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1.发明授权Method of preparing a transparent polumer material comprising a thermoplastic polycarbonate and mineral nanoparticles 有权制备包含热塑性聚碳酸酯和矿物纳米颗粒的透明聚合物材料的方法公开(公告)号：US09284422B2
公开(公告)日：2016-03-15
申请号：US12746011
申请日：2008-12-09
申请人： Virginie Boucher , Alexandra Roos , Sophie Duquesne , Serge Bourbigot , Laure Meynie , Karine Cavalier , Didier Sy , Marc Lacroix
发明人： Virginie Boucher , Alexandra Roos , Sophie Duquesne , Serge Bourbigot , Laure Meynie , Karine Cavalier , Didier Sy , Marc Lacroix
CPC分类号： C08J3/226 , B82Y30/00 , C08J5/005 , C08J2369/00 , C08J2425/00 , C08J2433/00 , C08J2469/00 , C08K3/26 , C08K5/005 , C08L25/04 , C08L33/12 , C08L69/00 , C08L2666/02
摘要： A method of preparing a transparent polymer material includes mixing mineral nanoparticles selected from nanoparticles of alkaline-earth metal carbonates, alkaline-earth metal sulfates, metallic oxides, oxides of metalloids, and siloxanes, and a composition A including at least one thermoplastic polymer in the molten state selected from polycarbonate (PC), polystyrene (PS) and polymethyl methacrylate (PMMA) in order to obtain a master-batch, the mixture of step i) including at least 25% and at most 75% by weight of the mineral nanoparticles. The master-batch obtained in step i) is mixed with a composition B of a thermoplastic polycarbonate matrix (PCm) in the molten state, to obtain a transparent polymer material including at most 10% by weight of the mineral nanoparticles, preferably at most 5% by weight of the mineral nanoparticles.
摘要翻译： 制备透明聚合物材料的方法包括混合选自碱土金属碳酸盐的纳米颗粒，碱土金属硫酸盐，金属氧化物，准金属氧化物和硅氧烷的矿物纳米颗粒和包含至少一种热塑性聚合物的组合物A 选自聚碳酸酯（PC），聚苯乙烯（PS）和聚甲基丙烯酸甲酯（PMMA）的熔融状态，以获得母料，步骤i）的混合物包含至少25重量％至多75重量％的矿物纳米颗粒 。 将步骤i）中获得的母料与熔融状态的热塑性聚碳酸酯基质（PCm）的组合物B混合，得到包含至多10重量％的矿物纳米颗粒的透明聚合物材料，优选至多5 重量％的矿物纳米颗粒。
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2.发明申请METHOD OF PREPARING A TRANSPARENT POLUMER MATERIAL COMPRISING A THERMOPLASTIC POLYCARBONATE AND MINDERAL NANOPARTICLES 有权制备包含热塑性聚碳酸酯和微粒纳米颗粒的透明聚合物材料的方法公开(公告)号：US20110034588A1
公开(公告)日：2011-02-10
申请号：US12746011
申请日：2008-12-09
申请人： Virginie Boucher , Alexandra Roos , Sophie Duquesne , Serge Bourbigot , Laure Meynie , Karine Cavalier , Didier Sy , Marc Lacroix
发明人： Virginie Boucher , Alexandra Roos , Sophie Duquesne , Serge Bourbigot , Laure Meynie , Karine Cavalier , Didier Sy , Marc Lacroix
CPC分类号： C08J3/226 , B82Y30/00 , C08J5/005 , C08J2369/00 , C08J2425/00 , C08J2433/00 , C08J2469/00 , C08K3/26 , C08K5/005 , C08L25/04 , C08L33/12 , C08L69/00 , C08L2666/02
摘要： A method of preparing a transparent polymer material includes mixing mineral nanoparticles selected from nanoparticles of alkaline-earth metal carbonates, alkaline-earth metal sulfates, metallic oxides, oxides of metalloids, and siloxanes, and a composition A including at least one thermoplastic polymer in the molten state selected from polycarbonate (PC), polystyrene (PS) and polymethyl methacrylate (PMMA) in order to obtain a master-batch, the mixture of step i) including at least 25% and at most 75% by weight of the mineral nanoparticles. The master-batch obtained in step i) is mixed with a composition B of a thermoplastic polycarbonate matrix (PCm) in the molten state, to obtain a transparent polymer material including at most 10% by weight of the mineral nanoparticles, preferably at most 5% by weight of the mineral nanoparticles.
