吸附剂具有小于10重量％的无定形粘合剂组分。 可以以类似的方式分离各个部分。
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公开(公告)号：US09162943B2
公开(公告)日：2015-10-20
申请号：US14718974
申请日：2015-05-21
Applicant: UOP LLC
Inventor： John Q. Chen , Peter K. Coughlin , Stanley J. Frey , James A. Johnson , Vasant P. Thakkar
CPC classification number: C07C5/3337 , C01B3/36 , C01B2203/0216 , C01B2203/0283 , C07C2/42 , C07C2/46 , C07C2523/40 , C10G9/00 , C10G11/00 , C10G51/023 , C10G51/04 , C10G57/00 , C10G57/02 , C10G69/00 , C10G69/04 , C10G69/06 , C10G2400/20 , C10G2400/30 , C07C15/02
Abstract: A method of processing a coal feed to produce aromatic hydrocarbon compounds includes providing a coal tar stream and converting the coal tar stream to a conversion product comprising at least olefins, paraffins, and aromatics. The process further includes separating the olefins and C5− paraffins from the conversion product, and contacting the separated olefins and the C5− paraffins with a catalyst to dehydrogenize, oligomerize, and cyclize the olefins and the C5− paraffins, to form aromatic hydrocarbon compounds.
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公开(公告)号：US20150251976A1
公开(公告)日：2015-09-10
申请号：US14718974
申请日：2015-05-21
Applicant: UOP LLC
Inventor： John Q. Chen , Peter K. Coughlin , Stanley J. Frey , James A. Johnson , Vasant P. Thakkar
CPC classification number: C07C5/3337 , C01B3/36 , C01B2203/0216 , C01B2203/0283 , C07C2/42 , C07C2/46 , C07C2523/40 , C10G9/00 , C10G11/00 , C10G51/023 , C10G51/04 , C10G57/00 , C10G57/02 , C10G69/00 , C10G69/04 , C10G69/06 , C10G2400/20 , C10G2400/30 , C07C15/02
Abstract: A method of processing a coal feed to produce aromatic hydrocarbon compounds includes providing a coal tar stream and converting the coal tar stream to a conversion product comprising at least olefins, paraffins, and aromatics. The process further includes separating the olefins and C5− paraffins from the conversion product, and contacting the separated olefins and the C5− paraffins with a catalyst to dehydrogenize, oligomerize, and cyclize the olefins and the C5− paraffins, to form aromatic hydrocarbon compounds.
Abstract translation: 一种加工煤原料以生产芳族烃化合物的方法包括提供煤焦油流并将煤焦油流转化为至少包含烯烃，链烷烃和芳族化合物的转化产物。 该方法还包括从转化产物中分离烯烃和C5-链烷烃，以及使分离的烯烃和C5-链烷烃与催化剂接触以使烯烃和C5-链烷烃脱氢，低聚和环化以形成芳族烃化合物。
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公开(公告)号：US20150251971A1
公开(公告)日：2015-09-10
申请号：US14718877
申请日：2015-05-21
Applicant: UOP LLC
Inventor： Stanley J. Frey , Paul T. Barger , Maureen L. Bricker , John Q. Chen , Peter K. Coughlin , James A. Johnson , Joseph A. Kocal , Matthew Lippmann , Vasant P. Thakkar , Kurt M. Vanden Bussche
CPC classification number: C07C4/18 , C07C4/06 , C07C7/12 , C07C2521/12 , C07C2529/06 , C07C2529/18 , C10B53/00 , C10C1/205 , C10G1/002 , C10G1/02 , C10G45/08 , C10G45/10 , C10G45/12 , C10G45/50 , C10G45/52 , C10G45/54 , C10G47/04 , C10G47/16 , C10G47/18 , C10G47/20 , C10G65/12 , C10G2300/1096 , C10G2400/30 , C07C15/06
Abstract: A process for selectively dealkylating aromatic compounds includes providing a coal tar stream comprising aromatic compounds and hydrotreating the coal tar stream to reduce a concentration of one or more of organic sulfur, nitrogen, and oxygen in the coal tar stream, and to hydrogenate at least a portion of the aromatic compounds in the coal tar stream. The process further includes hydrocracking the hydrotreated coal tar stream to further hydrogenate the aromatic compounds and to crack at least one ring of multi-ring aromatic compounds to form single-ring aromatic compounds. The single-ring aromatic compounds present in the hydrocracked stream are then dealkylated to remove alkyl groups containing two or more carbon atoms.
Abstract translation: 选择性地使烷基化芳族化合物的方法包括提供包含芳族化合物的煤焦油流并加氢处理煤焦油流以降低煤焦油流中的一种或多种有机硫，氮和氧的浓度，并将至少一种 煤焦油流中芳族化合物的一部分。 该方法还包括加氢裂化加氢处理的煤焦油流，以进一步氢化芳族化合物并裂解至少一个多环芳族化合物环以形成单环芳族化合物。 然后将存在于加氢裂化物流中的单环芳族化合物脱烷基化以除去含有两个或更多个碳原子的烷基。
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