摘要翻译： 制备透明聚合物材料的方法包括混合选自碱土金属碳酸盐的纳米颗粒，碱土金属硫酸盐，金属氧化物，准金属氧化物和硅氧烷的矿物纳米颗粒和包含至少一种热塑性聚合物的组合物A 选自聚碳酸酯（PC），聚苯乙烯（PS）和聚甲基丙烯酸甲酯（PMMA）的熔融状态，以获得母料，步骤i）的混合物包含至少25重量％至多75重量％的矿物纳米颗粒 。 将步骤i）中获得的母料与熔融状态的热塑性聚碳酸酯基质（PCm）的组合物B混合，得到包含至多10重量％的矿物纳米颗粒的透明聚合物材料，优选至多5 重量％的矿物纳米颗粒。
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3.发明授权Method for preparing a transparent polymer material including mineral nanoparticles with a shape factor strictly higher than 1.0 有权制备透明聚合物材料的方法，包括形状因子严格高于1.0的矿物纳米颗粒公开(公告)号：US08278382B2
公开(公告)日：2012-10-02
申请号：US13130677
申请日：2009-11-27
申请人： Virginie Boucher , Sophie Duquesne , Serge Bourbigot , Didier Sy , Marc Lacroix , Alexandra Roos , Nathalie Cornet , Laure Meynie
发明人： Virginie Boucher , Sophie Duquesne , Serge Bourbigot , Didier Sy , Marc Lacroix , Alexandra Roos , Nathalie Cornet , Laure Meynie
CPC分类号： C08J3/203 , B82Y30/00 , C08J3/201 , C08J5/005 , C08J2369/00 , C08K3/013 , C08L25/04 , C08L33/06 , C08L69/00 , C08L77/00 , C08L2666/02
摘要： The present invention provides a method of preparing a transparent polymer material, the method comprising steps i) and ii) in any order, the steps consisting in: i) mixing: mineral nanoparticles having a form factor strictly greater than 1.0; and a polymer matrix comprising a quantity of at least 80% by weight of a polycarbonate (PC) first thermoplastic polymer and of a second transparent thermoplastic polymer other than the first thermoplastic polymer, in order to obtain a mixture; and ii) heating the polymer matrix to the molten state, on its own or in the mixture; to obtain the transparent, polymer material, the mixture of step i) comprising a quantity of mineral nanoparticles having a form factor strictly greater than 1.0 that is strictly less than 5% by weight.
摘要翻译： 本发明提供一种制备透明聚合物材料的方法，该方法包括步骤i）和ii）以任何顺序，步骤包括：i）混合：具有严格大于1.0的形状因子的矿物纳米颗粒; 以及包含至少80重量％的聚碳酸酯（PC）第一热塑性聚合物和除第一热塑性聚合物之外的第二透明热塑性聚合物的量的聚合物基质，以获得混合物; 和ii）将聚合物基体自身或混合物加热至熔融状态; 为了获得透明的聚合物材料，步骤i）的混合物包含一定量的严格小于1.0的严格小于5重量％的形状因子的矿物纳米颗粒。
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4.发明申请METHOD FOR PREPARING A TRANSPARENT POLYMER MATERIAL INCLUDING MINDERAL NANOPARTICLES WITH A SHAPE FACTOR STRICTLY HIGHER THAN 1.0 有权制备透明聚合物材料的方法，其中包括具有严格高于1.0的形状因子的微量纳米颗粒公开(公告)号：US20110281989A1
公开(公告)日：2011-11-17
申请号：US13130677
申请日：2009-11-27
申请人： Virginie Boucher , Sophie Duquesne , Serge Bourbigot , Didier Sy , Marc Lacroix , Alexandra Roos , Nathalie Cornet , Laure Meynie
发明人： Virginie Boucher , Sophie Duquesne , Serge Bourbigot , Didier Sy , Marc Lacroix , Alexandra Roos , Nathalie Cornet , Laure Meynie
IPC分类号： C08L69/00 , C08K3/26 , C08K3/22 , C08K3/30 , C08K11/00 , C08L33/26 , C08L33/08 , C08L25/06 , C08K3/34 , B82Y30/00
CPC分类号： C08J3/203 , B82Y30/00 , C08J3/201 , C08J5/005 , C08J2369/00 , C08K3/013 , C08L25/04 , C08L33/06 , C08L69/00 , C08L77/00 , C08L2666/02
摘要： The present invention provides a method of preparing a transparent polymer material, the method comprising steps i) and ii) in any order, the steps consisting in: i) mixing: mineral nanoparticles having a form factor strictly greater than 1.0; and a polymer matrix comprising a quantity of at least 80% by weight of a polycarbonate (PC) first thermoplastic polymer and of a second transparent thermoplastic polymer other than the first thermoplastic polymer, in order to obtain a mixture; and ii) heating the polymer matrix to the molten state, on its own or in the mixture; to obtain the transparent, polymer material, the mixture of step i) comprising a quantity of mineral nanoparticles having a form factor strictly greater than 1.0 that is strictly less than 5% by weight.
摘要翻译： 本发明提供一种制备透明聚合物材料的方法，该方法包括步骤i）和ii）以任何顺序，步骤包括：i）混合：具有严格大于1.0的形状因子的矿物纳米颗粒; 以及包含至少80重量％的聚碳酸酯（PC）第一热塑性聚合物和除第一热塑性聚合物之外的第二透明热塑性聚合物的量的聚合物基质，以获得混合物; 和ii）将聚合物基体自身或混合物加热至熔融状态; 为了获得透明的聚合物材料，步骤i）的混合物包含一定量的严格小于1.0的严格小于5重量％的形状因子的矿物纳米颗粒。
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5.发明授权Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and surface-modified mineral nanoparticles 有权制备包含热塑性聚碳酸酯和表面改性矿物纳米颗粒的透明聚合物材料的方法公开(公告)号：US09163125B2
公开(公告)日：2015-10-20
申请号：US12744529
申请日：2008-12-09
申请人： Anne Christmann , Jean-Francois Hochepied , Jose-Marie Lopez-Cuesta , Laure Meynie , Alexandra Roos , Nathalie Cornet , Karine Cavalier , Didier Sy , Marc Lacroix
发明人： Anne Christmann , Jean-Francois Hochepied , Jose-Marie Lopez-Cuesta , Laure Meynie , Alexandra Roos , Nathalie Cornet , Karine Cavalier , Didier Sy , Marc Lacroix
CPC分类号： C08J5/005 , B82Y30/00 , C08J2369/00 , C08K3/22 , C08K3/26 , C08K5/5425
摘要： A method of preparing a transparent polymer material includes i) obtaining composite nanoparticles having mineral nanoparticles at least partially coated with at least one monomer and/or at least one polymer suitable for promoting physicochemical interactions at the interface between the mineral nanoparticles and a thermoplastic polycarbonate matrix, the mineral nanoparticles being surface-modified by the monomer and/or the polymer, either directly by grafting or directly by adsorption of the monomer and/or polymer onto the surface of the mineral nanoparticles; or via a coupling agent selected from a chlorosilane or an organosilane including a functional group that is capable of reacting by a radical pathway. The composite nanoparticles obtained in step i) are mixed with the thermoplastic polycarbonate matrix in the molten state to obtain the transparent polymer material.
摘要翻译： 制备透明聚合物材料的方法包括：i）获得具有至少部分地涂覆有至少一种单体和/或至少一种适于促进矿物纳米颗粒和热塑性聚碳酸酯基质之间的界面处的物理化学相互作用的至少一种聚合物的矿物纳米颗粒的复合纳米颗粒 ，矿物纳米颗粒由单体和/或聚合物进行表面改性，直接通过接枝或直接通过将单体和/或聚合物吸附到矿物纳米颗粒的表面上; 或通过选自氯硅烷或含有能够通过自由基途径反应的官能团的有机硅烷的偶联剂。 将步骤i）中获得的复合纳米颗粒与熔融状态的热塑性聚碳酸酯基质混合，得到透明聚合物材料。
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6.发明申请METHOD OF PREPARING A TRANSPARENT POLYMER MATERIAL COMPRISING A THERMOPLASTIC POLYCARBONATE AND SURFACE-MODIFIED MINERAL NANOPARTICLES 有权制备包含热塑性聚碳酸酯和表面改性矿物纳米粒子的透明聚合物材料的方法公开(公告)号：US20110034585A1
公开(公告)日：2011-02-10
申请号：US12744529
申请日：2008-12-09
申请人： Anne Christmann , Jean-Francois Hochepied , Jose-Marie Lopez-Cuesta , Laure Meynie , Alexandra Roos , Nathalie Cornet , Karine Cavalier , Didier Sy , Marc Lacroix
发明人： Anne Christmann , Jean-Francois Hochepied , Jose-Marie Lopez-Cuesta , Laure Meynie , Alexandra Roos , Nathalie Cornet , Karine Cavalier , Didier Sy , Marc Lacroix
CPC分类号： C08J5/005 , B82Y30/00 , C08J2369/00 , C08K3/22 , C08K3/26 , C08K5/5425
摘要： A method of preparing a transparent polymer material includes i) obtaining composite nanoparticles having mineral nanoparticles at least partially coated with at least one monomer and/or at least one polymer suitable for promoting physicochemical interactions at the interface between the mineral nanoparticles and a thermoplastic polycarbonate matrix, the mineral nanoparticles being surface-modified by the monomer and/or the polymer, either directly by grafting or directly by adsorption of the monomer and/or polymer onto the surface of the mineral nanoparticles; or via a coupling agent selected from a chlorosilane or an organosilane including a functional group that is capable of reacting by a radical pathway. The composite nanoparticles obtained in step i) are mixed with the thermoplastic polycarbonate matrix in the molten state to obtain the transparent polymer material.
摘要翻译： 制备透明聚合物材料的方法包括：i）获得具有至少部分地涂覆有至少一种单体和/或至少一种适于促进矿物纳米颗粒和热塑性聚碳酸酯基质之间的界面处的物理化学相互作用的至少一种聚合物的矿物纳米颗粒的复合纳米颗粒 ，矿物纳米颗粒由单体和/或聚合物进行表面改性，直接通过接枝或直接通过将单体和/或聚合物吸附到矿物纳米颗粒的表面上; 或通过选自氯硅烷或含有能够通过自由基途径反应的官能团的有机硅烷的偶联剂。 将步骤i）中获得的复合纳米颗粒与熔融状态的热塑性聚碳酸酯基质混合，得到透明聚合物材料。
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